be formed. Equipment * 10 ml pentanol | * condenser | * 10 ml glacial acetic acid | * Heating Mantel | * 1 ml conc. Sulfuric acid | * Funnel | * 50 ml flask | * 15ml 1molL-1 Na2CO3 | * Boiling chips | * Seperating Funnel | * Retort Stand | * Safety Glasses | Method 1. 10 ml of Pentanol‚12ml of glacial acetic acid and 1ml of concentrated sulfuric acid were placed in a 50 ml flask. 2. Added afew boiling chips and assembled the refluxing apparatus
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EXPERIMENT A PREPARATION OF ASPIRIN Abstract This report gives a detailed account of the experimental preparation of aspirin in a laboratory environment as well as some basic industrial background on the product. It also contains information about safety precautions put in place to ensure the safety of the team who carried out the experiment. All results obtained have been included as well as a detailed analysis of what they represent alongside any improvements to the method used. Introduction
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Preparation and melting point of Aspirin Aspirin is a painkilling drug and is produced worldwide to reduce and stop pain. Aspirin is made up of ehtanoylation of 2-hydroxbenzenecarboxylic acid in a presence of phosphoric acid. AIM: The aim of the experiment is to prepare and produce aspirin as pure as possible. I will do this threw preparing the aspirin and purifying the product threw recrystallization. I will then obtain a melting point of my product to get an estimate of its purity. By the end
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Preparation of Bromotriphenylmethane Abstract The structure of a major component of star anise oil was derived by analyzing its IR spectroscopy melting point of after oxidation and purification. From the evidence obtained‚ it was concluded that the exact structured should be p-methoxybenzoic acid. Introduction The purpose of this experiment is to determine the structure of the major component of star anise oil. It is already known that this component has a molecular formula C10H12O. This
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OF PURE AND APPLIED CHEMISTRY Visayas State University Visca‚ Baybay City‚ Leyte Name: Alecsa May S. Celaya BS-Chemistry 3 Date Submitted: December 19‚ 2014 Lab. Schedule: MW 2:00 – 5:00 pm Rating: Group No. 11 Experiment No. 5 Preparation of KAl(SO4)2•12H2O (Alum) OBJECTIVES This experiment aimed to: prepare KAl(SO4)2•12H2O‚ commonly referred to as alum‚ from aluminum metal from a canned soft drink‚ and determine the mass of the alum collected and its percent yield. METHODOLOGY
Free Stoichiometry Chemical reaction Aluminium
Buffer Preparation (Gozani Lab) 1. 1 M Tris-HCl Buffers pH Volume (L) TrisBase (g) HCl (ml) pH 7.0 2 242.2 150-155 pH 7.5 2 242.2 120-125 pH 8.0 2 242.2 80-85 Autoclavable. 2. EDTA 0.5 M (pH8.0) 0.5M‚ 1L: 148 g EDTA + ~30-40 g NaOH to adjust pH (or 186 g EDTA-Na.2H2O + ~20 g NaOH) Note: pH adjusted by NaOH is essential for solubility. Autoclavable. 3. TAE DNA Electrophoresis Buffer (50 X) (2 M Tris‚ 50 mM EDTA) 2L 484 g Tris 114.2 ml glacial acetic acid 200 ml 0.5 M EDTA 8.0 To make
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American Type Culture Collection) is used for the production of Penicillin. Preparation of Different Salts of Phenyl acetic acid. Sodium phenyl acetate For 100 ml preparation‚ few grams of PAA (of known percentage) are dissolved in certain volume of De-Mineralized water. The pH of the solution is maintained between 6.6-7 by adding NaOH in drops. Molecular Weight-159. Potassium phenyl acetate For 100 ml preparation‚ few grams of PAA (of known percentage) are dissolved in certain volume of De-Mineralized
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20 – 03 – 13 EXPERIMENT: - PREPARATION OF POLYURETHANES AIM Synthesis of polyurethanes OBJECTIVES - Mixing a diisocyanate and a diol in polyurethane synthesis of two distinct products. - Comparing polyurethane from castor oil to that made from polyethylene glycol. - To establish the type of foams in terms rigidity or flexibility. THEORY Polyurethanes‚ also known as polycarbamates‚ belong to a larger class of compounds called polymers. Polymers are macromolecules made up
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L’Oreal : Strategies for the Indian Market Session 4: Preparation Questions 1. Evaluate L’Oreal’s entry strategy in the Indian market with respect to the product‚ promotion‚ pricing and place decisions? 2. What have been the changes in the marketing strategy of L’Oreal in the last 8 years? Evaluate them with respect to selection of product / market and each element of the marketing mix? 3. What factors helped the rapid adoption of Excellence colorants among its target customers?
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Learning Activity 1 Preparation of Acetanilide Abstract Recrystallization is a common method of purifying organic substances through the difference in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heating water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes from the solution‚ molecules of other compounds
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