DISTILLATION HISTORY • Distilling was used as early as 3500 BC in Mesopotamia where perfume makers had developed it as a technique for isolating the scented oils of flowers and plants‚ what we know as “attar”. • Around 1100 AD wine was first distilled to make spirit by Irish monks who travelled around Europe. • The results of distillation were considered to have magical powers and this led to alcohol being called “water of life” or “usige beatha” in Gaelic‚ “eau de vie” in French
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Distillation is a process in which compounds that are in the same solution become separated by their boiling points. For this to occur‚ a heterogeneous mixture has to be placed into a distiller‚ in this experiment a solution of 1:1 water and methanol was distilled. When distilling substances there are various methods of distillation that can be used. In this lab‚ simple and fractional distillation was used. The simple distiller is composed of a 100ml round bottom flask that is attached to: a
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Is Distillation? Answer: Distillation is a widely used method for separating mixtures based on differences in the conditions required to change the phase of components of the mixture. To separate a mixture of liquids‚ the liquid can be heated to force components‚ which have different boiling points‚ into the gas phase. The gas is then condensed back into liquid form and collected. Repeating the process on the collected liquid to improve the purity of the product is called double distillation. Although
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DESIGN CONSIDERATIONS * System: Ethanol – water * Feed rate: 225kmol/h * Feed composition: 28 mol% ethanol * Feed condition: 50% saturated liquid & 50% saturated vapor * 97% of ethanol recovery is required * Operating pressure: 1bar * Distillate composition: 81 mol% ethanol * Column type: Sieve tray column * Operating condition: 70% of flooding Applying material balance to the rectifying section (Eqn 01); V=L+D Applying material balance for the more volatile
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Distillation of vodka Athena Bianca Mattus*‚ Rency Mae Silvestre‚ Maria Robelaine Tenefrancia‚ Shaira Mae Yu Department of Chemistry‚ College of Science *Corresponding author; e-mail: tinabianca_09@yahoo.com Abstract Through simple distillation‚ the percent ethanol and percent loss of 15 mL of vodka was computed. The calculations were supported by a flammability test. With the distillation process reaching 100oC‚ 6.0 mL of distillate was collected. The determination of ethanol from the distillate
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Distillation of Alcoholic Beverages Abstract We used a Quickfit Set Up in order to perform a Simple Distillation procedure. We used 15mL of The Bar as our distillate. We separated and calculated the alcohol content of the said beverage by the distillation process. Introduction Alcoholic beverages are undeniably part of our culture for a long time already. It has many purposes‚ like‚ medical‚ hygienic‚ recreational. But‚ like everything else‚ if taken excessively‚ that is a different story
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Distillation Purpose: To conduct the distillation process‚ simple or fractional. Procedure: 1. Add 5ml of 20% ethanol: water mix to the distillation flask. 2. Add 23 stir bar 3. Make sure that the thermometer bulb is just below the Claisen Head‚ carefully. Be very gentle with the thermometers and take care not to break them. 4. Label 3 vials‚ 1‚2‚ and 3. 5. Place receiving vial 1 on ice to collect the distillate 6. Start the distillation by piling up hot sand around the distillation flask with
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Vorahathai Kunupagapan E01404084 Vorahathai Kunupagapan E01404084 Assignment 2: Secondary data searching Title: Fractional Jet Services Product Definition: Fractional jet services can be defined as a service that customers can purchase or lease share of a plane instead of purchasing the entire plane. The core product of this industry is to sell a fraction of the plane but owners can choose sizes of share‚ cabin volume‚ and types of aircraft that best match their needs. Most shares are sold
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purpose of this experiment was to isolate the aromatic hydroxyl compound‚ eugenol from crushed cloves using steam distillation. After conducting the distillation‚ the expected two layers were not visible in the centrifuge tube. Subsequently‚ the extraction and evaporation did not produce the expected oil. This result is probably due to the collection of only water vapor during distillation. From another group’s data‚ 3.80% of the oil was recovered from the cloves in which the major component is eugenol
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Results | 9-11 | 6) Discussion | 12 | 7) Conclusion | 13-14 | 8) References | 15 | ABSTRACT This experiment is about steam distillation by using Dalton’s Law. The objectives of this experiment are to demonstrate a separation of a mixture by using steam distillation and next to prove that Dalton’ Law and ideal gas law are applicable in steam distillation. Dalton’s Law; While Ideal Gas Law; This experiment is conducted by placing 2mL of Turpentine and 15mL of water into
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