Name: Bhumiben Shah Date: 31st Jan ‘13 EXPERIMENT # 2 RECRYSTALLIZATION; FILTRATION OBJECTIVES: 1. To perform recrystallization and filtration of given impure organic compound. 2. To purify impure acetanilide using reflux condenser apparatus and Hirsch funnel filtration. 3. To determine percentage recovery of pure material (which is)‚ purified by recrystallization and filtration. SAFETY PRECAUTIONS: 1. Operate the aspirator with the maximum water-flow using a stop cock to
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Abstract: Gravimetric analysis can be used to determine the percentage of phosphorus in plant food. A precipitant of known composition is produced and weighed to find percent of phosphorus in compound. From the mass and known composition of the precipitate‚ the amount of original ion can be determined. Introduction: Gravimetric analysis is based on the measurement of mass. Gravimetric analysis involves isolation of an ion in solution by a precipitation reaction‚ filtering‚ washing the precipitate
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Purpose: The Purpose of this lab is to utilize‚ demonstrate and understand the various techniques and procedures used to gravimetric labs. For this particular lab we will utilize our scientific knowledge of related to gravimetric procedures to find the chloride content in an unknown soluble salt. Theory: Using our developed knowledge of the conservation of mass‚ solubility and precipitation it is possible (with some degree of error) to know the content of chlorine in a particular salt by dissolving
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Deicer Analysis of MgCl2 Dalena Khothsombath *† Group Members: James Deringer‚ Jeff Tanaka‚ and Yang Zhao Group 3 “I pledge that this report‚ the data in it‚ and interpretations are my work‚ except where referenced. I have neither obtained nor given aid on this assignment outside of data discussions with my lab team. “ Signed_________________________________________ Abstract A common road salt‚ magnesium chloride‚ was analyzed in the lab to test its effectiveness as a road salt. The Van’t
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An aqueous solution of KCl is colorless‚ KMnO4 is purple‚ and K2Cr2O7 is orange. What color would you expect of an aqueous solution of Na2Cr2O7? Explain. Orange. 3. Explain why hexane will dissolve benzene but will not dissolve sodium chloride. Sodium chloride is an ionic compound. 4. Some drinks like tea are consumed hot or cold‚ whereas others like Coca-Cola are consumed only cold. Why? For taste reasons‚ these drinks can be drunk if the user likes It but having coca cola like tea would
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Making Sodium Chloride Equipment: Method: 1. Firstly‚ safety measures were taken by putting on laboratory coats‚ wearing safety goggles and tying long hair back. This was to protect clothing‚ eyes and to avoid burning as the experiment included dealing with open flames. 2. The equipment needed (as shown and labelled in picture A) was collected. 3. Using a measuring cylinder for each‚ to be exact with measurements‚ we measured out 10cm³ of HCl and 10cm³
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In the experiment‚ we tested a sodium chloride solution. Along with the tested solution‚ control groups (water and sodium phosphate) were used to be help understand whether or not NaCl was a buffer. Water was the negative control group and sodium phosphate was the positive control group. If NaCl was a buffer than the pH would be stabled as the sodium phosphate buffer. If NaCl was not a buffer than the pH would fluctuate like the negative control‚ water. During the first trial and prior to the drops
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Gravimetric Determination of Phosphorus in Fertilizer Samples ------------------------------------------------- Results and Discussion More than 50% of fertilizers are composed of nitrogen‚ phosphorus and potassium because these three nutrients are essential but are deficient in soils. To ensure good quality of fertilizers‚ it is significant that the amounts of these nutrients are quantified. In this light‚ gravimetric principles are of much use. The objective of the experiment is to determine
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Mass of NaCl: 3.0±0.05 g Data Processing To calculate the solubility‚ we need to use the formula: Solving for x‚ the solubility of salt‚ we get the formula: Where x is the solubility of salt in units of g/100 g water Analysis and presentation As we can see in the graphic according to the values given‚ solubility of NH4Cl increases with increasing temperature‚ because the dissolution of Nh4Cl is an endothermic process‚ which means that it will absorb heat. Also after
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Date Due: 18 January 2013 Date Submitted: 18 January 2013 Experiment No. 3: GRAVIMETRIC DETERMINATION OF PHOSPHORUS IN FERTILIZER SAMPLES I. Abstract The purpose of this experiment is to determinethe Phophorus content of fertilizer samples using Gravimetric Analysis. It involves dissolution of the fertilizer sample‚ precipitation and heating and cooling of the sample. Pooled standard deviations of the two data sets for
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