Objective: The objective of this experiment is to use acid-base extraction techniques to separate a mixture of organic compounds based on acidity and/or basicity. After the three compounds are separated we will recover them into their salt forms and then purify them by recrystallization and identify them by their melting points. Procedure: Extraction of Carboxylic Acid A pre-weighed (0.315g) mixture of Carboxylic acid‚ a phenol‚ and neutral substance was placed into a reaction tube (tube 1).
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12:30-4:30 Hyejin Cho 12 June 2013 Separation of a Mixture Abstract: In this experiment‚ the three processes of extraction‚ sublimation and recrystallization will be used to separate a mixture of salicylic acid and naphthalene. The first part of extraction will be to separate the salicylic acid from the naphthalene using diethyl ether and aqueous sodium bicarbonate. The naphthalene will reside in the ether and be the top layer‚ while the salicylic acid resides in the sodium bicarbonate bottom
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[pic] Soap From Wikipedia‚ the free encyclopedia Jump to: navigation‚ search For other uses‚ see Soap (disambiguation). [pic] [pic] A collection of decorative soaps‚ often found in hotels [pic] [pic] Two equivalent images of the chemical structure of sodium stearate‚ a typical soap. In chemistry‚ soap is a salt of a fatty acid.[1] Soaps are mainly used as surfactants for washing‚ bathing‚ and cleaning‚ but they are also used in textile spinning and are important components of lubricants
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39. The Viscosity of Liquids After studying the present lecture‚ you will be able to Define viscosity and viscosity coefficient Outline the method to measure viscosity using Ostwald viscometer Determine the average molecular weight of a polymer Determine the surface concentration of 1-butanol in aqueous solution Measure the distribution coefficient of a solute betweenn two solvents 39.1 Introduction Viscosity‚ one of the transport properties‚ arises because of intermolecular attractive and
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LIQUID CRYSTALS Introduction What are Liquid crystals ? Its History & Discovery Any of various liquids in which molecules are regularly arrayed like a solid crystal along one or two dimensions‚ but are free in the other dimensions as with typical liquids. Liquid crystals often display unusual and often manipulable optical properties such as anisotropic scattering. They can be divided into two classes‚ Thermo tropic(nematic‚ chiral nematic‚ and smectic.) and Lyotropic. Transitions to thermotropic
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The Little Heat Engine: Heat Transfer in Solids‚ Liquids and Gases The question now is wherein the mistake consists and how it can be removed. Max Planck‚ Philosophy of Physics‚ 1936. While it is true that the field of thermodynamics can be complex‚1-8 the basic ideas behind the study of heat (or energy) transfer remain simple. Let us begin this study with an ideal solid‚ S1‚ in an empty universe. S1 contains atoms arranged in a
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Introduction: The theory behind the extraction of a solution containing benzoic acid‚ cellulose‚ and methyl orange involves many components pertaining to the fundamental ideas of solubility and polarity. Using the concepts of like dissolving like and acid base reactions‚ a solution of organic acid (benzoic acid)‚ a water soluble compound cellulose‚ and an organic soluble compound methyl orange‚ can be separated and benzoic acid can be isolated by a method of extraction. At the fundamental level
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experiment two solutions are used. According to the definition of viscosity mobile liquids have a relatively low viscosity. Fluidity is the reciprocal of viscosity‚ given as equation 1: F=1/ η. Fluidity is advantageous because solutions of mixed solutions of nonassociating liquids are roughly additive. In this experiment binary solutions are used‚ so if each pure liquid has fluidities Fa and Fb‚ the fluidity of a mixture is given by: Equation1 (Halpern‚ 17-3).
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for later experiments. This experiment involves the separation of benzoic acid from a more crude form‚ consisting of benzoic acid‚ methyl orange‚ a common acid/base indicator‚ and cellulose‚ a natural polymer of glucose (Huston‚ and Liu 17-24). The technique that is used to perform this separation is called extraction. Extraction is a systematic process of separating mixtures of compounds‚ taking advantage of the affinity differences of compounds to separate them (Padias 128-37). This technique recognizes
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EXPERIMENT 13： Extraction: Extraction with acid and alkali Objective 1. To recover the benzoic acid and p-dichlorobenzene from its mixture from its mixture by using acid-alkali extraction. 2. To determine the percentage recovery and melting point of the recovered benzoic acid and p-dichlorobenzene. Introduction Acid-base extraction is a process which purifying the acids and bases from mixtures based on their chemical properties. Acid-base extraction is performed to isolate the compounds and natural
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