VI: Conclusion: The melting point of a compound is the temperature at which the solid is in equilibrium with its liquid. A solid compound changes to a liquid when the molecules acquire enough energy to overcome intermolecular forces holding them together in an crystalline lattice structure. The melting point range is defined as the span of temperature from the point at which the crystals first begin to liquefy to the point at which the entire sample is liquid. This data can be tabulated experimentally
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and Purification of Solids Melting Points CH-337 Abstract: The purpose of this experiment was to find the eutectic point for the mixture of naphthalene and biphenyl. This was done by measuring the melting point of both pure substances and five mixtures of different ratios. The purpose of the second section was to identify an unknown sample by measuring its melting point and mixing it with two known substances and comparing them. The results suggest that the eutectic point is closest to the weight
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PREPARATION OF ASPIRIN AND DETERMINATION OF THE MELTING POINT Ferrer‚ Lara Melissa V. Faculty of Engineering University of Santo Tomas Manila‚ Philippines ABSTRACT This experiment involved three steps: synthesis of aspirin‚ isolation and purification‚ and the estimation of purity of the final product. The synthesis involved the reaction of salicylic acid and acetic anhydride in the presence of a catalyst‚ phosphoric acid‚ H3PO4. When the aspirin was prepared‚ it was isolated and filtered. The percentage
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Measuring the Melting Points of Compounds and Mixtures Introduction This exercise dealt with the melting points of pure mandelic acid and benzoic acid. The eutectic temperature and composition of mandelic and benzoic acid mixtures were determined. And finally‚ an unknown was identified by its mixtures and melting point. The melting point of a compound is used by organic chemists not only to identify the compound‚ but also to establish its purity. To determine the melting point two temperatures
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the esterification of p-aminobenzoic acid with ethanol. The percent yield of crude product was determined to be 21% and the melting point was recorded at 86.2°C ± 0.2°C‚ with a 6.3% error from 92°C‚ the literature melting point of pure benzocaine. The crude product was then recrystallized to improve the purity of benzocaine and 57.4% was recovered. The new melting point range was measured at 89.1°C ± 0.3°C‚ which has a 3.15% error. The infrared spectrum of the recrystallized product was measured
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Organic Chemistry Lab EXPERIMENT #2 and #3 Extraction and Evaporation Recrystallization and Melting Point Measurement PURPOSE: 1. To the components of a simulated pharmaceutical preparation‚ Panacetin‚ and identifying the unknown component of the mixture through extraction and separation methods. 2. To learn how to purify by recrystallization‚ how to dry them and how to obtain a melting point. PRECAUTION: ACETANILIDE AND PHENACETIN ARE EYE AND SKIN IRRITANTS. Minimize contact with
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Experiment 2&3 Recrystallization and Melting Points Determinantion of Benzoic Acid Abstract In experiment 2‚ recrystallization was used to purify the crude benzoic acid extracted from a mixture during experiment 1. Then a percent recovery for this recrystallization process was calculated. In experiment 3‚ the melting point ranges of the crude and purified benzoic acid were both determined by using Melt Temp Apparatus. Introduction Recrystallization is a purification technique for non-volatile
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The Purity and Purification of Solids Melting Point Lab Introduction: The point of this lab was to determine the eutectic point for the naphthalene biphenyl mixture‚ as well as determining the melting point of an unknown substance by comparing it with two known samples. Melting point is a temperature in which a substance changes from solid state to liquid state. Melting points are used to determine whether the given substance is pure or not. Substances that melt sharply‚ less than 1-2°C indicates
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Question 1 (5 points) 1. Which of the following may lead to vertical integration? a) Technological interdependencies b) Reduced search and bargaining cost c) The hold-up problem d) All of the above Question 2 (5 points) Effective collusion generally is more difficult when a) the number of oligopolistic firms involved decreases b) the number of oligopolistic firms involved increases c) when customer orders are small‚ frequent‚ and received on a regular basis as compared
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(unknown) of Pancetin from last experiment and then compare its melt point to the two other possible substances. Theory Panacetin should be made up of about 50 percent of the unknown component that we previously separated out of Panacetin for testing. We suspect that this unknown compound is either acetanilide or phenacetin. From the solubility of acetaminophen and phenacetin‚ we could know both of them are relatively soluble in boiling water but insoluble in cold water so that we took the recrystallization
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