Synthesis‚ Recrystallization of β-D-Glucose Pentaacetate from its Original D-Glucose and it comparison with literature though Melting point‚ TLC‚ IR‚ 1H and 13C NMR Abstract: The synthesis of the product: β-D-glucose pentaacetate is done though the acetylation using acetic anhydride with D-glucose with the help of sodium acetate. The recrystallization of the product is done though a polar solvent like water. The Result of this experiment has a percentage yield of 61% and analytical methods
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Qualitative Analysis Lab Report Organic Chemistry Laboratory II ABSTRACT: The purpose of this lab was to separate and purify two unknown compounds‚ one solid and one liquid‚ from an ethereal solution using the techniques of chemically active extraction‚ vacuum filtration‚ simple distillation‚ and recrystallization. Then identifying information was compiled about these unknowns by obtaining experimental melting/boiling point ranges‚ and analyzing IR and proton/carbon NMR spectrums It was determined
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Title: Competing Nucleophiles (Exp 24‚ pp 211-221‚ pp 808-823‚ pp 836-842) Purpose: The purpose of this experiment is to determine the nucleophilic strength of chloride and bromide ions as it reacts with 1-butanol (n-butyl) and 2-methyl-2-propanol (t-butyl alcohol) under SN1 and SN2 conditions. Method: 40 g of ice and approximately 30 ml of sulfuric acid is cautiously added to a 100 mL beaker respectively. Weigh 7.6 g of ammonium chloride and 14.0 g of ammonium bromide and place it in
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Abstract:The Wittig Reaction is a nucleophilic addition in which an alkene is formed as a product. Both the E and Z isomers of the alkene result. Substituents on the aromatic aldehyde affect the E/Z ratio of products that form. In this experiment‚ a nitro group was used as the substituent in the ortho‚ meta and para positions‚ with benzaldehyde as the control. Each of the four aldehydes reacted with (carbethoxymethylene) triphenylphosphorane to produce ethyl cinnamate‚ ethyl-3-(2-nitrophenyl)acrylate
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Experiment 1: Mechanism of Nitrile Oxide and Alkene Cycloaddition 1. Purpose: to clarify the mechanism for the cycloaddition reaction between benzonitrile oxide and an alkene‚ and to test the regiochemistry of the reaction between benzonitrile oxide and styrene. 2. Plan: Each student in a group of three will work to create a reaction with the Benzonitrile Oxide with‚ cis-stilbene‚ trans-stilbene‚ or styrene in an Erlenmyer flask. With this Reaction solution thin layer chromatography will be
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Experiment B10- Photocromism and Piezochromism Reece Harms 4320288 Introduction This experiment investigates an oxidative coupling reaction in an to synthesise triphenylimidazole dimer from 2‚4‚5-triphenyl-1H-imidazole. The resulting compound was investigated for both photochromic and piezochromic properties by way of formation of a stable radical‚ utilizing visual observations and UV-Vis as a means of distinction. Both the oxidative coupling reaction and the dimers interaction with light
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C│H│M│C│4│1 Letters 2013‚ Volume 1‚ Issue 1 A Perkin Reaction: Synthesis of (E)- and (Z)-Phenylcinnamic acids Thusanth Jogarajah‚ Dr. Lana Mikhaylichenko * Department of Physical and Environmental Sciences‚ University of Toronto Scarborough‚ 1265 Military Trial‚ Scarborough‚ ON‚ M1C 1A4 Received: February 6‚ 2013; E-mail Thusanth.Jogarajah@mail.utoronto.ca Abstract – Add text here Introduction: The name of this reaction is called the Perkin’s reaction. The reaction was
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S OUTHEAST ASIAN J T ROP MED P UBLIC H EALTH ANTI-HEAD LICE EFFECT OF ANNONA SQUAMOSA SEEDS Junya Intaranongpai 1‚ Warinthorn Chavasiri 2 and Wandee Gritsanapan 1 1 Department of Pharmacognosy‚ Faculty of Pharmacy‚ Mahidol University‚ Bangkok; Department of Chemistry‚ Faculty of Science‚ Chulalongkorn University‚ Bangkok‚ Thailand 2 Abstract. The present study focused on the separation and identification of the active compounds against head lice from the hexane extract of Annona squamosa
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Abstract Chemically active extraction was used to separate two unknown compounds from each other and to determine what compound class each compound belongs. The solid unknown was purified by recrystallization and its melting point range was determined to be 109-111°C. The liquid unknown was purified by simple distillation and its boiling point was determined to be 95°C. An IR spectrum was collected for each of the purified compounds; the solid was determined to be 3-toluic acid and the liquid was
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University of Pittsburgh for free where he later received his PhD degree in 1962. During his studies‚ he learned about nuclear magnetic resonance (NMR). Then he was drafted into the Army from 1954-1955 then left to work at the State University of New York at Stony Brook. He realized new images could be made from NMR. Lauterbur’s breakthrough idea was to vary the strength of the magnetic field over the object which in turn emitted various radio waves that could be turned into images . Then he turned to
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