precipitated into silver chloride through precipitation gravimetry. The colloidal silver chloride originally formed was converted to a crystalline solid by controlling certain parameters of the experiment such as temperature‚ pH of the solution‚ and concentration of AgNO3. Once the solid was large enough‚ it could be washed‚ filtered‚ and weighed. The percentage of chloride present was found to be 24.73695223 (±0.00000006) %. Introduction The purpose of this lab was to determine
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(2013) Report By: ____________ Lab Partner: ___________ Group: CHEM 1001 Tuesday AM‚ Group H Purpose: This lab was conducted in order to determine the content of chloride in an unknown salt‚ using gravimetric analysis. Theory: The salt chloride content is easy to find because it is slightly soluble‚ making it possible to turn it into a precipitate. A precipitate reaction can be done using silver to isolate the specific ion. Ag+(aq)
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salt. Theory: AgCl(s) is a very insoluble solid‚ yet still does have some solubility. Because of these traits‚ the following reaction is able to occur: Ag+(aq) + Cl−(aq) → AgCl(s) . This reaction is able to occur in both directions. When a soluble silver salt such as AgNO3 is added to a solution containing Cl−(aq) ion‚ then the added Ag+(aq) precipitates as AgCl(s) until all the chloride is consumed. For this particular reaction K sp = 1.6 x 10−10. The reason why the solution is precipitated in
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Fingerprints KEY Chemical Reaction Silver nitrate (AgNO3) can react with the salt (NaCl) left from the perspiration on the friction ridge skin to form solid silver chloride (AgCl) and sodium nitrate. The silver chloride can then be converted to silver oxide (Ag2O)‚ which is dark in color and can be more easily seen. Challenge Suppose the fingerprint processing technique that uses silver nitrate to react with the salt from perspiration produced 5.8 x 10-2 grams of silver chloride. How many grams of salt
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The History and technology of Opalotypes Fig 1; Unknown‚ date unknown Opalotype 383 x 280mm; From the collection of CCMC; Introduction The Opalotype consists of almost any photographic technique as long as it used on opal glass. It was in use from the mid 1800 ’s through to the1930 ’s and most of the methods of photographic production that were used during the 19th century were tried out with opalotypes. However despite it ’s long-lived history‚ Opalotypes are sadly treated as a very minor
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flammable 1-chlorobutane 92.58 78 -123 0.881 Irritant‚ Flammable 2-chlorobutane 92.57 68 -140 0.870 Flammable‚ Irritant 2-bromobutane 137.02 91 -112 1.250 Flammable‚ Irritant Ethyl Alcohol 46.07 79 -114 0.789 Flammable‚ Irritant Silver Nitrate 169.87 444 212 4.350 irritant Sodium Iodide 149.89 1300 651 3.667 irritant water 18.02 100 at 1atm 0 at 1atm 0.997 none Procedure See Introduction to Organic Laboratory Techniques: A Microscale Approach‚ 5th edition by Pavia‚ Lampman
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results | Constant: Volume of urine and silver nitrate solution | cm3 | Use 2cm3 of urine for each sample and 10cm3 of silver nitrate solution for every trial. | If different volumes of urine sample and silver nitrate solution are used‚ the concentration of the mixture will be different and this will affect the end result of the experiment. | Concentration of potassium thiocyanate and silver nitrate | M | 0.1 M of potassium thiocyanate and silver nitrate are used. | A higher concentration will
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Acetone is a good solvent for Sn2 reactions because it is a polar aprotic solvent. We will be examining Sn2 reactions with an ethanolic solution of silver nitrate. The silver ion coordinates with a lone pair on the halogen which begins to weaken the carbon-halogen bond. In the rate determining step‚ the carbocation and solid silver halide is formed. We will monitor the reaction by looking for the formation of the solid. R X Ag+ R X Ag R+ + AgX Procedure: Sn2 Assemble
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Sample Analysis. Precipitates and Complexes of Silver Ion Data for Determining Formulas Solutions containing NH3‚ CO32–‚ Cl–‚ I–‚ PO43–‚ and S2O32– ions were added to equal proportions of a silver nitrate solution‚ which contained the complex ion Ag(H2O)2+. All of the added solutions were also clear and colorless. |AgNO3 (aq) by itself |Colorless solution | |AgNO3 (aq) with NH3 (aq)
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Radha Shukla Determination of the Empirical Formula of Silver Oxide Will/Radha College Chemistry 9/12 – 9/13 9/17 The purpose of this lab is to use one of the ways to identify different compounds and be able to tell them apart. Based off of experimentation‚ the empirical formula of the given silver oxide will be determined. Materials: Chemicals: Silver Oxide‚ 0.5g Equipment: Balance‚ 0.001-g or 0.0001-g precision Bunsen Burner Clay pipestem triangle Crucible and cubicle lid‚ 15-
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