Grignard Reaction: Synthesis of Triphenylmethanol Hai Liu TA: Ara Austin Mondays: 11:30-2:20 Abstract: In this experiment‚ phenylmagnesium bromide‚ a Grignard reagent was synthesized from bromobenzene and magnesium strips in a diethyl ether solvent. The Grignard reagent was then converted to triphenylmethanol‚ a tertiary alcohol with HCl. The reaction for phenylmagnesium bromide was: The reaction for Grignard to triphenylmethanol was: In the formation of the Grignard reagent
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Writing Practical Reports Aim: To observe what happens during and after a chemical reaction. Equipment: Concentrated nitric acid in a glass dropping bottle Small pieces of Copper 250ml Beaker 2 M Lead nitrate in a dropping bottle 2 M Potassium iodide in a dropping bottle 2 M Copper sulfate in a dropping bottle 2 M Sodium hydroxide in a dropping bottle 2 M Hydrochloric acid in a dropping bottle 4 Pyrex test tubes Test tube rack Spatula Bunsen burner‚ gauze
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Link reaction The link reaction takes place in the mitochondrial matrix and its main function is to turn the pyruvate into acetate for the kerb cycle. During the link reaction the pyruvate molecule undergoes decarboxylation and dehydrogenation‚ the enzymes pyruvate decarboxylase and pyruvate dehydrogenase remove the carboxyl group (which becomes a carbon dioxide molecule) and removes the hydrogen atoms from the pyruvate molecule. The coenzyme NAD accepts the two hydrogen atoms and becomes reduced
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The Grignard Reaction Abstract Through the use of the Grignard reaction‚ a carbon-carbon bond was formed‚ thereby resulting in the formation of triphenylmethanol from phenyl magnesium bromide and benzophenone. A recrystallization was performed to purify the Grignard product by dissolving the product in methanol. From here‚ a melting point range of 147.0 °C to 150.8 °C was obtained. The purified product yielded an IR spectrum with major peaks of 3471.82 cm-1‚ 3060.90 cm-1‚ 1597.38 cm-1‚ and 1489
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the value of the sum for Reaction 1 and Reaction 2’s change in temperature‚ compared to Reaction 3’s change in temperature. Reaction 1 was the dissolution of solid sodium hydroxide in water with a ΔH°rxn of -47047 J/mol‚ Reaction 2 was the neutralization of liquid sodium hydroxide with HCl with a ΔH°rxn of -31289 J/mol and Reaction 3 was the dissolution and neutralization of solid NaOH with HCl with a ΔH°rxn of -91000 J/mol. Consequently‚ the sum of Reaction 1 and Reaction 2 was -78336 J/mol‚ similar
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affecting the rate of reaction‚ PNPP (p-nitrophenyl phosphate) + H20 ? PNP (p-nitrophenol) + H3P04. This reaction is catalyzed by the enzyme phosphatase. Different environments produced different reaction rates as environmental factors affect the efficiency of phosphatase. This is because environmental factors can change the tertiary structure of phosphatase‚ which alters its active site‚ and thus changes its efficiency to catalyze the reaction. We measured the rate of reaction‚ by using a chromogenic
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Examples of synthesis reactions: 1. Metal + oxygen → metal oxide EX. 2Mg(s) + O2(g) → 2MgO(s) 2. Nonmetal + oxygen → nonmetallic oxide EX. C(s) + O2(g) → CO2(g) 3. Metal oxide + water → metallic hydroxide EX. MgO(s) + H2O(l) → Mg(OH)2(s) 4. Nonmetallic oxide + water → acid EX. CO2(g) + H2O(l) → ; H2CO3(aq) 5. Metal + nonmetal → salt EX. 2 Na(s) + Cl2(g) → 2NaCl(s) 6. A few nonmetals combine with each other. EX. 2P(s) + 3Cl2(g) →
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NaHCO3 and NaCl and calculate a balanced equation for this reaction. Safety: • Wear safety goggles at all time • Handle all chemicals with care • Use equipment like tongs when handling warm/hot objects • If chemicals are spilt on self‚ wash off immediately • Stand at all times Hypothesis: The NaHCO3 will react successfully with the HCl and will form NaCl‚ H2O and CO2. Then be able to work out a balanced equation for the reaction and work out the moles of NaHCO3 and NaCl. Materials:
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observe how the change in solvent polarity affects the rate and to determine the kinetics of a solvolysis reaction. In this experiment‚ we used 1-chloro-1-phenylethane in acetone in one reaction with 50% ethanol-50% water and in another reaction with 40% ethanol-60% water. To monitor he rate of reaction‚ we would need the concentration of the alkyl chloride at the beginning of the reaction and at a time t‚ but since we did not determine the concentrations‚ we monitored the rate of formation of
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A. Introduction Title: The effect of reading Shakespeare on reaction time Research Question: Does reading a passage of Shakespeare decrease a person’s reaction time while completing a puzzle? One day in class‚ I was reading an interesting article about how people who read and are exposed to Shakespeare and Wordsworth and other renowned writers have better brain activity‚ attention spans‚ and can have more moments of beneficial self-reflection. In the article‚ scientists and psychologists at Liverpool
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