3.3. Characterization of the S2 VNP loaded liquid SNEDDS 3.3.1. Assessment of self-emulsification efficiency The emulsification time for S2‚ which is the time needed for SNEDDS to form homogeneous transparent mixture upon dilution‚ was 12 sec when 1 gm of VNP SNEDDS was added to 200 ml of 0.1 N HCl. When the same experiment was performed but by using 500 ml distilled water‚ the time required for the complete disappearance of SNEDDS was 14 sec. The emulsification in both media is under grade A of
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The kinetic equation‚ half-life values‚ correlation coefficient and pre-harvest interval (PHI) of the trifloxystrobin and tebuconazole residue dissipation were calculated from the experimental data and summarized in Table 4. The dissipation dynamics of trifloxystrobin on green tea leaves followed a first-order rate equation as follows C = 2.5472e-0.245x (r=0.9797) and C = 6.5457e-0.207x (r= 0.9804) with the half-life of 2.83 and 3.34 days for trifloxystrobin at RD and DRD‚ respectively. The half-life
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What is the Difference between Flammable and Combustible Liquids? Put simply‚ flammable and combustible liquids are liquids that can burn. The real difference lies within their flash point range‚ or lowest temperature at which vapours of the material will ignite when supplied with an ignition source. Flammable and combustible liquids are utilised in most workplaces‚ from manufacturing to retail and service entities. To ensure the safety of property‚ people‚ and the environment‚ both flammable
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1.1.1 Galacturonic Acid Analysis (for Pectin Analysis) Defattening of Mango Peel Powder (Tunchaiyaphum et al.‚ 2013) 1. Weigh about 3 g sample and put into thimble of the soxhlet extractor. 2. Pour in 150 mL of absolute ethanol to the flask of the soxhlet extractor. 3. Extract at boiling temperature of ethanol for 4 hours. 4. Remove solid contents from the thimble. Set aside to dry. Acid Hydrolysis of MPP (Rehman et al.‚ 2004) 1. Mix defatted peel powder with water at pH 2.5 adjusted w/ 0.1 N H2SO4
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For the first part of the experiment‚ it began by weighing 4.0ml of methyl salicylate into a flask—a stir bar was added. While stirring‚ 40ml of 6M sodium hydroxide was added and the solution was heated and boiled for about 15 minutes. After the 15 minutes‚ a bit of water was used to wash down the sides of the flask and the solution was cooled. It was boiled for another 15 minutes‚ after this the solution was cooled for 5 minutes in an ice water bath. While the flaks was in the ice bath‚ 50ml of
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1. The Tums tablet is insoluble in water. The water turns foggy when the Tums tablet is added. The particles of the tablet are suspended in the water‚ therefore the water appeared foggy and opaque. The Alka-Seltzer is soluble in water. The ingredients of Alka-Seltzer and the water react together to produce gas‚ thus bubbles formed in the solution. Whereas‚ the Rolaids tablet did not dissolve in water. The powder remained afloat on the surface of the water. Unlike the Tums tablet‚ Rolaids does not
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In this lab‚ caffeine was extracted from black tea‚ and green tea through a vacuum filtration‚ and a rotovap. The melting point of the sample of black tea was 219.12-236.05 ˚c‚ and for the green tea it was 176.22-227.6 ˚c. The % error of the melting point indicates how much error there was from the melting point taken experimentally. The % error of the melting point for black tea was 0.44%‚ and for green tea it is 3.15%.Since the theoretical melting point of caffeine is between 235-237 ˚c‚ we can
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Compound Molecular Structure Molecular Weight (g/mol) Melting point (0C) Solubility Hazard Sulfuric acid (H2SO4) 98.079 10 Miscible in water Hazardous in case of eye contact (irritant)‚ of ingestion‚ of inhalation. Slightly hazardous in case of skin contact (irritant) Ammonium Bromide (NH4Br) 97.94 452 Soluble in water Hazardous in case of eye contact (irritant)‚ of ingestion‚ of inhalation. 1-Butanol (C4H10O) 74.12 -89.8 Soluble in water. Very soluble in acetone‚ miscible with ethanol‚
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The Physical Properties of Eleven Chemical Compounds Problem: Discover whether various chemical compounds are molecular or ionic and if they are acidic or basic. Hypothesis: If the compound is ionic‚ then it will be soluble because the energy given off water molecules compensates for the energy needed to break ionic bonds‚ also‚ if the compound is Ionic‚ it will be an electrolyte‚ because they mostly break up into ions when in water. If the compound is molecular‚ then it will be soluble‚ it cannot
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Laboratory report Experiment one Acetylation of α-D- glucopyranose 1. Reagents (1)2.5g(0.014mol) powdered D-glucose (2)0.5g ZnCl2 (3)12.5ml acetic anhydride (4)Cold water (5)120ml Ice water (6)Methanol 2. Physical properties Compounds | M.W. g/mol | M.P.℃ | B.P.℃ | Density g/cm3 | D-glucose | 180.16 | 146 | - | 1.54 | ZnCl2 | 136.315 | 292 | 756 | 2.907 | Acetic anhydride | 102.9 | -73.1 | 139.8 | 1.082 | Methanol | 32.04 | -98~-97 | 64.7 | 0.7918 | α-D-
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