Jennie K. Daniels Organic Chemistry 2121 11 February 2014 Synthesis of Aspirin Salicylic acid derivatives‚ or salicin‚ are found in the bark of the willow tree. In the 5th century B.C.‚ Hippocrates ground the bark into a powder‚ and later‚ the Natives Americans chewed on the bark to alleviate fever and pain1. In the 19th century‚ a German chemist by the name of Felix Hoffman wanted to find a medication that would ease
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REPORT EXPERIMENT 9 CARBOXYLIC ACID AND DERIVATIVES Date: January 19‚ 2004 Objectives: 1. To understand the reactions of carboxylic compounds and derivatives. 2. To know the methods for preparing carboxylic acid derivatives. 3. To know the methods for testing the carboxylic acid derivatives. Experimental Procedures: 9.1 Solubility 1. Prepare 3 test tubes with 3 ml of water in each. 2. Place 3 drops of acetic acid‚ benzoic acid‚ and oxalic acid in separate test tubes. 3. Shake and observe
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extraction‚ crystallization and melting point determination‚ preparations of organic compound and separation of mixtures. The Techniques Students are REQUIRED to read and understand the various techniques that will be covered in the laboratory sessions from the textbook. | Techniques | Page | 1 | Laboratory Safety | 6 | 2 | Laboratory Glassware | 31 | 3 | Measurement of Volume and Weight | 39 | 4 | Heating and Cooling Methods | 58 | 5 | Reaction methods (eg: distillation‚ reflux) | 68 |
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SYNTHESIS OF ESTERS USING GREEN AND NON-GREEN CHEMISTRY Abstract Esters are a class of organic compounds with the general formula RCOOR’. Ester also contributes the flavor and aromas in fruits and flowers. The esterification reactions will use in the procedure‚ which are the interaction of a carboxylic acid with an alcohol‚ aided by an inorganic acid catalyst (H2SO4). Moreover‚ the green method will not use any catalyst but using heating source instead (microwave). Based on the comparison of
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Vol. 1 ACETIC ACID 115 ACETIC ACID 1. Introduction Acetic acid [64-19-7]‚ CH3COOH‚ is a corrosive organic acid having a sharp odor‚ burning taste‚ and pernicious blistering properties. It is found in ocean water‚ oilfield brines‚ rain‚ and at trace concentrations in many plant and animal liquids. It is central to all biological energy pathways. Fermentation of fruit and vegetable juices yields 2–12% acetic acid solutions‚ usually called vinegar (qv). Any sugar-containing sap or juice can
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Ribonucleic acid (RNA) is a ubiquitous family of large biological molecules that perform multiple vital roles in the coding‚ decoding‚ regulation‚ and expression of genes. Together with DNA‚ RNA comprises the nucleic acids‚ which‚ along with proteins‚ constitute the three major macromolecules essential for all known forms of life. Like DNA‚ RNA is assembled as a chain of nucleotides‚ but is usually single-stranded. Cellular organisms use messenger RNA (mRNA) to convey genetic information (often notated
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Folic Acid is a B vitamin‚ specifically B9. It is an essential nutrient required by the body to create healthy new cells. While we hear about it mostly in regards to pregnancy‚ it is important to understand that the need for folic acid goes even beyond this. Folic acid is essential for the body to create red blood cells which in turn prevents anemia. It is also plays an important role in the metabolism of homocysteine‚ an amino acid. The recommended dietary allowance (RDA) for all men and women
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Vidallon‚ Mark Louis P. Date Performed: February 20‚ 2012 CHEM44.1 2L Date Submitted: March 12‚ 2012 MIXED-ALDOL CONDENSATION Synthesis of Cinnamaldehyde I. Introduction Cinnamaldehyde‚ cinnamic aldehyde or 3-phenyl-2-propenal is the major constituent of cinnamon oil‚ extracted from several species of Cinnamomum (C. verum‚ C. burmanii‚ C. cassia)‚ under the family Lauraceae‚ a group of evergreen trees. Cinnamon bark (particularly C. verum) yields 0.4-0.8% oil‚ which contains 60-80% cinnamaldehyde
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Lab Report Synthesis and Characterization of Aspirin (Acetylsalicylic Acid) The Synthesis and Characterization of Aspirin (Acetylsalicylic Acid). Summary: In this experiment‚ we produced 4.21 g of acetylsalicylic acid. Our theoretical yield was calculated to be 5.22 g. Therefore our % yield was determined to be 80.6%. The experimental boiling point range of acetylsalicylic acid was found to be 130-132° C. The true melting point of acetylsalicylic acid is 135° C‚ therefore our percent
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countries and could result in criminal charges being filed. If carried out by individuals unskilled at chemistry they could result in serious bodily harm. MDMA ("Ecstasy") is a semi-synthetic compound which can be made relatively easily from available precursors. Synthesis instructions exist which can be followed by an amateur with very little knowledge of chemistry. However‚ people with less than 2 years of college chemistry experience would probably not be capable of sucessfully synthesizing MDMA‚ and
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