In this experiment‚ we used methyl benzoate from the last experiment with HNO3 and H2SO4 to synthesize methyl 3-nitrobenzoate. First we added methyl benzoate to 12 mL cooled conc. Sulfuric acid in a flask. In a separate flask‚ we made a solution of 4 mL conc. Sulfuric acid and 4 mL nitric acid and then added dropwise to the solution of methyl benzoate in an ice bath on a stir plate while maintaining the temperature of reaction between 5-15 °C. After the addition was complete we took the flask out
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Sodium From Wikipedia‚ the free encyclopedia This article is about the chemical element. For the PlayStation Home game‚ see Sodium (PlayStation Home). For the racehorse‚ seeSodium (horse). "Natrium" redirects here. For the town in West Virginia‚ see Natrium‚ West Virginia. Sodium 11Na
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Partitioning of organic acid food preservatives between oil and water Olaya Iturbe Navalpotro Student of Food National Institute -DTU Technical University of Denmark Index 1. Introduction …………………………………………………………..pg. 2-4 2. Theoretical background……………………………………………….pg. 5-18 2.1. Preservatives (Sorbic acid and Benzoic acid) 2.2. Solubility and partitioning of food preservatives in food system 2.3. Measurements of the preservatives partitioning in oil-water system 2.4. Influences of
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Abstract: The Preservative effect of brine at different concentrations on lettuce at tropical ambient temperature was examined. The effect of various concentrations of salt solutions on leaf surface and edge browning‚ texture‚ and colour were observed for five days. The experiment was laid out in a Complete Randomized Design (CRD) and each treatment repeated in triplicates including a control. Sensory qualities were examined by six panelists using a 5-point hedonic scale ranking. Results indicated
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Sodium chloride‚ also known as salt‚ common salt‚ table salt‚ or halite‚ is an ionic compound with the formula NaCl. Sodium chloride is the salt most responsible for the salinity of the ocean and of the extracellular fluid of many multicellular organisms. As the major ingredient in edible salt‚ it is commonly used as a condiment and food preservative. [edit] Properties Thermal conductivity of pure NaCl as a function of temperature has a maximum of 2.03 W/(cm K) at 8 K and decreases to 0.069 at 314
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Nitration of Methyl Benzoate Introduction: Nitration is an example of an electrophile aromatic substitution reaction‚ where nitro (NO2) group is being substituted for a hydrogen on an aromatic compound. This is achieved by the formation of the nitronium ion by protonation of nitric acid from sulfuric acid. The zirconium ion is a strong electrophile and can react with aromatic compound such as Methyl benzoate to form an arenium ion intermediate. The arenium ion is then depronated to reform
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ABSTRACT This experiment was conducted to synthesize methyl benzoate form benzoic acid and methanol by using the Fischer esterification method. The Fischer exterification technique is utilized in the academic and industrial settings due to the simplified synthesis and safety parameters of the overall reaction. Both benzoic acid and methanol are relatively cheap to obtain from a commercial source as well as being easy to store with a relatively long shelf life. The Fischer esterification method is
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ring that a nucleophile could add to‚ referred to as the ortho‚ para‚ or meta positions. In this experiment‚ the nucleophile will primarily add into the meta position. This is because the starting material is methyl benzoate‚ as opposed to just benzene. The ester group of methyl benzoate is capable of participating in the resonance of the ring. This withdraws electron density from the benzene ring‚ and is said to be deactivating. Deactivating substituents destabilize the carbocation intermediates formed
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Sodium is a mineral that is present only in small quantities in most natural foods‚ but salt is added‚ often in large amounts‚ in food processing and by cooks to enhance flavor. Sodium is the predominant ion in extra cellular fluid. Sodium (Na) is the predominant cation in extra cellular fluid and its concentration is under tight homeostatic control. Excess dietary sodium is excreted in the urine. The kidney very efficiently reabsorbs the mineral when intakes are low or losses are excessive. Sodium
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Nitration of Methyl Benzoate Abstract: This procedure demonstrates the nitration of methyl benzoate to prepare methyl m-nitrobenzoate. Methyl benzoate was treated with concentrated Nitric and Sulfuric acid to yield methyl m-nitrobenzoate. The product was then isolated and recrystallized using methanol. This reaction is an example of an electrophilic aromatic substitution reaction‚ in which the nitro group replaces a proton of the aromatic ring. Following recrystallization‚ melting point and infrared
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