Introduction: The technique used in this experiment is recrystallization. Recrystallization is an often-used method for purifying solids. Recrystallization works by taking advantage of the different solubility properties of compounds‚ and allows impurities to be removed from crude solids. Performing a recrystallization is usually a straightforward task. First‚ you add a small amount of solvent to the impure compound in a flask‚ and heat the contents until all the material has dissolved. Then‚ you
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Recrystallization and Melting Point Determination W. H. Bunnelle‚ L. A. Meyer‚ R. E. Glaser (Version 3) Introduction Consider what happens when a solid material is placed in a solvent in which it has a low solubility. Not much! A small fraction of the solid will dissolve‚ but the rest will just sit there. (Actually‚ it doesn’t just ’sit there’ since an equilibrium is in effect‚ with solid molecules going into solution‚ and an equivalent number of dissolved molecules reforming solid‚ but we
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References: Buchanan‚ G.W. "Solubility Tests and Recrystallization." CHEM 2203/2204 Organic Chemistry Laboratory Manual. By C.A. White. N.p.: n.p.‚ n.d. 21-31. Print. "IR Spectrum." Research Gate. N.p.‚ n.d. Web. 08 Oct. 2014. Wagner‚ Kathryn. "Like Dissolves Like." LIKE DISSOLVES LIKE (n.d.): n. pag. Web.
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Lab 3: Bromination of Acetanilide CHEM 2110 Hassan Alsaleh 0525970 Due date :11/02/2015 Q1: To find the limiting reagent we need to find the number of moles of acetanilide‚ and the number of moles of Bromine. Mass of Acetanilide used = 0.67g Molar mass of Acetanilide = 135.16g/mol[1] Number of moles of Acetanilide = (0.67g) / (135.16g/mol) = 0‚005 mols Volume of Bromine = 0.25ml Density of Bromine = 3.103 g/ml[2] Mass of Bromine = (0.25ml) X (3.103g/ml) = 0.78g Molar mass of Bromine
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Mabel M. Kimble September 21‚ 2014 Chemistry 234 Recrystallization of Benzoic Acid ABSTRACT The recrystallization of Benzoic Acid was performed to fully master the ability to purify a solid compound. This form of purification technique is especially important in chemical identification‚ where the melting point of the compound is taken to confirm its purity. In order to perform recrystallization a solubility test much be completed. Four solvents (95% Ethanol‚ Petroleum Ether‚ Acetone and distilled
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Q: Which of the ff are branches of the aortic arch? A: Brachiocephalic‚ left common carotid‚ left subclavian Q: Which of the ff are branches of the subclavian arteries? A: thyrocervical‚ internal thoracic‚ and vertebral artery Q: Where is the carotid sinus located? A: Base of the internal carotid Q: Which of the ff are branches of the internal carotid? A: middle cerebral‚ anterior cerebral‚ ophthalmic artery Q: The gastroduodemal artery is a branch from which artery? A: Common hepatic artery
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molecular weight is 151.2 g/mol. The melting point of pure compound is in the range of 169-172 ℃. During lab Paracetamol medication was dissolved in water‚ purified and recrystallized again. The purpose of the experiment was to learn basic recrystallization techniques that include hot and cold filtration. During experimental procedure sample was purified and its final melting point was measured. Procedure 1.0 g of impure Paracetamol was added to the flask with 2 boiling chips. 30 mL of distilled
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Recrystallization of Benzoic acid Chemistry 204-002 Date: 4/9/2011 Hector Ortega Recrystallization is a method used to purify compounds‚ and this is a very important procedure because compounds are naturally impure. Polarity and solubility play a big role in this experiment and these characteristics are exploited in order to have a crystallization of the desired compound. In this experimented benzoic acid was crystallize using ethanol and water. I chose these solvents based on part C of the experiment
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Experiment 1: Recrystallization – Evaluation Summary Last Name: Xavier First Name: Jessica Date: October 1st 2013 Lab Day/TA/Group: Wednesday(1:35pm)/Group A Labs reports must be typed and chemical structures must be drawn with ChemDraw. Report must not exceed three pages (including this page). Page limit does not include any attached spectra or references. ** Deductions for hand written report/structures and exceeding page limit ** Report Breakdown Data/Results: _________________
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Recrystallization of Benzoic Acid Objective To purify benzoic acid by recrystallization and gain experience with a basic organic laboratory techniques. Background Products of chemical reactions are often contaminated with impurities. One method for purifying chemicals‚ recrystallization‚ takes advantage of the differences in the solubilities of the desired products and the impurities and the tendency for the slow formation of crystals to exclude impurities from the crystalline solid. HC HC
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