The Synthesis of Organic Aspirin ABSTRACT: The purpose of this experiment was to find out how a reaction undergoes for a globally known painkiller called aspirin‚ and to become familiar with achieving successful yields. Aspirin is synthesized from salicylic acid and acetic anhydride. Those two chemicals are mixed together along with sulfuric acid to form a crude solid. Filtration is used separate the impurities from the crude aspirin. To get purified aspirin‚ the precipitate was heated until all
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impurities have on the melting point of an organic compound? Soluble impurities affect the melting point of a solid in the following manner. a. The presence of an impurity in the molten compound reduces its vapor pressure thus lowering the melting point of the compound. b. Broaden the melting point range. 2. For what tow purpose are melting points routinely used a. To determine the identity of an organic solid. b. To determine the purity of an organic solid. 3. What effects on the measured melting
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nCH3 The first step in the lab is the preparation of the solvent used in the developing chamber for thin layer chromatography. The solvent used is a 3:1 mixture of toluene and petroleum. After the developing chamber is prepared‚ it is essential to begin preparation of the unknown DNPH derivative[6]. The preparation of the 1‚2 DNPH derivative of a ketone is in fact a small organic synthesis which produces a fraction of a gram of product. The second part of the lab makes use of NMR Spectrometry
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JOMO KENYATTA UNIVERSITY OF AGRICULTURE AND TECHNOLOGY DEPT: CIVIL ENGINEERING UNIT: CHEMISTRY 1 (SCH 2109) PRACTICAL REPORT EXPT 2: Standardization and Determination of Concentration of Hydrochloric Acid in a Given Solution by ARAKA BRAMWEL MBOGO EN251-0221/2010 TITLE: STANDARDIZATION and DETERMINATION OF THE CONCENTRATION OF HYDROCHLORIC ACID PRESENT IN A GIVEN SOLUTION Aims: To be able to standardize Sodium Hydroxide (NaOH) solution using a standard solution of Oxalic acid
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DENISTY LAB 2/25/13 Chemistry H. Mrs. Halme Objective: Your task is to determine the density of 3 known metals: Zinc‚ Copper‚ and Lead. They are each marked. You must then calculate the density of an unknown metal and determine its identity based on your data from your known samples. Reagents: None Equipment: Lead Copper Zinc Triple Beam Balance Graduated cylinder Unknown metal (Magnesium) Beaker Calculator Procedures Preparation: We observed the given equipment
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THE CHEMISTRY OF ORGANIC MOLECULES I. MACROMOLECULES-large molecules that are composed of smaller molecules and atoms that are bonded together. These are among the largest of all chemical molecules. A. Polymers-the largest of the macromolecules. These are composed of numerous‚ small identical subunits known as Monomers. There are 4 major polymers that are important for living organisms. These polymers are; carbohydrates‚ lipids‚ proteins and nucleic acids. B. Polymers
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|Chapter 5: | |Structure and Preparation of Alkenes. | |Elimination Reactions | Summary Alkenes contain the C=C functional group which can be prepared by 1‚2-elimination reactions such as: • dehydration of alcohols (- H2O) or • dehydrohalogenation of alkyl halides (- HX). Zaitsev’s rule indicates that the preferred product is the more highly substituted
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Experiment 12: Calorimetry and Hess’s Law Purpose: The purpose of this lab is to determine the enthalpy of reaction for the burning of one mole of magnesium in oxygen. Although the reaction is exothermic‚ the ∆HRXN will be determined by using calorimetry and then using Hess’s Law to manipulate the data collected to yield the answer needed. Procedures: Dillon‚ Stephanie. “ Calorimetry and Hess’s Law.” Laboratory Manual. Pearson Publishing‚ 2012‚ pp.168-177. Data and Results Part A
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UNIT 1: INTRODUCTION TO ORGANIC CHEMISTRY Objectives: At the end of this unit‚ the students should be able to: 1. Learn the Types of Structures a. Sawhorse Structures b. Newman Projections 2. Learn to draw the different Isomers a. Sawhorse Structures b. Newman Projections Types of Structures 1. Two-dimensional structural formula 4. Three-dimensional structural formula 2. Condensed structural formula 5. Sawhorse structures 3. Bond-line structural formula
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Title: Calculating the Atomic Mass of “Pennium” Purpose: The purpose of this lab is to calculate the atomic mass of “pennium” using pennies made before 1982 and pennies made 1982 or after. Hypothesis: The atomic mass of the pennium will be the average of the average masses of a pre-1982 penny and a post 1982 penny. Procedure: 1. Obtain a bag of pennies 2. Determine the total number of pennies in the bag. Record the value. 3. Sort the pennies by date into 2 piles. One pile should consist
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