Copper-Catalyzed Oxidation of Benzoin to Benzil prepared by Carl T. Wigal‚ Lebanon Valley College PURPOSE OF THE EXPERIMENT Oxidize benzoin to benzil using ammonium nitrate and copper(II) ion as a catalyst‚ monitoring the reaction by thin-layer chromatography. Characterize the product using melting point measurement and infrared spectroscopy. EXPERIMENTAL OPTIONS Semi-Microscale Oxidation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Microscale Oxidation . . . . . .
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Experiment 39 Oxidation – Reduction Titrations II : Analysis of Bleach A. Standardization of 0.05 M Na2S2O3 Solution KIO3 concentration 0.01 M Volume of KIO3 Trial #1 Trial #2 Final burette reading 15.01 mL 30.00 mL Initial burette reading 0.00 mL 15.01 mL Milliliters of KIO3 used 15.01 mL 14.99 mL Volume of Na2S2O3 Trial #1 Trial #2 Final burette reading 13.40 mL 25.78 mL Initial burette reading 0.03 mL 13.37 mL Milliliters of Na2S2O3 used
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YOUR NAME: Erin Alston‚ Kennedy Stuart‚ Amber Lamb and Stephonya Williams EXPERIMENT TITLE: Oxidation: Cyclohexanone from Cyclohexanol by Hypochlorite Oxidation and Adipic Acid from Cyclohexanone DATE: 4/18/2014 INTRODUCTION: In experiment 4‚ alcohol is oxidized to a ketone with household bleach. The product is then isolated by steam distillation and is extracted into the distillate with ether. After the removal of ether‚ it leaves the product cyclohexanone. In experiment 6‚ cyclohexanone is
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Name: Date of experiment: 04/02/12 Date of report: 04/03/12 Title: Oxidation – Reduction Activity Series Purpose: To determine relative oxidizing and reducing strengths of a series of metals and ions. Oxidation and reduction reaction occur simultaneously side by side. A reduction reaction occurs only if an oxidation reaction occurs and vise-versa. Electrons are given in oxidation while in reduction electrons are gained. Oxidizing agent is a chemical substance which has a large tendency to
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1. Mechanism of oxidation process In an oxidation process of silicon that usually takes place at very high temperature (thermal oxidation)‚ silicon (Si) reacts with either water vapor (H20) or oxygen (O2) to form silicon dioxide‚SiO2 on the silicon surface. The reaction is represented by following equations: Dry oxidation: Si + O2 → SiO2 Wet oxidation: Si + 2H2O → SiO2 + 2H2 The oxidation process can be implemented through diffusion
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Oxidation Number When elements combine to produce a compound‚ each element is assigned an “apparent” charge. This apparent charge‚ the charge an atom would have if both electrons in each bond were assigned to the more electronegative element‚ may be positive or negative. It is called the oxidation number or state of the element in the compound. Oxidation numbers are very useful in keeping track of what happens to electrons when various elements combine to form compounds. By remembering a few
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potassium permanganate solution was titrated thrice to give clear Mn2+ with an analyte of acidified FeSO4 until all the Fe2+ in the solution was oxidized to Fe3+. The color of the MnO4-/Mn2+ was used as the indicator for the titration. A balanced oxidation-reduction‚ the molarity/normality of the standards potassium permanganate‚ and the volume of potassium permanganate used allowed the determination of the concentration of the FeSO4. Equipment and Chemicals: Chemicals: * Iron (II) ammonium sulfate
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STK 1084 Inorganic Chemistry I‚ LU 3 Oxidation – Reduction Reactions‚ Prepared By: Dr. Tay Meng Guan‚ Faculty of Resource Science and Technology‚ Universiti Malaysia Sarawak. LU 3 Oxidation and Reduction Reactions 3.1 Ideas of Oxidation and Reduction Oxidation of an atom can be occurred in the following conditions: 1. Losing an electron from the orbitals. e.g.: A A+ + e- 2. Adding an electronegative element (e.g.: F‚ Cl‚ Br‚ O) to a molecule. e.g.: A + F AF 3. Losing hydrogen
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procedure. Results and Analysis {Limiting reagent} Mass benzoin = 2.0050g (0.00945 mole) Mass sodium borohydride = 0.4059g (0.0107 mole) Mass compound A used to form compound B = 1.0647g Results Mass (g) moles Molecular formula Yield (%) Mp (pure) Compound A 1.7458 0.00815 C14H14O2 86.22 138-139 Compound C 0.4255 0.001988 C14H14O2 40.02 136-138 Spectral Analysis IR Absorption (cm-1) Assignment Benzoin 3411‚ 3374 OH 2961‚ 2903 C-H aromatic 2358 C-O
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Synthesis of Benzoin Date of Experiment: 1-26-15 Chelsea Price Lab Partner: Joey Simmons Abstract: In this experiment‚ benzoin was synthesized from benzaldehyde‚ using thiamine hydrochloric acid as a catalyst. The thiamine HCl was deprotonated by sodium hydroxide and acted as a nucleophile to attack the benzaldehyde. A water-cooled condenser was used to heat the solution at reflux. Vacuum filtration was used to wash and dry the product. The benzoin product was recrystallized
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