Bleach Oxidation of 9-Hydroxyfluorene The purpose of this experiment was to oxidize an alcohol (9-hydroxyfluorene) to a ketone (9-fluorenone) using aqueous sodium hypochlorite (bleach) as the oxidizing agent‚ while introducing techniques used in microscale experiments. Reaction: Results 1. Recrystallized Product Yield Product yield = (actual yield/theoretical yield) x 100% 3mL 9-hydroxyfluorene x (1mL/1000mL) x (0.09 mol/L) = 2.7 x 10-4 moles 0.05g 9-fluorenone / (180.20g/mol) = 2.77 x 10-4
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YOUR NAME: Erin Alston‚ Kennedy Stuart‚ Amber Lamb and Stephonya Williams EXPERIMENT TITLE: Oxidation: Cyclohexanone from Cyclohexanol by Hypochlorite Oxidation and Adipic Acid from Cyclohexanone DATE: 4/18/2014 INTRODUCTION: In experiment 4‚ alcohol is oxidized to a ketone with household bleach. The product is then isolated by steam distillation and is extracted into the distillate with ether. After the removal of ether‚ it leaves the product cyclohexanone. In experiment 6‚ cyclohexanone is
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of that substance by titrating the sample with a solution of a strong oxidizing agent. In this lab‚ a solution of KMnO4‚ an oxidizing agent‚ will be standardized by titration with a solution containing a known concentration of iron (II) ions‚ (Fe+). The concentration of oxalic acid solution will be determined by titration with the MnO4- solution that had been standardized first. The purpose of this lab is to standardize a solution of potassium permanganate by redox titration with a standard solution
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To prepare a temporary mount of aleaf peel to show stomata. B) Materials required:- Fresh leaves of plant‚ compound microscope‚ glass slides‚ cover slips‚ water‚ glycerine‚ safranine‚ blotting paper‚ needles‚ brush etc. C) Theory :- i) Stomata are minutepore present on the surface of the leaves. ii) Though they are found on both the upper and lower epidermis of the leaf‚ they are more in number on the lower epidermis. iii) Each stoma has two bean shaped
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Module 16 Notes Reduction/Oxidation Reactions • Oxidation number: The charge that an atom in a molecule would develop if the most electronegative atoms in the molecule took the shared electrons from the less electronegative atoms. • Oxidation numbers are not real; they are only based on assumptions. They are useful bookkeeping tools though‚ and can help us keep track of electrons during a reaction. • The sum of all oxidation numbers in a molecule must equal the charge of that molecule. • Rules
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1. Mechanism of oxidation process In an oxidation process of silicon that usually takes place at very high temperature (thermal oxidation)‚ silicon (Si) reacts with either water vapor (H20) or oxygen (O2) to form silicon dioxide‚SiO2 on the silicon surface. The reaction is represented by following equations: Dry oxidation: Si + O2 → SiO2 Wet oxidation: Si + 2H2O → SiO2 + 2H2 The oxidation process can be implemented through diffusion
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OIXDATION(AND(REDUCTION(–(REDOX(CHEM(1( ( KEY(REDOX(CONCEPTS( •! Oxidation)and)reduction)are)electron(transfer(processes)(reactions).)) o! Oxidation(–(Loss)of)electrons)) !! Reductant((reducing)agent))–)undergoes)oxidation.)) o! Reduction(–(Gain)of)electrons)) !! Oxidant((oxidising)agent))–)undergoes)reduction.)) ! Example:(((((((((((Mg(s)(+(2H+(aq)( (Mg2+(aq)(+(H2(g)( o! This!reaction!can!be!broken!up!into!two!halfEreactions(( !! Oxidation:)Mg(s))")Mg2+)+)2e:)(lost)electrons))( !! Reduction:)2H+)+)2e:)")H2)(gained)electrons))(
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OXIDATION AND REDUCTION Oxygen makes up only about 20% of the air‚ yet is the essential component for so many reactions. Without it fuels would not burn‚ iron would not rust and we would be unable to obtain energy from our food molecules through respiration. Indeed animal life on the planet did not evolve until a certain concentration of oxygen had built up in the atmosphere over 600 million years ago. The term oxidation has been in use for a long time to describe these and other reactions where
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Oxidation of Cyclohexanol Introduction: The oxidation of cyclohexanol involves using household bleach to oxidize this secondary alcohol and produce a ketone product‚ cyclohexanone. Oxidation-reduction (redox) reactions occur when the oxidation state of atoms change due to a transfer of electrons. Oxidation occurs when electrons are ‘lost’ to the formation of bonds and reduction occurs when electrons are ‘gained’ in the braking of bonds (Levine). Using this reaction and its product‚ a redox experiment
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Making an Activity Series of Metals using different Solutions Purpose/ Hypothesis: The purpose of this lab was to clearly identify the reactivity of magnesium‚ zinc and copper. The metals reactivity will be exemplified as it will be tested with different solutions such as zinc sulfate (ZnSO4)‚ copper sulfate (CuSO4)‚ hydrochloric acid (HCL)‚ magnesium sulfate (Mg2SO4)‚ iron (II) sulfate (FeSO4) and tin (II) chloride (SnCl2). This will allow us in creating an activity series to visually see the reactivity
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