A Report of Experiment 1 Purification and Identification of An Unknown Mixture Aim To separate a mixture of a neutral (ester‚ alcohol‚ ketone‚ aldehyde or ether) and an acidic compound (phenol or carboxylic acid) or a neutral and a basic compound (amine)‚ and to identify the unknown mixture by physical (M.P. or B.P.) and spectroscopic methods (NMR‚ IR and MS). Method The mixture (sample number: 27) was dissolved in 200 mL of CH2Cl2 and then extracted with 10% NaOH. The acid was removed
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Experiment 15 The Purification of Water Date Performed: 9/25/2012 Joe Shmoe Date Submitted: 9/26/2012 Chemistry 1046L-sec07 Lab TA: Blankity Blank Purpose: The purpose of this experiment is to learn about the various processes by which water is processed and treated. This experiment will involve removing chemical impurities in water through using techniques such as absorption spectrophotometry‚ sample collection‚ serial dilution‚ filtration PH and graphical analysis. If this
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quite pure. 2. Suppose you were performing a recrystallization and you had just added the optimal amount of boiling solvent to dissolve your impure solid…but then you a squirrel ran by and you decided to chase it. When you got refocused and returned to your experiment‚ you realized that you’d left your Erlenmeyer flask containing your recrystallization solution on the hot plate for too long. (1) How did you know that you’d left your flask on the hot plate for too long? and (2) how can you correct
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Recrystallization Experiment 2: Recrystallization & Melting Point • Most important method for the purification of organic solids • Separation of compounds based on differences in solubility between the compound of interest and its contaminants • Basic technique: 1. dissolve impure sample in an "appropriate" hot solvent Part A: Choosing a Solvent Part B: Purification of Phenacetin 2. cool solution slowly to induce crystal growth 3. filter resulting mixture to isolate crystals Reading:
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mummion assignment Task 1 – purification Aim We were given a sample of mummion in the form of dried mud from a lake; the aim of the practical was to purify the sample and separate it from the insoluble impurities into the form of mummion salt. Context A long time ago mummion was used to preserve the bodies of ‘mummies’ in ancient Egypt‚ mummion along with other naturally occurring preservatives was used to treat the organs before the bodies were wrapped. This purification practical happens very often
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Synthesis of Acetanilide By: Rick Whitely April 9‚ 2013 Organic Chemistry Lab 1; Professor J. Hutchison Recrystallization is a common method of purifying organic substances through the differences in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heated water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes
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Experiment AM1.4--Bending moments in a simply supported beam Student name JunJie Liu Student ID 1512042 Experiment Date 24 Nov 2014 Lab group Mech 7 Introduction In this lab report we show the basic methods of measuring bending moment at the “cut” assuming only simply supported beam with point loads (showed in figure 1) and illustrate the relationship among bending moment and distance between
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Osmosis Experiment Dennis M. Feliciano Grand Canyon University BIO100L Biology Concepts Lab June 25‚ 2011 Osmosis Experiment Materials Grapes (unblemished) Raisins (larger is better) Water Salt Four small containers (i.e.‚ drinking cups or clear glasses) A metric ruler Methods and Procedure Place 1 cup (236 ml) of water in each of the 4 containers. In 2 of the containers‚ add 1 tablespoon (14.8 ml) of table salt and mix well. Measure the length and width of a raisin and place
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Colegio de San Juan de Letran College of Liberal Arts and Sciences Experiment #3 SEPARATION AND PURIFICATION OF ORGANIC COMPOUNDS: CRYSTALLIZATION Gomez‚ Paola Anne M. DOP: 2 July 2013 Student no. : 4120403 DOS: 9 July 2013 Group: Carcinogenic Remarks: _____________________________________________________________________ Engr. C. D. Sanchez Instructor THEORETICAL DISCUSSION Crystallization is a technique which chemists use to purify solid compounds. It is
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RECRYSTALLIZATION OF ACETANILIDE ABSTRACT Recrystallization is the primary method for purifying solid organic compounds through the differences in solubility at different temperatures. In this experiment‚ a suitable solvent was first determined. Acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heating water bath. The hot solution was filtered and the filtrate‚ cooled slowly in an ice bath as crystals started forming
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