the aromatic hydroxyl compound‚ eugenol from crushed cloves using steam distillation. After conducting the distillation‚ the expected two layers were not visible in the centrifuge tube. Subsequently‚ the extraction and evaporation did not produce the expected oil. This result is probably due to the collection of only water vapor during distillation. From another group’s data‚ 3.80% of the oil was recovered from the cloves in which the major component is eugenol. The IR spectrum obtained is consistent
Premium Water Distillation Evaporation
Isolation of Acetyleugenol (Clove Oil) from Cloves Purpose In this experiment‚ you will obtain the essential oil from cloves by steam distillation. You will then separate a component (acetyleugenol) from the oil by liquid-liquid extraction. Finally‚ you will isolate the acetyleugenol by using a rotovap for reduced pressure distillation‚ which will remove the organic solvent (dichloromethane). Background Whole cloves contain between 14% and 20% by weight of essential oils‚ but
Premium Distillation
Experiment 2: Isolation of Eugenol from Cloves Background; Readings on Vapor pressure‚ Raoult’s Law from TRO: A mixture of the essential oils‚ eugenol and acetyleugenol‚ will be steam distilled from cloves. These compounds are isolated from aqueous distillate by extraction into dichloromethane. The dichloromethane solution is shaken with aqueous sodium hydroxide‚ which will react with eugenol‚ to yield the sodium salt of eugenol in the basic aqueous
Premium Distillation Vapor pressure Sodium hydroxide
Infrared Spectroscopy Organic Chemistry Lab 301A B. The purpose of this lab is to study Infrared Spectroscopy‚ which focuses on the study of the electromagnetic spectrum. The area to be studied is the infrared region‚ which is made up of gamma‚ X‚ and UV rays. We want to be able to identify spectra’s to their complementary structures. The background of this experiment particularly deals with the study of compound structure determination‚ and traits. We must be aware of the functional groups
Premium Light Infrared Ultraviolet
Experiment 4: Isolation of Essential Oils from Eugenol Background: Anyone who has walked through a forest or who enjoys the variety of fragrances that flowers have to offer knows that many plants and trees have their own distinctively pleasant odors. These odors are due to the volatile essential oils‚ many of which have been prized commodities since ancient times. If a list of commercially important essential oils was compiled the list would exceed 200 essential oils. Thyme‚ garlic‚ peppermint
Premium Distillation Water
Steam Distillation Purpose: To use steam distillation to purify heat sensitive‚ natural products‚ like essential oils. Procedure Please refer to: Williamson‚ Macroscale &Microscale Organic Experiments 4th Ed.‚ pgs.98-109 Results Table 1.1: Steam distillation Drop # (every third drop) Temperature (ºC) Addition of 0.5 mL water 1 100.3 Water added 2 100.5 3 100.5 Water added 4 100.6 Water added 5 100.6 6 100.6 Water added 7 100.6 8 100.6 Water added 9 100.3 10 100.6
Premium Water Distillation Vapor pressure
Results | 9-11 | 6) Discussion | 12 | 7) Conclusion | 13-14 | 8) References | 15 | ABSTRACT This experiment is about steam distillation by using Dalton’s Law. The objectives of this experiment are to demonstrate a separation of a mixture by using steam distillation and next to prove that Dalton’ Law and ideal gas law are applicable in steam distillation. Dalton’s Law; While Ideal Gas Law; This experiment is conducted by placing 2mL of Turpentine and 15mL of water into
Free Gas Pressure Distillation
Steam Distillation 6.6.12 Aim: To isolate and extract citrol from lemongrass oil using steam distillation. Theory: Impure chemicals are usually purified using distillation‚ allowing the changes in boiling points to separate the substances. Chemicals with high boiling points decompose before reaching the temperature necessary for separation‚ leading to the invention of steam distillation. The contamination is separated at lower temperatures and allows the separation of chemicals from their
Premium Distillation
perform a steam distillation using a microscale distillation apparatus and isolate a natural product from cloves. Introduction By performing steam distillation we can isolate eugenol at lower temperature than its usual boiling point of 248 degree Celsius. Eugenol belongs to a category called essential oil. Many of these compounds are used as flavoring and perfumes and in the past were considered the essence of plant from which they were derived. Structure of eugenol (clove oil) and eugenol acetate:
Premium Distillation Essential oil Solvent
Isolation and Identification of Eugenol: The Fragrant Component of Cloves *Adri‚ Kiersten Jayne R.‚ Aguinaldo‚ Samuel Jr. Group 2 Department of Chemistry‚ College of Science University of Santo Tomas‚ España‚ Manila 1008 Abstract. In this experiment‚ the primary objective was to isolate eugenol from cloves. An amount of 30 grams of dried cloves and 300 mL of water was distilled over a flame for over 2 hours. The distillate underwent extraction with dichloromethane‚ water and sodium hydroxide
Premium Oxygen Water Chemistry