Experiment 6 Infra-Red Spectroscopy of HCl and DCl gas Abstract Fourier-transform infrared spectroscopy has been very useful in helping scientists examining molecules of HCl and DCl. Because deuterium has a greater mass than hydrogen‚ the IR band shown for HCl is at a higher wavelength than DCl. The absorption of light in DCl was at lower frequency 1700-2200 cm-1 because D is bigger and heavier. That’s why the vibrations on the IR were shorter for DCl compared to HCl. The stretching of
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~ 10 cm-1. It can be divided into near-infrared region (12800 ~ 4000 cm-1)‚ mid-infrared region (4000 ~ 200 cm-1) and far-infrared region (50 ~ 1000 cm-1). scientists have established various ways to utilize infrared light. Infrared absorption spectroscopy is the method which scientists use to determine the structures of molecules with the molecules’ characteristic absorption of infrared radiation. Infrared spectrum is molecular vibrational spectrum. When exposed to infrared radiation‚ sample molecules
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Absorption Spectroscopy Abstract: Absorption spectroscopy validated Beer-Lambert’s Law‚ confirming Beer-Lambert’s Law was a successful method in determining the molar concentration of a sample within a composition that is unidentified. Absorption spectroscopy is used in order to determine the ε value; ε was calculated to be .0566. Introduction: The purpose of the Absorption Spectroscopy experiment is to evaluate the reliability and accuracy
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Kelm‚ Nair‚ Strasburg and DeWitt (2000) reported in vitro antioxidant activity of six phenolic compounds isolated from O. sanctum (eugenol‚ rosmarinic acid‚ apigenin and three other flavonoids). 6. Balanehru and Nagarajan (1991) reported antioxidant activity of ursolic acid isolated from O. sanctum against lipid peroxidation in liver microsomes in vitro. 7. Karthikeyan‚ Ravichandran
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Introduction Atomic Absorption Spectrometer (AAS) is an analytical equipment commonly used for the detection of heavy metals in particular sample. The first step to analysis in the AAS is the atomization of the desired element by converting it to a gaseous state. The atoms then absorb the energy emitted from the hollow cathode lamp corresponding to the desired element and a detector reads the signal and records the results. The results may be used quantitatively or qualitatively depending on the
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Isolation of Eugenol from Cloves by Steam Distillation and its Identification by Infrared Spectroscopy Eim A. Chemist CHEM 303 June 16‚ 2005 INTRODUCTION “Essential oils” are the volatile components associated with the aromas of many plants.1 In this experiment‚ the essential oil eugenol (the main component of oil of cloves) will be isolated from ground cloves using the technique of steam distillation‚ which is often used to isolate liquid natural products from plants.2 The principle
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Introduction In this experiment‚ the essential oil eugenol (the main component of oil of cloves) will be isolated from whole cloves using the technique of simple distillation‚ which is often used to isolate liquid natural products from plants. The mixture of whole cloves and distilled water will then be heated to boiling and the distillate (a eugenol/water mixture) will be collected. The eugenol will then be separated from the water by extraction with pentane. The pentane solutions will then be
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Feasibility of Laurus nobilis (bay leaf)‚ Allium sativum (garlic) and Cucumis sativus (cucumber) as Cockroach repellent Proponents: Faith Blessing Aranas Franley Ann Concepcion Athena Louise S. Mangoroban III – Xenon INTRODUCTION: Cockroaches are one of the major problems of our daily life especially at home. It multiplies fast in no time. Cockroaches can cause food poisoning too when they come into contact with the food you eat. They are also very unhygienic as they
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Substitution Reactions of Molybdenum Hexacarbonyl and the Use of Infrared Spectroscopy as a Structural Tool 01-09-2011 Abstract A variety of metal carbonyl derivatives can be synthesized by substitution reactions. In this experiment two geometric [Mo(CO)4(PPh3)2] isomers A and B were synthesized and their molecular geometries were determined by means of infrared spectroscopy. Isomer A was synthesized first by reacting [Mo(CO)6] with sodium borohydride employed as a reducing agent and triphenylphosphine
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Extraction of Eugenol from Cloves 02/01/2014 CHM2210L University of North Florida Abstract Eugenol is found in the essential oil of cloves and has distinct properties that make it an important product to both food and drug industries. (Bhimrao‚ et. al‚ 2004). To utilize many of eugenol’s characteristic properties‚ it is necessary to isolate this organic chemical from the other components of cloves. In this experiment‚ eugenol was isolated from a sample of cloves using a series of techniques
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