All the reagents and solvents used for synthesizing the title compound were of Analar grade (Merck) and were used as such without further purification. The 2-naphthol derived Mannich base 1-((4-methylpiperazin-1-yl)(phenyl)methyl)naphthalen-2-ol (MPN) was synthesized according to the general procedure described in the literatures [13‚ 14]. The 2-naphthol (4.33 g‚ 0.03 mol) was dissolved in 30ml of ethanol and it was mixed with N-methylpiperizine (3.0 mL‚ 0.03 mol) by continuous stirrer at room
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6. FIRST DERIVATIVE ZERO CROSSING METHOD 6.1. ABSTRACT: Simple‚ specific‚ accurate and precise 1st order derivative zero-crossing spectroscopic method was developed for simultaneous determination of PHENYLEPHRINE and EBASTINE from their binary mixture. In this 1st derivative zero-crossing spectroscopic method the amplitudes of the 1st order derivative of the spectra of the binary mixture containing PHE and EBS were measured at 252.2 nm (zero crossing of EBS) for determination of PHE and at 274.8
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When it comes to providing a state-of-the-art‚ durable metal coating‚ there is no better option than powder coating. This unique process can protect vehicles‚ buildings and even smaller items such as patio furniture. So how does the powder coating process work? The experts at Powder Vision‚ Inc. in Issaquah‚ WA offer an inside look at their unique work process. Part Preparation: The first step to a successful powder coating is to remove dirt‚ oil and other contaminants from the parts that will be
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Spectrophotometric determination of Ascorbic acid Concentration in an Unknown Solution Introduction: The naturally occurring organic compound with antioxidant properties is Ascorbic acid shortly referred as (AA). Normally the color of Ascorbic acid is white‚ but in some cases of impure samples it appears yellow in color. Ascorbic acid is solid in state. In water it dissolves well to give mildly acidic solutions. Ascorbic acid is one form ("vitamer") of vitamin C [1]. So‚ Ascorbic Acid (AA)
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Aim: To react NaHCO3 with HCl to form NaCl and two other products and then calculate the mole relationships between NaHCO3 and NaCl and calculate a balanced equation for this reaction. Safety: • Wear safety goggles at all time • Handle all chemicals with care • Use equipment like tongs when handling warm/hot objects • If chemicals are spilt on self‚ wash off immediately • Stand at all times Hypothesis: The NaHCO3 will react successfully with the HCl and will form NaCl‚ H2O and
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Organic Lab Trial 1 Trial 2 Trial 3 Observations We added the 30ml of warm water with 4.7 grams of borax powder in to the cup labeled ‘Borax Solution’ and also added a few dots of green food coloring. We then stirred it until all the solutions were completely mixed. When this happened the borax and water turned into a watery green solution. then we added 15ml of glue in the cup labeled ‘Ball mixture’ and added the mixture we made
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Ashley Spees CHM 261- Batzer Chem Final Write Up- Kool Aid Lab Total Acid This part of the lab requires titration of Kool Aid with an NaOH solution. The reason titrations are used is to determine the concentration of an unknown solution by reacting a strong acid with a strong base. Titrations are hard to accomplish‚ though‚ due to the fact that indicators used to show the endpoints are very sensitive and one drop could make the solution titrate past its endpoint. Blue stock solution: 3 mg/L
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Alka-Seltzer Experiment Ideas 1.) Put Alka-Seltzer in different liquids and observe the reactions. 2.) Put Alka-Seltzer in different sealed containers (film canisters‚ sandwich bags‚ etc. and observe the reactions. 3.) Explore activity using Pop Rocks candy. 4.) Put Alka-Seltzer tablets into four different liquids (milk‚ orange juice‚ Coke‚ water) observe the reactions. 5.) Place Alka-Seltzer on a plate and pour a steady stream of water on it to see if it reacts any differently than
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Experiment #5: Acid Burn!!! Introduction The goal of this lab was to correctly prepare a 0.2M solution of NaOH‚ identify highly acidic household cleaning chemicals‚ and determine their concentration (molarity) through titrations using the previously prepared 0.2M NaOH solution. Experimental First‚ to create 0.5L of 0.2M solution of NaOH‚ standard 3M NaOH solution was obtained. Next‚ calculations were performed to determine the amount 3M NaOH necessary to create 0.5L of the 0.2M solution and‚ as
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Lab Report # 11 By: Andrew Hoitt CHEM 105 Lab 11/29/2012 Lab # 11 – Acid - Base Titration Introduction: The purpose of this lab is to determine the molarity (M) of an unknown HCl solution. A NaOH solution will be made and its molarity calculated. A sample of the NaOH solution will be titrated against the unknown HCl solution to calculated the volume needed to neutralize it. With these volumes the unknown molarity can be calculated. Theory: Solutions
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