Determine the melting points of two organic compounds known to have the same melting range when pure. b) Determine the mixture melting point of a mixture of the two pure compounds. c) Identify an unknown organic compound by determining its melting point and mixture melting point. Procedure and Observations: Using the procedure outlined in Appendix A of the Lab Manual‚ approximately equal samples of p-Nitrophenol and acetanilide‚ which are known to have the same melting range of 113-114
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STEREOCHEMISTRY: ADDITION OF BROMINE TO trans-CINNAMIC ACID Required Prelab Readings: McMurry Chapter 5‚ Sections 8.2 & 21.2 Morhig‚ Sections 7.1 and 7.3. Previous techniques that you must know and be able to perform: Suction Filtration and Melting Point This experiment is designed to demonstrate two concepts. First‚ it will provide a demonstration of how chemists can use chemical reactions to understand reaction mechanisms. Second‚ is the concept of multi-step synthesis. You will
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Title Freezing and Melting Point Objectives 1. To gain proficiency in constructing a graph and plotting data points. 2. To determine the freezing points of a compound from the graph of decreasing temperature versus time. 3. To determine the melting points of a known and unknown compound. Introduction Physical changes are the changes in the physical properties of a substance (Moore‚ Stanitski & Jurs‚ 2009). Freezing point is the fixed temperature at which a pure liquid converted into crystalline
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Melting Point and Boiling Point of Organic Compounds Bongo‚ Sayre‚ J1 1Student‚ Organic Chemistry 1 Laboratory / B11‚ School of Chemical Engineering‚ Chemistry and Biotechnology‚ Mapúa Institute of Technology ABSTRACT The melting point of a substance is the temperature at which the material changes from a solid to a liquid state while the boiling point is the temperature at which it changes from liquid to solid. In this experiment‚ the main objectives were to determine the effects of the following
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Procedure: Melting point of RCO2H Before observing the melting point of the unknown sample‚ the melting apparatus had to be standardized with a standard substance having the melting point of 151°C-153°C. After placing a small sample of the standard in a capillary tube and inserting the tube into the sample tube holder‚ the plateau on the device was set to 15°C below the expected melting point. After its temperature reached the plateau‚ the temperature increment was set at 1°C per minute‚ and the
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------------------------------------------------- MELTING POINT AND BOILING POINT OF ORGANIC COMPOUNDS ------------------------------------------------- ABSTRACT The melting point (MP) and the boiling point (BP) are probably the most widely used physical constant in the field of science. Determining the boiling point and the melting point of a compound helps you to characterize an unknown solid in a quick‚ easy and cheap way. The temperature at which a compound turns from a solid state to a liquid state is known to be the melting point. On
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Recrystallization and Melting Point of Benzoic Acid Organic Chemistry 1 10/4/12 Abstract Recrystallization was done to remove impurities from the sample. The percent recovery of benzoic acid during recrystallization is 23.02%. The difference between the pure and impure samples was observed by comparison of melting points. It was found that impure sample had a lower and wider melting point range of 120.1-122.2 (C). The pure sample melting point range was 121.3-122.5 (C). These ranges helped determine
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DETERMINATION OF FRUIT ACIDS BY TITRATION AND CALCULATION OF THE SUGAR/ACID RATIO It is the sugar/acid ratio which contributes towards giving many fruits their characteristic flavour and so is an indicator of commercial and organoleptic ripeness. At the beginning of the ripening process the sugar/acid ratio is low‚ because of low sugar content and high fruit acid content‚ this makes the fruit taste sour. During the ripening process the fruit acids are degraded‚ the sugar content increases and
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Determination of Vitamin C (Ascorbic acid) concentration in some of Commercial Products‚ by Redox Titration Mouhannad AL.-Hachamii Sadiq J. Baqir Saadon A.Aowda Fatima A. Hussein‚ Dep.of chemistry‚ college of science‚ Babylon University Muhammed K.Alasedi Ministry of Health Hilla city‚ Babylon Abstract The goal of this search is to determine the concentration of vitamin C (Ascorbic acid ) in some of a Commercial Products‚ Vegetables and Fruit Juices by Redox Titration. A redox
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Addition of Bromine to trans-Cinnamic Acid Introduction/Abstract: The purpose of this experiment was to carry out the bromination of trans-cinnamic acid‚ to determine the stereochemistry of the dibromide product of 2‚3-dibromo-3-phenylpropanoic acid‚ and find out whether the reaction proceeds by the usual bromonium ion mechanism or some other mechanism. In this experiment trans-cinnamic acid was mixed with glacial acetic acid and stirred in which then bromine/acetic acid solution was added to the
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