Department of Psychology‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Four organic samples: hexane‚ cyclohexene‚ napthalene and toulene were given to serve as reference standards to characterize and distinguish four unknown given samples. Nitration‚ bromine and basic oxidation testswere conducted to classify the different samples from being an aliphatic‚ or aromatic‚ saturated or unsaturated and alkylated or non-alkylated hydrocarbons. The physical state and color were noted by simple physical
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Abstract: The purpose of this lab is to prepare phenylmagnesium bromide‚ a Grignard reagent‚ and react it with benzophenone to give triphenylmethanol. Once made‚ the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone‚ benzophenone. The result is an alkoxide that is then protonated to give the alcohol‚ triphenylmethanol. The purity of the final product will then be considered by melting point and IR spectroscopy. Final purified triphenylmethanol weighed 8.02 grams
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Abstract This experiment is about the synthesis of 3-nitrobenzaldehyde through nitration. The nitration of benzaldehyde is an example of an electrophilic aromatic substitution reaction‚ in which a proton of an aromatic ring is replaced by a nitro group. Many aromatic substitution reactions are known to occur when an aromatic substrate is allowed to react with a suitable electrophilic reagent‚ and many other groups besides nitro may be introduced into the ring. Although the reaction produced a low
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-123ºC 79ºC .88 g/cm3 Yes 1-Bromobutane C4H9Br 137.02 g/mol -112ºC 101.4ºC 1.26 g/cm3 Yes 2-Chlorobutane C4H9Cl 93.56 g/mol -140ºC 68ºC 0.87 g/cm3 Yes 2-Chloro-2-methylpropane C4H9Cl 92.57 g/mol -26ºC 51ºC 0.84 g/cm3 Yes Bromobenzene C6H5Br 157.01 g/mol -30.8ºC 156ºC 1.49 g/cm3 Yes Cis-1-Chloro-2-butene C4H7Cl 90.55 g/mol -65ºC 63.5ºC 0.923 g/mL Yes Trans-1-Chloro-2-butene C4H7Cl 90.55 g/mol -65ºC 68ºC 0.923 g/mL Yes 1-Chloro-2-methylpropane C4H9Cl 92
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as well as an iodine crystal‚ which facilitates the reaction by cleaning the surface of the magnesium metal. Bromobenzene and anhydrous diethyl ether were then added to the flask. Anhydrous ether was used because at this point‚ no water was to enter the reaction. The reaction was triggered by swirling and the heat of a human hand. From here‚ the refluxing began and ended once the bromobenzene addition was completed. The second phase of the experiment involved the reaction of the phenylmagnesium bromide
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CONTENTS CONTENTS | PAGES | 1) Abstract | 2-3 | 2) Introduction | 4-6 | 3) Objectives‚ Materials and Apparatus‚ Chemicals | 7 | 4) Method | 8 | 5) Results | 9-11 | 6) Discussion | 12 | 7) Conclusion | 13-14 | 8) References | 15 | ABSTRACT This experiment is about steam distillation by using Dalton’s Law. The objectives of this experiment are to demonstrate a separation of a mixture by using steam distillation and next to prove that Dalton’ Law and ideal gas law are
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Halides in Substitution Reactions Materials & Methods: Materials used: 1-bromobutane 1-chlorobutane bromocyclopentane Bromocylcohexane 2-chlorobutane 2-bromobutane 2-chloro2-metylpropane 2-bromo-2-methylpropane Crotyl chloride Bromobenzene Benzyl chloride 1-chloroadamantene Methods/Techniques: Physiochemical Research: Reagent | Formula Weight | Density | Boiling Point | Melting Point | Color | 1-bromobutane | 137.023 g/mol | 1.2676 g/ml | 372-376 K | 160.7 K | Clear |
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electrophile in the nitration reaction‚ will attack the benzene ring and produces the nitrobenzene ring. Resonance-stabilized arenium ion is created when the nucleophilic carbon pi bond on the acetanilide reacts with the nitronium ion. The aromaticity of the compound is lost in this important step. Water‚ acting as the Lewis base‚ removes a proton from the carbon bonded to the nitro group‚ an aromatic benzyl structure is created again: nitroacetanilide; thus ending the nitration reaction (1). Next
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Preparation of methyl m-nitrobenzoate by nitration using methyl benzoate‚ nitric acid‚ and sulfuric acid Aileen Quintana TA: Sijie Tues/Thurs 11:50 42067 Introduction: The purpose of this lab was to explore the concepts of electrophilic aromatic substitution‚ specifically nitration by synthesizing methyl m-nitrobenzoate using methyl benzoate‚ nitric acid and sulfuric acid. This nitration is a type of electrophilic aromatic substitution. A
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stabilized therefore produces a stable carbocation which favors SN1. Benzyl Chloride This reaction occurred in 2:09 because this chemical is resonance stabilized therefore produces a stable carbocation which favors SN1. Bromobenzene This did not react because bromobenzene produces and unstable carbocation. Bromocyclohexane This reacted in 10 seconds because bromocyclohexane is secondary bromine‚ and has steric strain‚ since it is a cyclic compound. The bigger steric in a molecule‚ the harder
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