(mol) Theoretical moles of Product (mol) Theoretical mass of Product (g) Actual Mass of Product (g) % yield 〖CuSO〗_4 (s) 1.992 g .0124 mol .0124 mol 3.047 g 2.640 g 86.64% Solubility of Precipitate ion [Cu(NH_3 )_4 ]SO_4*H_2 O+Solvent Observation of Solubility [Cu(NH_3 )_4 ]SO_4*H_2 O + Acetone When the precipitate ion was added to ~1 mL of acetone there was a strong property of insolubility. Even when a stir rod was used to mix the precipitate in the acetone‚ the
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solution‚ in the presence of high concentration of hydronium ions‚ protons will be transferred from the strong acid H3O+ to the basic benzoate ion. This will yield benzoic acid‚ C6H5COOH which precipitates from the solution as it has a really poor solubility (0.34g/100ml). The fundamental reaction is sketched out below: As can be seen from the difference in the pKa values‚ H3O+ is a much stronger acid than benzoic acid. So‚ the equilibrium of the reaction strongly favours its completion
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The solubility of calcium hydroxide Aim: to find out the solubility of a substance that only partially dissolves in water. Method: place about 100cm3 of distilled water in a flask and add about one spatula of solid calcium hydroxide. Stopper the flask and shake well for one minute. Leave to stand for at least 24 hours. Titrate 10cm3 samples against 0.05 mol dm-3 hydrochloric acid solution using methyl orange as an indicator. Obtain enough results to calculate an accurate average‚ and then
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EXPERIMENT 2: Recrystallization and Melting Point Recrystallization (or Crystallization) is a technique used to purify solids. This procedure relies on the fact that solubility increases as temperature increases (you can dissolve more sugar in hot water than in cold water). As a hot‚ saturated solution cools‚ it becomes supersaturated and the solute precipitates (crystallizes) out. In a recrystallization procedure‚ an impure (crude) solid is dissolved in a hot solvent. As this solution is cooled
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Lab report for Experiment #2: Extraction Your Name: Name of TA: Lab Partner’s Name: Lab Section: Title: Experiment #2: Extraction Purpose: What is the purpose of this lab? In your OWN words! Observations: Weighed out 3.2568 grams of chemical mixture that was yellow in color. Dissolved dry chemicals in 38 ml CH2Cl2 with gentle heating. Poured the yellow solution into sep funnel. Added 10 ml CH2Cl2 to flask to rinse‚ poured solution into sep funnel. Added 15 ml 3 M
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sulfanilamide that was recovered‚ and to determine the purity of the final product. Introduction In this experiment‚ recrystallization will be the method used to purify the solute sulfanilamide using ethanol as the solvent. Based on the solubility curve on the solubility versus temperature graph‚ the ideal solvent will allow the solute to be soluble at higher temperatures and insoluble at lower temperatures‚ thus making ethanol an excellent solvent for crystallizing sulfanilamide. Sulfanilamide
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Recrystallization of Benzoic acid Chemistry 204-002 Date: 4/9/2011 Hector Ortega Recrystallization is a method used to purify compounds‚ and this is a very important procedure because compounds are naturally impure. Polarity and solubility play a big role in this experiment and these characteristics are exploited in order to have a crystallization of the desired compound. In this experimented benzoic acid was crystallize using ethanol and water. I chose these solvents based on part C of the experiment
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Experiment18 Aim To determination the partition coefficient of ethanoic acid between water and butan-2-ol. Procedure 1. The room temperature was recorded. 2. 15cm3 of the given aqueous ethanoic acid and 15cm3 of butan-2-ol were poured into a 100cm3 separating funnel‚ using suitable apparatus. The funnel was stoppered and was shook vigorously for 1 to 2 minutes. (The pressure in the funnel was released by occasionally opening the tap.) 3. 10cm3 of each layer was separated
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solvent and state the purpose of each operation. 1] dissolve solid product in minimum volume of hot solvent .. Purpose ... to get into solution 2] cool solution in a mixture of ice‚ water and salt. Purpose .. to enable pure product to crystallise‚ solubility decreases with temp‚ so cold. Impurities are present in small quantities‚ so do not saturate and are left in solution. 2a] if it all sets solid‚ you haven’t used enough solvent‚ so add a little more and warm until everything dissolves. Purpose:
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STRENGTHENING OF METALS There are 4 major ways to strengthen metals‚ and all work because they make dislocation motion more difficult. They also reduce the ductility: 1) Cold work (Strain Hardening) 2) Reduce grain size (Strengthening by Grain Size Reduction) 3) Add other elements in solid solution (Solid Solution Strengthening) 4) Add second phase particles (Precipitation or Age Hardening) • These mechanisms may be combined. • For example‚ the world’s strongest structural material (with
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