#15 Synthesis of Ethyl Salicylate from Salicylic Acid ____________________________________________________________ _______________ Purpose: Salicylic acid is converted to the liquid ethyl salicylate by addition of ethanol. Yields of salicylic acid (week 1) and ethyl salicylate will be found‚ as well as the overall yield of the 2-step conversion of acetyl salicylic acid to ethyl salicylate. Introduction: Esters are formed from the reaction of acids and alcohols: O O
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Experiment 15 & 16: Preparation of 1-bromobutane‚ an SN2 reaction Preparation of 2-chloro-2-methylbutane‚ an SN1 reaction Introduction The purpose of this experiment is to synthesize 1-bromobutane from 1-butanol and sodium bromide. In order for this reaction to reach completion there are four major operations that need to be performed. The four major operations include refluxing‚ simple distillation‚ separation‚ and drying. To begin‚ in order for the compounds to react they will be dissolved
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Rate of Evaporation of Different Liquids Objective of the Project This project is of the rate of evaporation of different liquid‚ in which we also discuss the factors which affect the rate of liquid. Introduction When liquid is placed in an open vessel. It slowly escapes into gaseous phase ventually leaving the vessel empty. This phenomenon is known as vaporization or evaporation. Evaporation of liquids can be explained in the terms of kinetic molecular model although there
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Subject: Experiment 23: Stereochemistry of the Addition of Bromine to trans-Cinnamic Acid Introduction/Abstract: The purpose of this experiment was to carry out the bromination of trans-cinnamic acid‚ to determine the stereochemistry of the dibromide product of 2‚3-dibromo-3-phenylpropanoic acid‚ and find out whether the reaction proceeds by the usual bromonium ion mechanism or some other mechanism. In this experiment trans-cinnamic acid was mixed with glacial acetic acid and stirred in which
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Glycerin has an impartial‚ sweet-tasting‚ lackluster‚ thick fluid which hardens to a sticky glue and which has a high breaking point. Glycerin can be broken down in water or liquor‚ however not oil. Interestingly‚ numerous things will disintegrate into the glycerin simpler than they do into water or liquor. So it is a decent dissolvable. Glycerin is additionally exceptionally "hygroscopic" which implies that it ingests water from the air. An illustration if left a jug of unadulterated the glycerin
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Working out mean or average results 26.3+26.1+23.8= 76.2/3=25.4 The average ml of HCL needed in order to react for a colour change was 26.5ml. NaHCo3+ HCl NaCl+H2O+Co2 Calculation: 25 ml 0.1 mole dm3 26.3+26.1+23.8= 76.2 ml 76.2÷3=25.4÷1000=0.025 volume 0.1x0.25ml=0.025 moles 0.025÷0.254=0.98 (Rounded up to one decimals places) =0.1 M To begin with concentration I have choose three volumes form my results table which I have added them and then divided by three to get an average results. Describe
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Introduction A polymer is a large molecule comprised of numerous smaller molecules. It is possible for these large molecules to be linear‚ moderately branched‚ or highly interconnected. In the latter case the structure progresses into a large three-dimensional complex. The small molecules that serve as the basic building blocks for these large molecules are known as monomers (See Figure 1.1). An example of the relationship between a monomer and polymer is the commercially important material polyvinylchloride
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Organic Chemistry Experiment - Hydrocarbons Thursday‚ April 12‚ 2007 1:34 PM Purpose: To Identify an unknown Hydrocarbon Procedure: Procedure listed in handout "Organic Chemistry Experiment -- Hydrocarbons" Hazards: Open flame and hydrocarbons are flammable. Equations: 1. . 3. . 4. . 5. . Unknown #: 1B s-6 Hyd-3 (colorless liquid) Data/Observations: Test Bromine addition Alkane Mixture of hexane and dichloromethane was originally clear liquid. After adding 3 drops red color Br2/CH2Cl
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EXPERIMENTAL DETAILS All chemicals used were Merck reagent grade. Solutions were formulated with chromium sulfate (Cr¬2(SO4)3.6H2O) as chromium source in the quantities presented in (Table 1); Solutions were heated to 60°C for three hours during complexation reaction as in [29]‚ and pH was adjusted to 3 units without HCl or NH3 . Table1- electrolyte and electrodeposition parameter The coatings were deposited on a 1 x 1.5 cm2 cooper plate sample. Preparation for all specimens was as follow: Firstly
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Acetylsalicylic acid is the active pharmaceutical ingredient in aspirin and can be synthesized by the esterification reaction of salicylic acid and acetic anhydride in the presence of an acid catalyst. An esterification reaction is when an acid is converted into an ester by combining with an alcohol and removing a water molecule. When heating the salicylic acid mixture in the warm water bath‚ the mixture should be removed from the bath within 8 minutes‚ to reduce the chance of the acetylsalicylic
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