Purpose: To observe the characteristic colors produced when certain metallic ions are vaporized. Metallic Ion Color in Flame Na+ Light Orange K+ Pink / Orange Li Red Ca2+ Dark Orange Sr2+ Red Cu2 Green Co+2 Salmon Pink Ammonium Dichlorate Orange Sparks K2CR2O7 Orange Fe+1 No Reaction NaCl Orange Strantium Chloride Scarlet Red Ni+2 Dark Orange Copper Sulfate (solid) Green Fe+2
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Determining Red 40 Concentrations Using Absorption with Beer’s Law Introduction I like color and enjoyed learning about wavelengths and the spectrum of light‚ so I considered incorporating something related to that into my Internal Assessment. We also had just used concentrations in our Group 4 Project‚ so when I found an experiment that dealt with both of these I thought it was a great idea. This experiment is not completely original; the basic concept has been used multiple times. It uses Beer’s
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the forming Butyl 2-Cyano-(3‚5 dichloro-phenyl)-2-propenoate. The analyses that were used to prove its composition and structure include; IR spectroscopy‚ thin layer chromatography (TLC)‚ and CHN analysis. A radical copolymerization reaction was conducted‚ with the initiation by radical initiator 1‚1’-azobiscyclohexanecarbonitrile. CHN analysis‚ IR spectroscopy‚ and Proton NMR analysis were used to prove its composition and structure. 1. Introduction The American Chemical Society databases were investigated
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compounds (Wikipedia may be helpful). What would be a good estimate for the pKa of Eugenol? Eugenol‚ pKa=10.19 at 25 degrees C. 3.) The recovered clove oil will be analyzed by Infrared Spectroscopy. What are the basic principles of Infrared Spectroscopy (can be included in the introduction if you prefer). How will we be able to distinguish between Eugenol and Acetyleugenol by IR sprectroscopy? Molecule atoms act like they are connected by flexible springs instead
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(III) chloride were synthesized and isolated. From the ultraviolet-visible spectrum‚ infrared spectrum‚ and molar conductivity each compounds was distinguished and characterized to show fundamental differences between the three. Furthermore‚ IR spectroscopy is suitable for distinguishing between the nitro- and nitrito-linkage isomers because they have different vibrational patterns from one another. Given enough time‚ the more stable thermodynamic linkage isomer [Co(NH3)5NO2]Cl2 will be formed as
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this experiment‚ the nature of linkage isomers will be observed on the example of nitritopentaamminecobalt(III) Chloride and nitropentaamminecobalt(III) Chloride. Their relative stability will be compared on standard conditions and the infrared spectroscopy of both the isomers will be obtained to analyze the characteristic absorption bands for the nitro and nitrito group. Yield for nitritopentamminecobalt(III) Chloride was obtained to be = 1.9221 g(73.24 %) and yield for nitropentamminecobalt(III)
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RAMAN inactive Liquid Particle Explorer: Number Size‚ Composition in Minutes Image Analysis 5µ m 9 Liquid Particle Explorer: Number Size‚ Composition in Minutes 8µ m Automated Spectroscopy 10 Liquid Particle Explorer: Number Size‚ Composition in Minutes RAMAN Spectroscopy laser spectrometer 11 nodge ccd- detector Liquid Particle Explorer: Number Size‚ Composition in Minutes Documentation data tracking 12
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The purpose of this lab was for students to familiarize and perfect the simple distillation method to produce 4-Methylcyclohexene and to gain experience using an IR spectroscopy to characterize the product of the reaction in favor of equilibrium. B. Results and Discussion: C. Experimental: 24 mL of 4-methylcyclohexanol‚ 5mL of phosphoric acid‚ and 1mL of concentrated sulfuric acid was added to a 250 mL round bottom flask and mixed thoroughly with a magnetic stirrer. A simple distillation
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New forensic laser technique for hair analysis Using a new laser technique‚ Jim Moran and his colleagues at Pacific Northwest National Laboratory‚ have devised a method of separating out the parts of hair samples that can reveal details about the recent history of the person to whom it belongs. In their paper‚ published in Rapid Communications in Mass Spectrometry‚ they describe a process they’ve devised whereby hair samples are pulled apart‚ rather than burned as a whole before being measured
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Experiment A Spectroscopic determination of Iron with Phenanthroline Unknown # 2 Mass of Mohr’s Salt: 0.2040 1. 5mL of 6M acetic acid was measured and transferred into a 100mL volumetric flask with a pipette and diluted to the mark. Concentration = [0.2040(±0.0001)g/100(±0.08)mL]*[(1mol/392.16g)/(1L/1000mL)] = 0.005202(±0.09382%) = 0.005202(±0.000005)mol/L 2. 10mL of the above stock solution was transferred to a 250 mL volumetric flask and diluted to the mark. Concentration
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