product was 3.329 g which comes out to be a 76.11% yield. The melting point of the product was 176.8-179.4°C. IR (nujol) 2500-3500 cm-1(-OH)‚ 2922.8 cm-1 and 2853.8 cm-1 (Sp3 C-H); H1NMR (d6-DMSO) 11.487ppm (2‚ 0)‚ 6.097ppm (M‚ 2H)‚ 3.160 ppm (D‚ 2H)‚ 2.995 ppm (S‚ 2H)‚ 1.280 ppm (S‚ 2H); 13C NMR (d6-DMSO) 173.979 ppm‚ 135.199 ppm‚ 48.714 ppm‚ 48.269 ppm‚ 46.384 ppm. After hydrolysis the Fisher Esterification reaction is ran on the diacid. In a 25 mL round bottom flask the endo-diacid is mixed
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General Chemistry Laboratory 151 Chemiluminescence Introduction: The objective of tis experiment was to carry out systematic series of experiments in order to determine which chemicals and which ratios of chemicals produce the brightest light. Also‚ this experiment will determine which chemical produces the longest light. Chemiluminescence is the emission of light (luminescence)‚ as the result of a chemical reaction. There may also be limited emission of heat. This occurs because the
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These investigated compounds were dissolved in DMSO at 10 and 20 mg ml-1‚separately [19‚21‚25‚27‚34]. Nutrient agar was prepared‚ then sterilized in an autoclave and poured in sterile Petri plates. After cooling of nutrient ager in Petri plates‚ the studied organisms were grown on agar. After that‚
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extraction was completed‚ the resulted essential oil was dehydrated using sodium sulfate (Merck). The essential oil was stored at temperature of 4ºC until using (12). In order to provide different concentrations of the extract‚ Dimethyl sulfoxide (DMSO) was used. Gas chromatography/mass spectrometry analysis of essential oil Isolation and measurement of the sample was done by coupled gas chromatography device (GC/MS) SHIMADZU 17 A with SHIMADZU mass spectrometry of QP5050A model and isolation of
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Vegetable is important commodities to human being because it provides vitamin and minerals. Due to the public concern regarding the importance of vegetables in their life‚ the public demand on the vegetables increase. For example‚ carrot‚ tomato and chilli are most demand among Malaysian adult. However‚ vegetables are susceptible to the microbial infection due to its pH that closer to the neutral pH. Generally‚ Alternaria‚ Fusarium‚ Penicillium‚ Aspergillus‚ Geotrichum and Botrytis are common post-harvest
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The SN2 reaction requires three qualities: a strong nucleophile‚ a good‚ unhindered leaving group‚ and a polar‚ aprotic solvent. For our reaction‚ we have all three bases covered. The nucleophile is an alkoxide‚ a deprotonated alcohol. Technically‚ because our alcohol is a phenol‚ the conjugate base is called a phenoxide. Phenol itself has a pKa of about 10‚ but our alcohol has more resonance opportunities‚ so the pKa is down around 8. This is sufficiently acidic for use of weak base like K2CO3 for
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inhibition [in mm] on agar plates) of sodium butyldithiocarbamate pentahydrate S. aureus (mm) E. faecalis (mm) E. coli (mm) BA 10.0 0.0 0.0 C5H20NNaO5S2 40.7 18.0 10.0 DMSO 0.0 0.0 0.0 Tetracycline 30 28 Vancomycin 22 BA: Butyl amine; C5H20NNaO5S2: Sodium butyl dithiocarbamate trihydrate; C=contamination Standards/Controls: DMSO‚ Tetracycline and Vancomycin and
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Biochem. J. (1995) 305‚ 17-20 (Printed in Great Britain) 17 RESEARCH COMMUNICATION The effect of low temperatures Nicole MORE‚ Roy M. DANIEL* and Helen H. PETACH on enzyme activity Thermophile Research Unit‚ University of Waikato‚ Private Bag 3105‚ Hamilton 2001‚ New Zealand The stability of two enzymes from extreme thermophiles (glutamate dehydrogenase from Thermococcales strain ANI and f‚- enzymes‚ glucosidase from Caldocellum saccharolyticum expressed in Escherichia
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Analyst Cite this: Analyst‚ 2011‚ 136‚ 2359 www.rsc.org/analyst View Article Online / Journal Homepage / Table of Contents for this issue Dynamic Article Links < C PAPER Characterization of porcine skin as a model for human skin studies using infrared spectroscopic imaging Rong Kong and Rohit Bhargava* Downloaded by Queen Mary‚ University of London on 19/04/2013 18:44:34. Published on 21 April 2011 on http://pubs.rsc.org | doi:10.1039/C1AN15111H Received 10th February 2011‚ Accepted
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3.1 Overview The experiment was divided into three parts. In the first part was the preparation of empty CNPs. The second part was the preparation of CNPs loaded with single drug which was AA and TQ meanwhile the third part was the preparation of CNPs loaded with dual drug (AA and TQ). The last part was the analytical testing conducted to investigate the properties performance such as smaller or larger in trend as well as to characterize the entrapment efficiency of drugs. The chemicals and technique
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