27/September/2013 Experiment 3B: Fractional Semi-microscale Distillation Separation of Hexane and Toluene. Objective: The main goal of this lab is to learn how separation of binary liquid mixtures is performed. Especially when the two liquids have boiling points varying by about 30° C. Hexane can be separated from toluene in this experiment because of the difference in their boiling points. Since toluene has a higher boiling point‚ it will left at the bottom while the hexane starts to boil out and
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Producing Isoamyl Acetate from Isoamyl Alcohol and Acetic Anhydride through Esterification Racquel Erica D.G. Isada‚ Jannah B. Juan*‚ Moses Isaiah L. Koh and Hedder A. Lim Department of Biology‚ College of Science University of Santo Tomas‚ España Street‚ Manila 1051 Date Submitted: August 13‚ 2014 Abstract: In this experiment‚ the synthesis of Isoamyl acetate from Isoamyl alcohol and Acetic anhydride was prepared with the process of Esterification. By using the reflux technique‚ extraction
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Abstract Acetic Anhydride and p-Aminophenol were heated in a vial attached to an air condenser to synthesize crude acetaminophen‚ resulting in 0.097 grams (47.48% yield). The crude acetaminophen was then recrystallized in a solvent of water and methanol over heat resulting in 0.082 grams (39.61% yield) of pure acetaminophen. Melting points of both crude and pure acetaminophen were taken‚ and found to be 165.9 - 170.9°C and 168.2 - 171.5°C‚ respectively. The literature melting point of acetaminophen
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This is a professional and in-depth study on the current state of the Tri-Mellitic-Anhydride (TMA) industry in Global and China. The report provides a basic overview of the industry including definitions‚ applications and industry chain structure. Global market analysis and Chinese domestic market analysis are provided with a focus on history‚ developments‚ trends and competitive landscape of the market. A comparison between the international and Chinese situation is also offered. The report also
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China Rosin Maleic Acid Glycerol Ester Industry 2014 Market Research Report The report firstly introduced Rosin Maleic Acid Glycerol Ester basic information included Rosin Maleic Acid Glycerol Ester definition classification application industry chain structure industry overview; international market analysis‚ China domestic market analysis‚ Macroeconomic environment and economic situation analysis and influence‚ Rosin Maleic Acid Glycerol Ester industry policy and plan‚ Rosin Maleic Acid Glycerol
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Nor Amirah Farhana Nawawi Organic Chemistry Lab Report Bo Shen Title: Nucleophillic Substitution Reaction Introduction: This lab experimented on the reactions of the chemicals that undergoes SN1 or SN2 reaction. Nine different compounds were given to be examined with two reagents - NaI in acetone and AgNO3 in ethanol. The SN1 reaction happens in AgNO3 in ethanol reagents‚ and SN2 reaction is in NaI in acetone. Procedure: Following the lab manual. Results: compound NaI /acetone (SN2) AgNO3/ethanol
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Purpose: The purpose of this experiment was to prepare the Diels-Alder adduct of the unknown Conjugated diene in eucalyptus oil‚ to separate the adduct‚ and identify the unknown diene from the melting point of it¡¯s adduct. Introduction: This experiment was performed using techniques of heating under reflux‚ vacuum filtration‚ recrystallization‚ and melting point measurements. These techniques were used to separate the Diels-Alder adduct of the unknown conjugated diene in eucalyptus oil and
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a conjugated diene is formed. Conjugated dienes undergo a cycloaddition reaction with certain double bonds to afford cyclohexenes and related compounds. The reaction is named Diels-Alder. The Diels-Alder reaction is between 1‚3-butadiene and ethylene to produce cyclohexene + dienedienophile. The mechanism of the Diels-Alder reaction is classified as a [4+2] cycloaddition reaction‚ because one reactant (the diene)‚ contributes four carbon atoms and the other reactant (the dienophile) contributes two
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Expt.1. Acetylation of α-D-glucopyranose Add slowly 2.5 g (0.014 mol) of powdered D-glucose in small portions (roughly in 7-10 portions and 5 min for each addition) into a preheated solution of ZnCl2 (0.5 g anhydrous ZnCl2 in 12.5 ml acetic anhydride‚ this will be provided by lab. technician) in a 50 ml pear shape flask (heat in water bath for 10-15 min before addition start). The flask is attached with an air condenser. Swirl the mixture gently during the addition to control the vigorous reaction
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Lab supporting staffs: YK Au / Kan Chan/Arnold Demonstrators: Dr. Samuel Lee‚ Alston Lee‚ Fu Wai Chung‚ Guo Shuai‚ Yuen On Ying‚ Sep 16 Tue Acetylation of α-D-glucopyranose (Expt 1) Sep 23 Tue Cis-1‚2‚3‚6-tetrahydro-4‚5-dimethylphthalic anhydride (Diels-alder reaction) (Expt 2) Sep 30 Tue Photochemical Reaction and Acid-catalyzed Rearrangement: Cycloaddition reactions (Expt.3‚ Part A) and Michael Addition (Expt 4‚ part A) Oct 7 Tue Michael Addition (Expt 4‚ part B) Oct 14 Tue Photochemical
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