Epoxidation Reactions Lab Report 2 Abstract An oxygen atom is transferred from a peroxy acid to the carbon=carbon double bond thus forming an epoxide. Scheme 1. Oxone Epoxidation. Scheme 2. mCPBA Epoxidation. The percent yield for the Oxone epoxidation reaction was 65% yield and the mCPBA epoxidation reaction was 70% yield. Oxone is the greener alternative because using mCPBA is twice as expensive as Oxone and leaves behind the epoxide plus m-chlorobenzoic acid while Oxone creates non-toxic
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Patel Chem 101 10-13-09 Introduction The objective of this lab was to show how stoichiometry is applied to a specific chemical reaction. Stoichiometry is pretty much the math behind chemistry. Doing stoichiometry can calculate masses‚ moles‚ and percents with a chemical equation. The use of stoichiometry is how we were able to find the limiting reagent in this lab. A limiting reagent is the chemical that will be used up first. Many calculations had to be made throughout this lab. Some
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Object Length (cm) Length (mm) Length (M) CD 12cm 120mm .12M Key 5.3cm 53mm .053M Spoon 15.5cm 155mm .155M Fork 19.8cm 198mm .198M Water Temperature C° Temperature F° Temperature K Hot from tap 38 C° 100.4 F° 311K Boiling 93 C° 199.4 F° 366K Boiling 5 minutes 95 C° 203.0 F° 368K Cold from tap 15 C° 59 F° 288K Ice water 1 minute 8 C° 46.4 F° 281K Ice water 5 minutes 5 C° 41.0 F° 278K Object Estimated mass (g) Actual mass (g) Actual mass (Kg) Mechanical pencil 4g 5
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References 1.) Lehman‚ John. Operational Organic Chemistry‚ 3rd Edition. Experiment 4 (pp. 38-45; 680-687; 644-650)‚ Prentice-Hall‚ 1999. 2.) Laboratory Reference Manual: Experiment 3. Retrieved from: http://academic.reed.edu/chemistry/alan/201_202/lab_manual/expt_salicylic_acid/background.html 3.) Lab 5: Synthesis of Salicylic Acid. Retrieved from: http://academic.evergreen.edu/curricular/whatscookin/Lab%20five%20%20methyl%20saliclate.htm 4.) Handout: Synthesis of Salicylic Acid. Retrieved
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of the major findings in The Organic Trade Association’s 2010 Organic Industry Survey. The complete report is available for purchase by going online (http://www.ota.com/bookstore/14.html) or by contacting ssexton@ota.com. U.S. Organic Industry Overview Despite the economic recession that gripped the United States in 2009‚ the organic market continued to experience growth. In 2009‚ total U.S. organic consumer product sales grew 5.3% to reach $26.6 billion. Organic sales growth continued to outpace
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sciencebyjones.com/safety_rules.htm Thanks to the Flinn Scientific Safety Rules for much of the below. General Guidelines 1. Conduct yourself in a responsible manner at all times in the laboratory. 2. Be familiar with your lab assignment before you come to lab. Follow all written and verbal instructions carefully. If you do not understand a direction or part of a procedure‚ ask the teacher before proceeding. 3. Never work alone. No student may work in the laboratory without an instructor
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Chem 105 Guide to the Formal Laboratory Report The purpose of a formal report is to communicate effectively to another person the goal‚ procedure‚ data analysis method‚ and results of your laboratory work. The report is divided into several well-defined sections. Each section must be present in a complete report. To earn an outcome point for the laboratory report‚ a student must submit a formal lab report that earns a score of at least 90/100. Each error (factual‚ grammatical‚ typographical
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Investigating the Determining Characteristics of Cations and Anions Chem 111 Sec 560 Introduction: The purpose of this lab was to study the specific characteristics of cations and anions‚ and ultimately to be able to identify an unknown substance based on our studies and tests using the logic trees developed through the experiment. A logic tree is a graphical display of the findings from this lab which‚ through a series of yes/no questions‚ elimination tests
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Pre-Laboratory Assignment 1. What are the hazards associated with sodium hydroxide (NaOH) solution? Sodium hydroxide solutions‚ especially in high concentrations‚ are toxic and corrosive. 2. (a) What buret reading should you record when the liquid level is as shown in Figure 2? In Figure 2‚ the lower meniscus lies below the 3 mL line and 4 minor gradations that signify 0.1 values. Estimating the uncertain digit to be 0.04 mL‚ the reading we record for this particular buret is 3.44 mL.
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Gabriel Alizaidy Liquid Chromatography September 14‚ 2009 Objective: To separate the components of unsweetened‚ grape flavored Kool-Aid. Procedure: Using two syringes‚ inject different concentrations of alcohol to extract red and blue dyes‚ and artificial flavoring. Data: Conclusion: Different dyes are shown when separated by different concentrations of isopropyl alcohol. Discussion of Theory: Chromatography‚ resolution and selectivity played major roles in making the experiment work
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