Organic Chemistry II Laboratory (ABCT357) Although studying fundamental theories of chemistry in the class is important to understand the concept of chemistry‚ carrying out experiments to corroborate the theories is also important. It is very important for students to get used to experiments in order to speed up their experiments. Expt.1. Acetylation of α-D-glucopyranose Add slowly 2.5 g (0.014 mol) of powdered D-glucose in small portions (roughly in 7-10 portions and 5 min for each addition)
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Thiamine-Catalyzed Benzoin Condensation I.Conclusion Benzoin was produced by reacting 2 mols of benzaldehyde with the catalyst thiamine to form a new C-C bond. A total of 2.626 grams were recovered. There was a 33% recovery of benzoin. The low percent recovery could be due to the purity of the limiting reactant‚ benzaldehyde. Upon filtration‚ the mother liquid appeared oily making it more likely that the low recovery was due to the solution ‘oiling out.’ This could be avoided in the future
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L09 Tree Balancing CX1007 Data Structures 2013/14 S2 Mark Yong Today • Importance of balance for BSTs • Balancing operaGons in self-‐balancing BSTs • Pseudocode + worked examples CX1007 Data Structures 2013/14 S2 2 Recall: Why use BSTs? • BSTs are a special form of BT L • At every
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Organic Chemistry II Laboratory (ABCT357/ABCT3757) Lab Manual 2014-2015 Lee Hang Wai‚ Alston (alston.lee@polyu.edu.hk) Dr. Lee Cheng Hao‚ Samuel (chenghao.lee@polyu.edu.hk) Organic Chemistry II Laboratory (ABCT357‚ ABCT3757) (Group one) Contact: Alston Lee (alston.lee@polyu.edu.hk) Tuesday 8:30-11:30 ‚ Laboratory: Y1315 Lab supporting staffs: YK Au / Kan Chan/Arnold Demonstrators: Dr. Samuel Lee‚ Alston Lee‚ Fu Wai Chung‚ Guo Shuai‚ Yuen On Ying‚ Sep 16 Tue Acetylation of α-D-glucopyranose (Expt
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The goal of this experiment was to synthesize dibenzalacetone by aldol synthesis. The name ’Aldol synthesis’ was taken from the words ’aldehyde and alcohol’. This is because the product of this reaction contains both an aldehyde and alcohol. The carbon-carbon bond-forming reaction is referred to as aldol addition. An aldol condensation yields many species of products if the reactant is more than one. Therefore‚ the aldehyde has to react with itself to yield one product. Procedure: Followed according
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SYNTHESIS AND CHARACTERIZATION OF HIGHLY CROSSLINKED HYALURONAN HYDROGELS Newell R. Washburn1‚ Sidi A. Bencherif1‚ Abiraman Srinivasan2‚ Jeffrey O. Hollinger2‚ Ferenc Horkay3‚ Krzysztof Matyjaszewski1 Departments of 1Chemistry and 2Biomedical Engineering Carnegie Mellon University‚ Pittsburgh‚ PA 15213 3 Laboratory of Integrative and Medical Biophysics National Institutes of Health‚ NICHD 13 South Drive‚ Bethesda‚ MD 20892 Introduction Methacrylation of hyaluronic acid (HA) with glycidyl methacrylate
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Post-Lab Report for Experiment 2: Cooperative Identification of an organic Solid October 6‚ 2013 Introduction: This experiment was focused on the cooperative identification of organic compound by its chemical properties such as: slow melting point‚ mixed melting point‚ Rf values in TLC experiment‚ IR spectrum analysis‚ and H NMR spectra. Such data can provide the the identity of functional groups and the identity of the compound itself. In this experiment
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Study Guide: Exam 1 1. How many different kinds of protons are present in each of the following compounds? A. a: 4; b: 4; c: 4 B. a: 4; b: 4; c: 5 C. a: 3; b: 3; c: 5 D. a: 3; b: 4; c: 5 E. a: 4; b: 3; c: 5 2. Which of the labeled hydrogens absorbs furthest upfield in the NMR? A. Ha B. Hb C. Hc D. Hd E. He 3. Which of the following compounds does not give a singlet in its NMR spectrum? A. A B. B C. C 4. Which of the circled protons in the molecules below would absorb furthest
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enables hospitals to move ahead and provide valuable services to customers (Sandrich‚ 2008). This facility serves veterans and the capital project proposal is for a Magnetic Resonance Imaging (MRI) compatible monitor and a program for sedation services for patients. Nursing support is necessary for monitoring patients during magnetic imaging for patients receiving oral and intravenous conscious sedation or pain management. In some cases anesthesia support may be necessary and a physician or radiologist
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A MIM/Coaxial Stub-Line CRLH Zeroth-Order Series-Mode Resonator used as an RF Coil Element for 7-Tesla Magnetic Resonance Imaging Andreas Rennings1 ‚ Jan Taro Svejda1 ‚ Simon Otto2 ‚ Klaus Solbach2 ‚ and Daniel Erni1 General and Theoretical Electrical Engineering (ATE)‚ 2 High Frequency Engineering (HFT)‚ Faculty of Engineering‚ University of Duisburg-Essen‚ and 1 CENIDE – Center for Nanointegration Duisburg Essen‚ D-47048 Duisburg‚ Germany 1 Abstract—A novel MIM/coaxial-stub composite right/lefthanded
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