Measuring the Melting Points of Compounds and Mixtures Introduction This exercise dealt with the melting points of pure mandelic acid and benzoic acid. The eutectic temperature and composition of mandelic and benzoic acid mixtures were determined. And finally‚ an unknown was identified by its mixtures and melting point. The melting point of a compound is used by organic chemists not only to identify the compound‚ but also to establish its purity. To determine the melting point two temperatures
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Introduction The purpose of the experiment was to determine the melting points of compounds using a Mel-Temp device. The melting point of naphthalene‚ urea‚ and sulfanilamide are found. This is then followed by the measuring of an unknown compound‚ and an impure sample (a small amount of naphthalene mixed with the unknown). Experiment In the lab‚ the height of the chemical in the capillary was set to 2-3 mm thickness. The voltage at the Mel-Temp started at a low setting of 1.5-2. The heat was
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Guadamuz Organic Chemistry Lab/ Chem 234 02/17/13 Lab 2: Melting Points Purpose: To determine the purity of a substance using melting point as physical property. We must also learn how to identify an unknown compound using its melting point. We got to identify an unknown compound using mixture melting point and finally we must learn to obtain an accurate melting point using Mel-Temp apparatus. Procedure: Set voltage to obtain the desired heating rate at the anticipated melting point range
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Melting Point Determination Lab Materials: Graduated pipette Capillary tube Tin wipe Sample Melting temperature apparatus Thermometer Procedure: Take open end of capillary tube and tap it gently into sample. Take tin wipe and place over the opening. Gently tab it so the sample will funnel to the bottom of the tube. You may also use a graduated pipette to accomplish this. Now‚ place the capillary tube in the designated spot in the melting apparatus‚ and once placed‚ turn the apparatus
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Title Freezing and Melting Point Objectives 1. To gain proficiency in constructing a graph and plotting data points. 2. To determine the freezing points of a compound from the graph of decreasing temperature versus time. 3. To determine the melting points of a known and unknown compound. Introduction Physical changes are the changes in the physical properties of a substance (Moore‚ Stanitski & Jurs‚ 2009). Freezing point is the fixed temperature at which a pure liquid converted into crystalline
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Organic Chemistry: CHP 225 Thomas Hsieh Experiment 2: Boiling Points o Date experiment was performed: September 16‚ 2011 o Objective: To determine the boiling point of organic compounds such as tert-butyl alcohol‚ sec-butyl alcohol‚ n-butyl alcohol‚ and an unknown. o Principle: Boiling point is the temperature at which gas and liquid phases coexist in equilibrium. At this temperature‚ the vaporization rate and the condensation rate are equal. The liquid and vapor reach a state of dynamic
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of an Unknown Compound using Mixed Melting Point Method Winnie Adrian Ibanez‚ Jerome Allan Japitana‚ and Dante Jimenez III Group no. 7‚ 2Chem a Department of Chemistry‚ College of Science‚ University of Santo Tomas‚ España‚ Manila‚ 1015‚ Philippines |ARTICLE INFO |ABSTRACT | |Article history: |Keywords: |An unknown compound was determined
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Purpose The purpose of this lab is to find the boiling point of the liquid and find the melting point of the solid. Procedure Boiling point: To find the boiling point of Isopropyl Alcohol I put about 1 mL of it in the test tube. Then I attached the thermometer to the test tube with a rubber band(make sure the thermometer bulb is lined up with the end of the test tube). After that I made a water bath with a beaker and put in the test tube with the thermometer. I then used a burner and a burner stand
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average set of results by about 2‚ but‚ when graphing the alkalise by the boiling and melting point they both follow the same slope‚ it continues to rise just like the results gathered in the example do. 2. Which of the 2 unknown substances was which? How did you figure this out? The two unknown substances were the methanol and propenol because each of them were being tested in this experiment to discover the boiling point of each of these alcohols by analysing each of their temperatures to eventually
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FREEZING POINT DEPRESSION AND BOILING POINT ELEVATION DAY 1 – 04 FEBRUARY 2015 Colligative Properties Depends on the NUMBER of solute‚ not on the nature of solute particles Freezing Point Depression Boiling Point Elevation Vapor Pressure Lowering Osmotic Pressure Electrolyte and Nonelectrolytes Electrolytes •Separates in water forming a solution that conducts electric current •IONIC COMPOUNDS Non- electrolytes • does not allow the flow of an electric current • COVALENT COMPOUNDS Freezing
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