Chromatography Lab Questions Pre-Lab Questions 1. A pencil is used rather than a pen to mark the “starting line” in step two because a pen or marker while be used to place a small dot of ink in the center of the X that is made with a pencil. 2. Capillary action is filling of pores in a solid with a liquid. Capillary action is caused by spotting or absorption and is allowed to seep or flow through. 3. The type of pen that will probably give better separation in this paper chromatography
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Introduction Table of Contents Introduction Materials Chemicals Equipment Safety Containers Measuring Devices Other Equipment Procedure Synthesis of Aspirin Crystalizing the Aspirin Recrystallizing the Crude Aspirin Finding the Melting Point Range Safety Precautions Acetic Anhydride Sulphuric and Salicylic Acid Heating Observations Mass of Aspirin Synthesized Melting Point Calculations Percentage Yield Maximum Yield Crude Product Final Product Melting Range Percentage
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Stoichiometry lab By: James Stewart Purpose: To calculate mole ratios Introduction: There are two types of chemical analysis; qualitative analysis which is the identification of a substance present in a material‚ and qualitative analysis which measures the amount of the substance. In this lab‚ you will perform a quantitative analysis of a two-step reaction. Copper(II) oxide will be synthesized from a known mass of copper(II) sulfate pentahydrate. Using the relationship of the balanced equation
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Calorimetry To determine the specific heat of a metal and its approximate atomic mass. To determine the heat of neutralization for a strong acid-strong base reaction. To determine the quantity and direction of heat flow for the dissolution of salt. Post Lab Questions and Answers: 1. In parts A and B in‚ the calorimeter‚ although a good insulator‚ absorbs some heat when the system is above room temperature. Is the reported value for the specific heat of the metal too high or too low? Explain. Is the reported
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rapid separation of compounds‚ and gives an indication of the number and nature of the components of a mixture. TLC can also be used to identify compounds by comparison with known samples‚ to check the purity of a compound‚ or to monitor the progress of a reaction‚ an extraction‚ or a purification procedure. This experiment will introduce you to the mechanics of TLC‚ and the chemical principles behind it. TLC is normally done on a small glass or plastic plate coated with a thin layer of a solid — the
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Name Lab Section GTA Station # 5. Extraction Pre-lab questions Complete the following questions and submit before beginning the experiment. 1. Which layer will be the aqueous layer when using dichloromethane (methylene chloride) as the solvent (i.e.‚ top or bottom)? Which layer will be the aqueous layer when using ether as the solvent? 2. When everything has been separated in Part D‚ which compounds will be in test tubes 1‚ 2‚ and 3?
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of the specialized underlying structures of these life-forms. In order for us to appreciate these special adaptation‚ we first need to know how a typical plant or an animal cell organelle behaves in different water and solute concentrations. In this lab‚ we will determine the effects of hypertonic‚ isotonic and hypotonic solutions on plant and animal cells. In general when an animals cell’s placed in hypertonic solution it shrivels; a plant cell on the other hand undergoes plasmolysis. When an animal
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A Report of Experiment 1 Purification and Identification of An Unknown Mixture Aim To separate a mixture of a neutral (ester‚ alcohol‚ ketone‚ aldehyde or ether) and an acidic compound (phenol or carboxylic acid) or a neutral and a basic compound (amine)‚ and to identify the unknown mixture by physical (M.P. or B.P.) and spectroscopic methods (NMR‚ IR and MS). Method The mixture (sample number: 27) was dissolved in 200 mL of CH2Cl2 and then extracted with 10% NaOH. The acid was removed
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Lab Report for Chemical Changes and Conservation of Mass Lab Previous to the reaction‚ the magnesium appeared to be a solid‚ white‚ black‚ and grey substance with many small dark particles within the substance. The hydrochloric acid was a clear liquid that looked like water It weighed 42.2 grams in total. During the reaction‚ the two substances produced bubbles‚ creating smoke and became warm with a smell that is irritating to the human nose. After the reaction‚ it appeared to be a clear‚ bubbly
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Due to rapid urbanization and uncontrolled growth rate of population‚ solid waste management has become acute in India. The current practices of the uncontrolled dumping of waste on the outskirts of countries have created a serious environmental and public health problem where as many issues. Plastic waste which is biggest problem in waste management is recycled in India in an “unorganized” way. 60% of the plastic-waste collected and segregated gets recycled back into materials for further processing
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