Alvarenga Lab Partner: Keren Appiahene Mussie Gide 10 September 2016 Experiment 2: Acid- Base Extraction Separation of an Organic Acid‚ a Base and a Neutral Compound Introduction: The extraction technique is often used in the organic lab to separate organic compounds from mixtures. One type of an extraction technique is the acid-base extraction‚ which is used to separate organic compounds from a mixture based on their acid-base properties.1 There are certain principles that must be taken into account when
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Separation and Purification of Organic Compounds Codilla‚ Christine‚ Cristobal‚ Marian‚ Dionisio‚ Jermaine‚ Dumaquita‚ Vanessa‚ Edrosolo‚ Lyka‚ Esquivel‚ Christine1 1University of Centro Escolar‚ Makati Date Performed: December 5‚ 2012 Date Submitted: December 17‚ 2012 Abstract The distillation process was successfully done because of the separation of water from the acetone. When the distillate was lighted with the matchstick it produced flame which indicates that there was more presence
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2014 Experiment No. 7 Unknown: 2 Compound: Table 6.1Physical Examination State Liquid Odor Smells like adhesive paste Color Pink-orange Flammability Flammable Table 6.2Physical Constant: Melting Point Parameter Experimental Theoretical (From Literature) Melting Point (oC) Trial 1 Trial 2 Average 88 88 86 86 Table 6.3Solubility Test Sample Solubility Solubility Class Water Ether 5% NaOH5% Na2CO3 5% HClConc. H2SO4 Unknown Sample + + + + + + Basic Compound Table 6.4Qualitative Tests
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Craig Delancy Separation of a Mixture Containing Calcium Carbonate and Naphthalene Objective: Finding a method to successfully separate a mixture of calcium carbonate and naphthalene. Properties to be considered: Calcium Carbonate Naphthalene Solubility in water slightly insoluble Solubility in ethanol insoluble partially Melting point 825 degrees C 80.2 degrees C Boiling point decomposes 218 degrees C Procedure: Subliming the mixture seemed to be the most
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Separation of the Components of a Mixture Purpose: To become familiar with the methods of separating substances from one another using decantation‚ extraction‚ and sublimation techniques. Apparatis and Chemicals: balance‚ Bunsen burner‚ rubber hose‚ tongs‚ 2 evaporating dishes‚ 2 watch glasses‚ 100-mL graduated cylinder‚ clay triangles‚ 2 ring stands‚ 2 iron rings‚ 2 glass stirring rods‚ unknown mixture of NaCl‚ NH4Cl‚ SiO2. Discussion: Mixtures are composed of two or more substances
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Analysis of an Unknown Mixture Performed: 2/13/14 Submitted: 3/3/14 Abstract: The purpose of this experiment was to separate and identify the two unknown compounds. The sample used was 105 and it contain 2-propanol and 2-heptanone. IR spectrums were taken of the contents of the second and sixth test tubes and showed the presence of an OH functional group and a small amount of ketone in test tube two and a large presence of ketone in test tube six. The average boiling points of the test tubes
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Separating Acids and Neutral Compounds by Solvent Extraction Introduction The purpose of this experiment was to use solvent extraction techniques in order to separate a mixture consisting of a carboxylic acid (p-toulic acid)‚ a phenol (p-tert-butylphenol)‚ and a neutral compound (acetanilide). Extraction is the process of selectively dissolving one or more of the compounds of a mixture into an appropriate solvent‚ the solution that contains these dissolved compounds is called an extract (Manion
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Objective: The objective of this experiment is to use acid-base extraction techniques to separate a mixture of organic compounds based on acidity and/or basicity. After the three compounds are separated we will recover them into their salt forms and then purify them by recrystallization and identify them by their melting points. Procedure: Extraction of Carboxylic Acid A pre-weighed (0.315g) mixture of Carboxylic acid‚ a phenol‚ and neutral substance was placed into a reaction tube (tube 1).
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Samantha Smith Organic Chem 255 Lab M/W 12:30-4:30 Hyejin Cho 12 June 2013 Separation of a Mixture Abstract: In this experiment‚ the three processes of extraction‚ sublimation and recrystallization will be used to separate a mixture of salicylic acid and naphthalene. The first part of extraction will be to separate the salicylic acid from the naphthalene using diethyl ether and aqueous sodium bicarbonate. The naphthalene will reside in the ether and be the top layer‚ while the
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TITLE: SEPARATION AND PURIFICATION OF ORGANIC COMPOUNDS AIMS: To isolate organic‚ inorganic and component from a given sample. To become acquainted with various separation methods. To examine the solubility behavior of the various compounds in a mixture using different solvents. INTRODUCTION A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require
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