Grignard reaction Abstract: In this laboratory‚ triphenylmethanol was synthesised from reacting benzophenone and bromobenzene using Grignard reaction. As the reaction was to set up to produce a Grignard reagent and then recrystallize it to obtain pure sample. The percentage yield obtained was 55% and its melting point was 161 co which is within the literature value 160-163 co. In addition to that the IR spectroscopy confirmed the molecule structure to be triphenylmethanol. Introduction: The Grignard
Premium Alcohol Ethanol Functional group
Substance | Structure | M.W. g/mol | Density g/cm^3 | MP (C) | Hazards | Naphthalene | | 128.17 | 1.14 | 80.26 | White crystalline solid‚ with odor | benzophenone | | 182.217 | 1.11 | 47.9 | Barely hazardous‚ don’t get in contact with eyes or skin | Methanol | | 32.04 | 0.79 | -98 | Extremely flammable | Petroleum ether | | 86.18 | 0.77 | -95 | Extremely Flammable | Procedure: 1. 2. Add 80mg of naphthalene to Craig tube. Add few drops of methanol hot solvent. 3. Place tube
Premium Oxygen Ethanol Chemistry
Lab Section GTA Station 1. Grignard Reaction Post-lab report Fill out the appropriate sections below. Show all work. Your calculated answers need to match the answers in the table. Also‚ attach the benzophenone and product spectra. Indicate appropriate stretches including differences in both spectra. Results | | Amounts and units | |Initial volume
Premium Infrared Nucleophile
was added to the round bottom flask drop-wise with additional washing of ~2.0 mL of diethyl ether. Iodine (catalyst) was added to facilitate the reaction. Phenylmagnesium bromide was obtained upon cooling of the solution to room temperature. Benzophenone (1.09 g) and diethyl ether (2.0 mL) mixture was then reacted with the Grignard product for 15 minutes. Red solidified adduct was observed. Next HCl (6.0 mL) was added drop-wise to the adduct; bilayer of triphenylmethanol and inorganic impurities
Premium Magnesium Diethyl ether Oxygen
Extraction and analysis of two compounds from unknown solution C ABSTRACT Liquid C and solid C were both extracted from unknown solution by first using chemically active liquid-liquid extract‚ followed by vacuum filtration. Liquid C and solid C were then purified with the use of simple distillation and recrystallization respectively. Through the process of recrystallization‚ the percentage purity of solid C was found to be 6.01%. The melting point range of purified solid C was 117.0 – 119
Premium Solvent Liquid Solubility
E5 & E6 Extraction of Chlorophyll from Fresh Spinach and Investigation of the Photochemistry of Chlorophyll Chlorophyll a Chlorophyll b E5 - Extraction of Chlorophyll from Fresh Spinach E6 - Investigation of the Photochemistry of Chlorophyll The aim of this experiment is to investigate the photochemistry of chlorophyll. This experiment will be performed in two lab periods. In the first lab period you will extract chlorophyll‚ the green pigment in leaves‚ from spinach.
Premium Chlorophyll Photosynthesis Chromatography
brown and cloudy. The conical vial was then rinsed with 2 ml of anhydrous ether to get any remaining solution into the reaction vessel. Simultaneously‚ 1.09 g of benzophenone and 2ml of anhydrous ether were added to a 3ml conical vial and gently stirred. The reaction vessel was taken off of the hot plate and allowed to cool. The benzophenone was then added to the reaction mixture while stirring vigorously. The conical vial was washed with anhydrous ether and transferred to the mixture. The reaction
Premium Chemistry Water Solvent
Lab II March 19‚ 2012 Abstract The purpose of this experiment was to synthesize the Grignard reagent‚ phenyl magnesium bromide‚ and then use the manufactured Grignard reagent to synthesize the alcohol‚ triphenylmethanol‚ by reacting with benzophenone and protonation by H3O+. The triphenylmethanol was purified by recrystallization. The melting point‚ Infrared Spectroscopy‚ 13C NMR‚ and 1H NMR were used to characterize and confirm the recrystallized substance was triphenylmethanol. Introduction
Premium Magnesium Oxygen Solvent
long-sighted‚ astigmatism‚ to name but a few. Researchers indicate that television emits blue light that also produced by the sun. The wavelength of light produced is 400-500 nm‚ potentially triggering the formation of free radical and injuring the photochemistry in the retina of children eyes. Finally‚ TV is the reason for having difficulty distinguishing between what is real and what is not. It is a common observation that children have imitation of acting as characters on TV show. Take “ chuyen la
Premium Television Eye Television program
TextBooks Sr No T-1 T-2 Title Engineering Chemistry Chemistry Reference Books Sr No R-1 Other Reading Sr No OR-1 OR-2 OR-3 OR-4 OR-5 OR-6 OR-7 Journals articles as Compulsary reading (specific articles‚ complete reference) http://onlinelibrary.wiley.com/journal/10.1002/(ISSN)1097-4601 ‚ http://www.springer.com/chemistry/electrochemistry/journal/10800 ‚ http://www.sciencedirect.com/science/journal/13882481 ‚ http://www.springerlink.com/content/100224/ ‚ http://www.sciencedirect.com/science/journal/00108545
Free Chemical bond Covalent bond Ionic bond