ether. To isolate the alcohol‚ dilute acid was used to convert the magnesium salt to free alcohol and the mixture was washed with water and sodium chloride to remove remaining magnesium salt and water. Anhydrous sodium sulfate was used to dry the organic layer and all solvent was removed through rotary evaporation. To purify the product‚ the crude product was washed with hexane and recrystallized from hot 2-propanol. 1) 2) 3) Figure 4. Reaction mechanism for the preparation of Grignard reagent
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References: Grossie‚ D. & Underwood K. (2011).Laboratory Guide for Chemistry. “Atomic Spectrometry”‚ Wright State University. Dayton‚ OH.
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Lab Report Quiz!!! | | | LabRepQuiz010 Question MC #19: All are true of the Materials and Methods section except___.Answer | | | | | | | | | | * Question 2 1 out of 1 points | | | LabRepQuiz010 Question MC #7: Which of the following is the best written sentence that includes the information below taken from an article written by Dr. Costanza‚ but avoids plagiarism? -A decade of research from Sunshine Health Clinic has shown that 20 minutes of exercise a day can
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Grignard Synthesis of Tirphenylmethanol David Szuminsky Organic Chemistry Lab II Shaopeng Zhang Monday 1PM 2/10/14 & 2/24/14 - Abstract A sample of triphenylmethanol was prepared using Grignard synthesis techniques. Reflux was used in order to speed up the reaction and the final product was purified using recrystallization methods. The percent recovery and percent yield were 80.46% and 47.526%‚ respectively. A melting point range of 85-87oC was obtained from
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Research & Design in Psychology / G Faculty of Health‚ University of Canberra LAB REPORT COVER SHEET Instructions: 1. Complete these details and the declarations electronically. 2. Insert this sheet at the start of your lab report. 3. Submit the entire assignment‚ including this coversheet‚ as one file via the lab report drop-box on Moodle. 4. For more information‚ see Lab report guidelines. |STUDENT NAME:
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Chemistry 2283g Experiment 1 – Alkyl Halides EXPERIMENT 1: Preparation and Reactivity of Alkyl Halides Relevant Sections in the text (Wade‚ 7 ed.) • 6.7 (p. 228) Reactions of alkyl halides • 6.8 – 6.12 (p. 229 – 242) The SN2 reaction: generality‚ factors affecting SN2 reactions‚ substrate reactivity‚ mechanism • 6.13 – 6.14 (p. 243 – 249) The SN1 reaction: mechanism‚ stereochemistry General Concepts The most common of the variety of methods available for preparing alkyl halides is the replacement
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encoded by EZH2‚ the EZH2 gene encodes part of the Polycomb group which make protein complexes that help to maintain genes transcriptional repressive state over successive cell generations. http://www.ncbi.nlm.nih.gov/gene/2146 Throughout this lab report template DNA that contains the gene EZH2 was provided‚ this will be amplified by a PCR and cloned into a vector. This Polycomb group proteins help maintain the cell identity during progress through chromatin
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Melting Points Elizabeth McGrail Organic Chemistry I 25 January 2013 ABSTRACT The objectives of this lab are‚ as follows; to understand what occurs at the molecular level when a substance melts; to understand the primary purpose of melting point data; to demonstrate the technique for obtaining the melting point of an organic substance; and to explain the effect of impurities on the melting point of a substance. Through the experimentation of three substances‚ tetracosane‚ 1-tetradecanol and
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Organic Lab Trial 1 Trial 2 Trial 3 Observations We added the 30ml of warm water with 4.7 grams of borax powder in to the cup labeled ‘Borax Solution’ and also added a few dots of green food coloring. We then stirred it until all the solutions were completely mixed. When this happened the borax and water turned into a watery green solution. then we added 15ml of glue in the cup labeled ‘Ball mixture’ and added the mixture we made
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marginal difference between the amounts of CO2 produced at different temperatures. The results showed that increased temperature causes an increase in fermentation rate and increased production of CO2. Introduction: Fermentation is the break down of organic matter‚ by microorganism‚ in the absence of oxygen also known as anaerobic (Van Neil‚ 2008). Our reactions occurs when yeasts is added to a solution of glucose and water. Fermentation starts with a process called glycolysis. In glycolysis Glucose
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