FOUNDATION IN SCIENCE INTRODUCTION TO PRACTICAL ORGANIC CHEMISTRY – MAKING AND PURIFYING ORGANIC COMPOUNDS Stage 1 – Deciding how much reagent to use Most organic reactions do not go to completion; most reach an equilibrium position with significant quantities of reactants still remaining. In addition‚ separating the desired product from the rest of the reaction mixture‚ and then purifying it‚ will result in the loss of more of the product. The amount of product obtained expressed as a percentage
Free Distillation Sulfuric acid Acetic acid
Introduction Friedel-Crafts acylation of anisole with acetic anhydride was used in this experiement to synthesize 4-methoxyacetophenone with the use of a reflux apparatus. Friedel-Crafts reactions can be done by alkylation‚ which involves mixing an alkyl or acyl halide with a Lewis acid‚ or acylation‚ which is done with acid chlorides or anhydrides(Lefevre). Acylation was used because it does not have as many disadvantages aklyations reactions have such as polyalkylation‚ second electrophilic attacks
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Objective: The purpose of the lab is to learn filtering techniques. Specifically‚ to form and filter a calcium carbonate precipitate using a Buchner funnel. Procedure: a.) Prepared a mixture of .5 M calcium nitrate (45 mL) and .01 M sodium carbonate by combining and stirring the two liquids in a beaker. Allow the mixture to stand. b.) Prepare the filtration assembly. The assembly consists of a tapered flask with a buchner funnel inserted in the top. The funnel has a rubber stopper attached
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Mario Troncoso 20025019 Dehydrating Cyclohexanol Structure/MSDS: Anhydrous calcium chloride—irritant and hygroscopic (calcium chloride) cyclohexanol—irritant and hygroscopic (cyclohexanol) cyclohexene—flammable and irritant (cyclohexene) Sulfuric acid—toxic and oxidizer (Sulfuric acid) phosphoric acid—corrosive (phosphoric acid) Results/Data: End product weighed 0.109g of cyclohexane and tested positive with bromine test Discussion: In order to perform
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Beer-Lambert Law Gabe Garrison & Paige England Buffalo High School Abstract In this lab‚ the Beer-Lambert Law is tested by using a spectrophotometer. This is a quick and easier way to determine the concentration of a solution. Keywords: Beer-Lambert Law‚ Spectrophotometer‚ concentration Beer-Lambert Law The Beer-Lambert-Law states that
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SYNTHESIS OF TRANS-9-(2-PHENYLETHENYL) ANTHRACENE (A WITTIG REACTION) Introduction: The purpose of this experiment is to convert carbonyl compounds to alkenes using Wittig reaction. In this case we will be synthesizing Trans-9-(2-phenylethenyl) anthracene from benzyltriphenylphosphonium chloride and 9-anthraldehyde. We will also aim to obtaining a high percent yield and purity for the synthesis of Trans-9-(2-phenylethenyl) anthracene. The mechanism for this reaction goes thus:
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Lab report April 14‚ 2013 Abstract: In this article‚ we will experiment on the significant in strength of the enzyme by using three different test tubes and measuring the amount of product they give off. To determine this we are going to test the amount of color absorbance by using a special tool to help us understand our results. We will see how our end results show the effect of the amount of concentration we apply to each test tube. The results would be shown by the support of two graphs
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Estimating Osmolarity of Plant Cells Criteria Assessed: DCP Introduction In this experiment you will be estimating the osmolarity of potato cells by finding their change in weight in solutions of known molarity. The object is to find the molarity where the mass does not change. No net change in weight indicates that there has been no net gain or loss of water. This is a means of indirectly finding the osmolarity of the cells themselves. Apparatus 1 large potato Petri dish 7 x 250 ml beakers
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Modbury High School SACE Stage 1 Chemistry Topic 5 Mole Concept and Stoichiometry Assignment 5: Volumetric analysis (titrations)‚ stoichiometry SOLUTIONS Note: Write answers neatly and legibly in your exercise book or on pad paper. ALWAYS include a title and name for your work and clearly indicate each answer. 1. a) 23.08 and 23.00 mL are concordant titre values. Average titre = (23.08 + 23.00) = 23.04 mL 2 b) Ca(OH)2
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Aim: determine the mass of calcium carbonate in chicken eggshells and hence its percentage by mass Apparatus Uncertainty 25.00 cm3 pipette ± 0.03 cm3 50.00 cm3 burette ± 0.05 cm3 250.0 cm3 volumetric flask ± 0.3 cm3 50.0 cm3 measuring cylinder ± 0.5 cm3 Electronic balance ± 0.01 g Uncertainty of apparatus Measurement Mass of eggshell = 3.15 ± 0.01 g Volume of HCl added = 50.00 ± 0.5 〖cm〗^3 Volume of solution = 250.0 ± 0.3 〖cm〗^3 Volume of NaOH pipetted = 25.00 ± 0.03 〖cm〗^3
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