thick white/yellow precipitate formed cloudy yellow precipitate formed REACTION W/ NH4OH does not dissolve; precipitate becomes defined does not dissolve; precipitate becomes defined does not dissolve TABLE 2: REACTION OF HALOGENS WITH HEXANE AND CHLORINE WATER REACTION NAF NABR KI COLOR OF THE TOP LAYER clear yellow pink IS THIS HALOGEN MORE OR LESS ACTIVE THAN CL? more less less TABLE 3: REACTION OF UNKOWN HALOGEN D WITH CA(NO3)2 AND AGNO3 REACTION USED TO
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There are many different binding modes of ligands to transition metal atoms. In past experiments with Co(II) and Co(III)‚ you observed that a ligand such as Chloride or amine can coordinate in a monodentate fashion. You also observed that carbonate occupies two sites of a transition metal and is known as a bidentate ligand. In this experiment‚ you will observe the reaction of a -bond in an olefin with a molybdenum metal center to form a piano-stool shaped molecule. The molybdenum metal retains
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Mapua Institute of Technology School of Chemical Engineering and Chemistry Muralla St.‚ Intramuros‚ Manila Melting Point and Boiling Point of Organic Compounds Group No. 5 Manacup‚ Cris Vincent L. Oblena‚ Adrian D. Ong‚ Joshua Jyro B.* *Leader ABSTRACT In compounds‚ two of the physical properties affected by the varying structures are melting point and boiling point. Through the use of the Thomas-Hoover Melting Point Apparatus or the micro method‚ the melting and boiling point of
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RECRYSTALLIZATION Lem Therese D. Delos Ama‚ Glenn Dale M. Desquitado‚ John Carlos M. Drapesa‚ Arianne Valerie B. Escritor‚ Elisha Ellis R. Esteva Group 4 2B Medical Technology Organic Chemistry Laboratory ABSTRACT In this experiment‚ acetanilide was used as the pure organic compound. Acetylation of aniline and acetic anhydride yields the crude product or crude acetanilide. The crude acetanilide was purified by dissolving it in hot water and then the solution was cooled slowly by placing in
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antibacterial and antifungal activity was subjected against clinically four bacterial strains and two fungal strains using agar well diffusion method and test tube dilution method respectively. The GC-MS study revealed the presence of ten compounds in n-hexane extract namely Hexadecane(1)‚ 2-[4a‚ 8-Dimethyl-3‚4‚4a‚5‚6-hexahydro-napthalene-2-yl]-prop-2-en-1-ol(2)‚ Heptadecane(3)‚ Benzene‚ [1-butylheptyl]-(4)‚ Benzene‚ [1-methyldecyl]-(5)‚ Oxirane‚ tetradecyl-(6)‚ Hexadecanoic acid‚ methyl ester(7)‚ Hexadecanoic
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Darlene Louise Estrada* and Rizhelle Evan Evaristo Department of Occupational Therapy‚ College of Rehabilitation Sciences University of Santo Tomas‚ Espaňa Street‚ Manila 1008 Date Submitted: February 2‚ 2011 Abstract: Organic compounds hexane‚ heptane‚ cyclohexane‚ cyclohexene‚ benzene‚ and toluene were subjected to different physical and chemical tests todifferentiate their intrinsic physical properties and chemical properties in terms ofstructure and behaviour. Nitration test (test
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In this lab‚ we extracted spinach pigments‚ and analyzed what colors of light these pigments absorb. By using TLC plate‚ hexane and acetone‚ I separated the pigments of spinach‚ and discovered that the main pigments were green and yellow. This works because with different polarities‚ pigments move at different rates. Hexane and acetone were also used to separate chlorophyll and carotene from spinach. Since they are polar‚ they can separate organic and inorganic things. From the experiment‚ I know
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protein from the subcellular organelles. This step is also known as homogenization. This step can be done with the use of blender. As the solution was homogenized‚ it may undergo saltation or acidation to remove impurities such as calcium anions. Hexane may also be used to defat the protein. Lastly‚ the solution undergoes differential centrifugation. This will separate the protein crude from the liquid. (Campbell) After protein purification‚ the crude now undergoes characterization. Activity assay
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handout "Organic Chemistry Experiment -- Hydrocarbons" Hazards: Open flame and hydrocarbons are flammable. Equations: 1. . 3. . 4. . 5. . Unknown #: 1B s-6 Hyd-3 (colorless liquid) Data/Observations: Test Bromine addition Alkane Mixture of hexane and dichloromethane was originally clear liquid. After adding 3 drops red color Br2/CH2Cl 2 the solution turned orange. Orange color held. Alkene Alkene used was pentene. Originally clear liquid. After addition‚ solution turned yellowish at first
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far to achieve accurate results. (7) In choosing a TLC solvent‚ a student found that a 50:50 hexane : acetone and 65:35 hexane : acetone give similar results. Which one should they use for their TLC plate development? Why? They should use hexane for their TLC plate development because you want to use the least polar solvent possible to achieve good results‚ and acetone is more polar than hexane. (8) Calculate the Rf values for compounds A‚ B and C below. (9) If a TLC plate shows only
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