The Purity and Purification of Solids Melting Point Lab Introduction: The point of this lab was to determine the eutectic point for the naphthalene biphenyl mixture‚ as well as determining the melting point of an unknown substance by comparing it with two known samples. Melting point is a temperature in which a substance changes from solid state to liquid state. Melting points are used to determine whether the given substance is pure or not. Substances that melt sharply‚ less than 1-2°C indicates
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Lab 6: Organic Compound Analysis Isabella O’Toole CHY 116 Friday 1:15-4:00 Lab Conducted on 4-12-13 and 4-19-13 4-26-13 This lab was conducted in order to determine the chemical composition of an unknown organic acid. A known mass of acid was dissolved into 30mL of either water or methanol (depending on solubility) and titrated with standardized sodium hydroxide. Data from this allowed the molar
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Identification of Unknown Organic Compound by Melting Point (M.P)‚ Boiling Point (B.P) and Infrared Spectroscopy Methods and Background The main objective of this lab is to identify the given unknown organic compounds with various methods. Identification of an unknown compound is important to perform through the process of melting point (M.P)‚ boiling point (B.P) and Infrared spectroscopy (I.R). Index of Hydrogen deficiency (IHD) and elemental analysis makes an experiment more efficient in
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Date Performed: November 18‚ 2010 2009 – 14077 Ma’am Rea Abuan Experiment # 1 SOLUBILITY OF ORGANIC COMPOUNDS State what types of intermolecular forces are present in solutions formed due to intermolecular attractions between the solute and the solvent. Compound 1 Compound 2 Intermolecular Forces Class S (Water-soluble) Compounds Acetone Water Hydrogen Bonding & London Dispersion Forces Diethyl Ether Dipole – Induced Dipole & London Dispersion Forces
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Experiment 1: Solubility of Organic Compounds (Answers to Questions) Q1. State what types of inetmolecular forces are present in solutions formed due to intermolecular attractions between the solute and the solvent. A1. For Water-Soluble Compounds: Acetone – Water: Hydrogen bonding and van der Waals forces Acetone – Diethyl Ether: Dipole – (induced) dipole and van der Waals forces Sucrose – Water: Hydrogen bonding and van der Waals forces Ethyl alcohol – Water: Hydrogen bonding
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Identifying Organic Compounds 2. Purpose/Problem: I am doing this experiment to find out what kind of organic compounds are in test tubes A‚ B‚ C and D. I am curious to know if substance D was the lipid because it seemed thin and had a slightly yellow tint of color to it. 3. Research: In my research I was informed about facts and appearances of lipids. First of all lipids are non-polar compounds‚ thus they won’t dissolve in water. This is also known as being hydrophobic. They are made with one
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Question 1 (5 points) 1. Which of the following may lead to vertical integration? a) Technological interdependencies b) Reduced search and bargaining cost c) The hold-up problem d) All of the above Question 2 (5 points) Effective collusion generally is more difficult when a) the number of oligopolistic firms involved decreases b) the number of oligopolistic firms involved increases c) when customer orders are small‚ frequent‚ and received on a regular basis as compared
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(unknown) of Pancetin from last experiment and then compare its melt point to the two other possible substances. Theory Panacetin should be made up of about 50 percent of the unknown component that we previously separated out of Panacetin for testing. We suspect that this unknown compound is either acetanilide or phenacetin. From the solubility of acetaminophen and phenacetin‚ we could know both of them are relatively soluble in boiling water but insoluble in cold water so that we took the recrystallization
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The Separation and Purification of Organic Compounds Sunshine Marie Introduction Each year‚ many thousands of new or unknown organic compounds are prepared or extracted from natural sources such as plants‚ fungi and animals. In order to identify an unknown organic compound or the components of a mixture of organic compounds‚ it is necessary firstly to separate and purify the compounds. At any given temperature‚ a certain number of molecules of a substance in the liquid state have sufficient
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slowly from an undisturbed solution".2 In general‚ crystallization is the easiest process to purify a solid substance to an acceptable quality for basic laboratory work. EXPERIMENTAL SECTION The experimental procedures can all be found in the PSU Organic Chemistry Fall 2008 laboratory manual. 1 The ’General Procedure for Recrystallization ’ as outlined in Appendix B was used to recrystallize two samples. First‚ each empty collection jar was weighed and recorded. In the first recrystallization‚ 1
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