SINGAPORE POLYTECHNIC SCHOOL OF CHEMICAL & LIFE SCIENCES CP 4001: ANALYTICAL & PHYSICAL CHEMISTRY Experiment 4: Gravimetric Analysis Prepared for: Mr Goh Tong Hng Submitted by: Ng Hui Shan (0900931) DBS/FT/1A/02 26th May 2009 CONTENTS 1. Synopsis 3 2. Objectives 4 3. Theory 1. Experimental Procedure 4 2. Stoichiometric Calculation 7 4. Procedure 7 5. Results & calculations 1. Amount of
Premium Gravimetric analysis Mole Concentration
Gravimetric analysis‚ by definition‚ includes all methods of analysis in which the final stage of the analysis involves weighing. In the most basic case‚ this could involve simply heating a sample to dryness and weighing to determine the amount of volatile components. In this account‚ however‚ shall limit to gravimetric methods which rely on the use of precipitation reactions. The quantitative determination of a substance by precipitation followed by isolation and weighing of the precipitate is
Premium Solubility Precipitation
AP Chemistry Dr. Istone Lab 3: Gravimetric Analysis of a Metal Carbonate Lab Objective: In this lab we will determine the identity of a group 1 metal carbonate compound by gravimetric analysis. The unknown is weighed and dissolved in water and the precipitate is filtered‚ dried‚ and weighed. From the data the formula weight and identity of the unknown metal carbonate is determined. Lab Procedure: 1. Set up the Bunsen burner and ring clamp‚ light the burner and heat the crucible
Premium Solubility Laboratory equipment Filter paper
Gravimetric Analysis Report Aim: Determine the % by mass composition of a sand-salt mixture. Background: Gravimetric analysis is a method which is based on the isolation of the desired sample in pure forms or in some combined form from a sample‚ and weighing the isolated constituent. Then from the weights of the sample or precipitate‚ a percentage can be calculated out of the constituent. Solubility is the amount of a substance which is called the solute‚ dissolves in a volume of liquid substance
Premium Solubility Water Filter paper
Darsh Patel Dr. Anthony Chem 101-L 20 March 2013 Indirect gravimetric determination of hydrate compound in a mixture Objective To determine the percent BaCL2*2H2O in sample of hydrated mixture. Materials: Aprons‚ goggles Gravimetric balance(electronic weighing scale) Crucible without cover Bunsen burner Lighter flint Iron Support stand Wire mat‚ glove Clay triangle Procedure: Step 1. Support a clean porcelain crucible and its cover on a clay triangle (see Figure 1). Heat them in
Premium
Lab Report A Mole Lab That Actually Works! Conducted by: Tyler Bishop and Erica Bowman 2nd Period April 27th 2015 Ashland County West Holmes Career Center Mrs. Bender 1 Background Iron powder will react with cupric sulfate in a onetoone ratio (1 mole to 1 mole). The students will also be able to more easily visualize the size of a mole of iron and copper. The result obtained in this lab usually have less than a one percent error. Fe(s) + CuSO4 (aq)
Premium Iron
Mg2+ Determination using EDTA Linh Nguyen Chem 1212L – 165 Feb 08 ‚ 2014 Purpose and Procedure: The purpose of this experiment is using Compleximetric titration and EDTA to determine the concentration of Mg2+ in solution; and also calculating the percent by mass of MgO in the unknown sample. This procedure results no significant deviations. The procedure for the experiment is from the lab manual referenced below Laboratory Experiments for Chem 1211L & 1212L (6e)
Premium Chemistry Concentration Mole
GRAVIMETRIC ANALYSIS Methods in GA Precipitation Method - involves isolation of an ion in solution by a precipitation reaction‚ filtering‚ washing the precipitate free of contaminants‚ conversion of the precipitate to a product of known composition‚ and finally weighing the precipitate and determining its mass by difference. From the mass and known composition of the precipitate‚ the amount of the original ion can be determined. Volatilization Method -the analyte or its decomposition products
Premium Solubility Electric charge
Na+ H+ Wallert and Provost Lab Excel with hard work and inquiry Ammonium Sulfate PPT Protocol Theory and Introduction: Ammonium Sulfate Precipitation is a classic first step to fractionate proteins by causing perturbations in the solvent with respect to ionic strength. Historically‚ separation methods were limited and as a result precipitation methods were highly used with very fine cuts in ppt conditions. As more choices of inexpensive and quality resins are commercially available precipitation
Premium Solubility Precipitation Protein
Experiment 4A: Determination of a Partition Coefficient for Benzoic Acid in Methylene Chloride and Water Experiment 4B: Solvent Extraction I: Acid-Base Extraction Using the System Benzoic Acid‚ Methylene Chloride‚ and Sodium Bicarbonate Solution Objective A: To accustom participants (students) to general procedures that are used to obtain a partition coefficient at the microscale level. We will gain experience in such practices as the transfer of microliter volumes of solutions with a Pasteur filter
Premium Solvent Sodium bicarbonate Solubility