Standardization and Titration of an Unknown Organic Acid Overview: Methods for counting the number of molecules in a sample is a major emphasis of laboratory work. In this experiment we will use the method of titration to count the number of acid molecules in a solution. Measuring mass is a relatively easy procedure to do in the lab (although a balance is expensive). Counting the number of particles requires more effort. Molecular counting can be done by setting an unknown amount of a substance equal to
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surroundings are mixtures of two or more substances in which each substance retains its own chemical identity and therefore its own properties. Mixtures are either homogeneous or heterogeneous. Mixtures that don’t have the same composition‚ properties‚ and appearance throughout the mixture are called Heterogeneous. Mixture that are uniform in composition‚ properties‚ and appearance throughout are called homogeneous. Sugar water is a homogeneous mixture and rocks is a heterogeneous mixture. Homogeneous
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this experiment is to separate a solution of an acidic and organic compound and purify its respective acidic product through the techniques of an acid base extraction‚ recrystallization‚ and use of Melt Temp (melting point range). The reaction of an unknown acid (3-chlorobenzoic acid) with diethyl and sodium hydroxide was observed‚ and the solution naturally separated into an aqueous and organic solution. The mixture of acid and organic solution was created and then separated through the Hirsch
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Experiment 2: Separation of a Mixture of Solids Purpose: This experiment allowed me to learn different separation techniques for various substances based on their specific chemical properties. Procedure: I began this experiment by using a magnet to pick up and collect the iron filings out of the mixture. Then the sand was separated by placing the mixture into a beaker and boiling it in distilled water in order to dissolve the salt and benzoic acid‚ once boiling the liquid was poured out leaving
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Experiment 1: Solubility of Organic Compounds (Answers to Questions) Q1. State what types of inetmolecular forces are present in solutions formed due to intermolecular attractions between the solute and the solvent. A1. For Water-Soluble Compounds: Acetone – Water: Hydrogen bonding and van der Waals forces Acetone – Diethyl Ether: Dipole – (induced) dipole and van der Waals forces Sucrose – Water: Hydrogen bonding and van der Waals forces Ethyl alcohol – Water: Hydrogen bonding
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Determination of Unknown Acid KEYWORDS: quantitative analysis‚ titration‚ buret‚ endpoint‚ standardization‚ half-equivalence point‚ calorimetric titration‚ potentiometric titration ABSTRACT: The concentration of sodium hydroxide was determined by colorimetric titration‚ and the identity of an unknown acid was determined by potentiometric titration. In the first titration‚ a strong acid standard‚ potassium hydrogen phthalate (KHP)‚ was used‚ to determine the concentration of a strong base‚ sodium hydroxide
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Separation Lab Purpose: This lab was based on the separation of the components of a mixture. A mixture can be defined as a physical combination of two or more pure substances. Separation techniques are used to separate components that are not chemically combined. All of these techniques involve changes in the physical state of a chemical compound rather than chemical changes. Sea sand‚ table salt‚ and two other unknown substances will be separated using the separation techniques in order to demonstrate
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Quantitative Separation of a Mixture Lab Pre-Lab Questions: 1. Define the following: Physical Change Heterogeneous Mixture Sublimation Filtrate Residue 2. List two physical separation methods. 3. List the formula for determining percent composition by mass. Objectives: 1. to separate a three component mixture and 2. determine the percent composition by mass of each component in the mixture. Materials: Ammonium chloride (NH4Cl)‚ Sodium chloride (NaCl also known as
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Separation and Identification of Organics from an Aqueous/Organic Environment through Physical Manipulation Date Lab Performed: Nov. 11/2013 Date Lab Submitted: Nov. 18/2013 Introduction We conducted this experiment to investigate the technique of liquid / liquid extraction‚ the miscibility of organics and water and the effect of a mixture of compounds in methylene chloride versus pure compounds retention time as introduced to a Gas
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Lab 6: Organic Compound Analysis Isabella O’Toole CHY 116 Friday 1:15-4:00 Lab Conducted on 4-12-13 and 4-19-13 4-26-13 This lab was conducted in order to determine the chemical composition of an unknown organic acid. A known mass of acid was dissolved into 30mL of either water or methanol (depending on solubility) and titrated with standardized sodium hydroxide. Data from this allowed the molar
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