The purpose of this experiment was to synthesize isopentyl acetate via an esterification reaction between acetic acid and isopentyl alcohol‚ using concentrated sulfuric acid as a catalyst. The product was washed with sodium hydrogen carbonate‚ as well as with water‚ then dried with anhydrous sodium sulfate. The product was then distilled using a Hickman still and characterized using infrared spectroscopy. The percent yield of isopentyl acetate was 61.52%. This may have been low due to not all of the
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Simple Distillation of Ethyl Acetate contaminated with Methyl Violet Operational OrganicChemistry A Problem Solving Approach to the Laboratory Course‚ 4th edition‚ by John Lehman‚ Experiment 4‚ OP-30 pg 710-719 I. Introduction The students will use the distillation method to extract pure Ethyl acetate by using the distillation equipment. The distillation is the process of vaporizing a liquid mixture in one vessel and condensing the vapors into the receiver. II. Experimental procedures. 1
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Synthesis of Isopentyl Acetate (Banana Oil) Using a Fischer Esterification Reaction Zhenshu Wang (Stan) TA: Aaron League September 23‚ 2012 Purpose: The purpose of the experiment was to perform the acid-catalyzed Fischer Esterification of acetic acid and isopentyl alcohol to form isopentyl acetate‚ or banana oil‚ which is used in flavor industries. The equilibrium of the reaction was changed by adding an excess amount of acetic acid. The reaction was refluxed and product was purified by extraction
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EFFECTS OF LEAD ACETATE IN THE EMBRYONIC DEVELOPMENT OF SEA URCHINS (Tripneustes gratilla) Belderol‚ Jacqueline Busmeon‚ Chadinne Dablo‚ Elgen Ray Edding‚ Desza Hulsey‚ Shirley Montano‚ Margaret Ragasa‚ Jay Andie Susaya‚ Mariz Veedor‚ Marielle Science Cluster University of the Philippines Visayas Cebu College Gorordo Avenue‚ Lahug‚ Cebu City 6000 ABSTRACT One of the greatest threats to health and the environment is the current problem regarding pollution. Pollution
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roxatidine acetate hydrochloride with cyclomaltoheptaose (b-cyclodextrin) using IR and NMR spectroscopy Arti Maheshwari a‚⇑‚ Manisha Sharma a‚ Deepak Sharma b a b Department of Chemistry‚ IET‚ Mangalayatan University‚ Beswan‚ Aligarh‚ India Department of Physics‚ IET‚ Mangalayatan University‚ Beswan‚ Aligarh‚ India a r t i c l e i n f o a b s t r a c t NMR chemical shift changes of the cyclomaltoheptaose (b-cyclodextrin‚ b-CD) cavity protons as well as roxatidine acetate hydrochloride
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Experiment 2: Synthesis of Isoamyl Acetate (Banana Flavor) Paul Symon C. Manuel*‚ Katherine Merene‚ Charlene Mondelo‚ and Pamela Mallari Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines Abstract: The purpose of this experiment was to synthesize isoamyl acetate via an esterification reaction between acetic acid and isoamyl alcohol‚ using concentrated sulfuric acid as a catalyst. The product was washed with sodium hydrogen carbonate‚ as well as with water‚ and then dried
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purification‚ and characterization of isoamyl acetate‚ or banana oil‚ was determined. The synthesis was completed by a reversible esterification reaction which required the heating of glacial acetic acid and isoamyl alcohol‚ combined with a sulfuric acid catalyst in hexane. In order to increase the efficiency of the reaction‚ LeChatelier’s Principle is utilized by removing water from the products. As a result‚ the reaction as a whole shifts the left producing more isoamyl acetate to try and balance the reaction
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Department of Biological Science‚ College of Science‚ University of Santo Tomas‚ Manila‚ Philippines Abstract This experiment is conducted to exhibit the synthesis of banana flavoring in the laboratory through the esterification of isoamyl alcohol and acetic anhydride with the use of the Fischer reaction. The set-up used was the reflux modified with a water bath at the constant temperature between 75-80oCelsius. The actual yield that was attained is 0.4271 grams of banana essence. The
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Camille B. Valdez‚ Ariza Yamashita Department of Biological Sciences‚ College of Science Group 11 Corresponding author: gerome_911@yahoo.com Abstract The purpose of this experiment was to synthesize isopentyl acetate via Fischer esterification reaction between acetic anhydride and isoamyl alcohol‚ using concentrated sulfuric acid as a catalyst. This reaction is characterized by the combining of an alcohol and an acid (with an acid catalyst) to yield and ester plus water. In order to accomplish this
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Neurophysiology of Nerve Impulses ACTIVITY 1 The Resting Membrane Potential 1. Explain why increasing extracellular K+ reduces the net diffusion of K+ out of the neuron through the K+ leak channels. If the extracellular K+ increases then the concentration of intracellular K+ will decrease causing a decrease in the steepness of the concentration gradient and fewer K+ ions would be drawn out. 2. Explain why increasing extracellular K+ causes the membrane potential to change to a less negative
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