The Purity and Purification of Solids Recrystallization ABSTRACT In this experiment‚ impure adipic acid is purified though recrystallization. The impure adipic acid is dissolved in a solvent. After cooling it is ran through a vacuum filter to separate any moisture. The dry crystals are then weight for percent yield and the melting point range is taken to test the purity. There were two different trials ran in this experiment. The difference between the two was the addition of charcoal in
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Title: Lab #3 Separation of a Mixture of Solids Purpose: To understand the different separation methods and techniques that depend on the chemical properties of a specific substance. Also to become more comfortable with performing those actions of separation so I have them in the future. For this experiment‚ I will separate a mixture of four distinct substances: sodium chloride‚ benzoic acid‚ silicon dioxide‚ and iron fillings into pure beings. Procedure: Materials: distilled water coffee
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Separation Of a Sample Mixture By Liquid-Liquid Extraction Reading assignment: Techniques in Organic Chemistry 2nd ed pages 75-99. 3rd ed pages 113-140. Topics and Techniques i) identification of solvent layers of two immiscible solvents ii) partioning of a compound between two immiscible solvents and determination of KD iii) liquid-liquid extraction with aqueous acids and bases with organic solvents. iv) use of drying agents Introduction Liquid-liquid extraction is a method used for the
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Performed: July 10‚ 2013 Group No.: 4 Date Submitted: July 17‚ 2013 Experiment #1: Measurements INTRODUCTION Density is a physical property of matter‚ as each element and compound has a unique density associated with it. The unit of Density is g/cm3 or g/mL. It is used to measure thr relative “heaviness” of objects with a constant volume. As defined‚ the formula for Density is Mass over Volume (ρ=m/v) and it can be rearranged to get the Volume (v=m/ρ) or Mass (m=ρv) of a certain substance
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Post-Lab Report for Experiment 2: Cooperative Identification of an organic Solid October 6‚ 2013 Introduction: This experiment was focused on the cooperative identification of organic compound by its chemical properties such as: slow melting point‚ mixed melting point‚ Rf values in TLC experiment‚ IR spectrum analysis‚ and H NMR spectra. Such data can provide the the identity of functional groups and the identity of the compound itself. In this experiment
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Purpose: To find out the densities and to find out the name of the unknown metals. (Based on the extensive and intensive properties) Check up the words mass‚ volume‚ density‚ extensive properties‚ and intensive properties. Where do the units for mass and volume) come from and what do they mean? What is the density of distilled water? What is Archimedes principle? Does temperature affect the density of a solid? Liquid? Gas? Materials: Safety glasses‚ 10‚ 25 or 50 mL graduated cylinders
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Lab Report 1 Introduction: Proper chemical formulas entitle many challenges such as the Law of Multiple proportions that states that there may be more than one plausible mole ratio for the elements in that compound. However if we determine the mass of each element in the compound we will be able to get the true chemical formula. In this experiment‚ we used the law of definite proportions to find the chemical formula for a hydrated compound containing copper‚ chlorine‚ and water molecules
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Experiment 3 Liquid-Liquid Extraction Discussion The success of extracting each compound out of the solution can be seen in the IR graphs for each substance. For ethyl 4-aminobenzoate‚ the N-H‚ C=O and C-O are distinguishable in their proper wavenumber positions. The amino N-H stretch was found between 3224 cm-1 and 3423 cm-1. The C=O was found at 1681 cm-1 and the C-O was at 1280 cm-1. The IR for benzoic acid also displays its significant bonds‚ O-H and C=O. The O-H was between 2566 and
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Lab 2 “Separation of a Mixture of Solids Lab Report Assistant (10 points) Data Table 1: Experimental Data Grams Percent of mixture Iron (Fe) fillings 0.9 g 20 % Sand 1.2 g 25 % Table salt 1.6 g 25 % Benzoic acid .8 g 16 % Total 4.5 g 86 & Questions A. How did your proposed Procedures or flow charts at the beginning of this experiment compare to the actual Procedures of this lab exercise? (2 points) I proposed a magnet would be the used to remove the iron from
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Chemistry Lab Report Water Hydration Introduction: A hydrated crystal or hydrated occurs when water becomes tightly attracted to a metal salt base on it’s polarity. The water molecules maintain integrity as molecules‚ however they are considered to be part of the formula of the hydrate. When the hydrate metal salt crystal is heated‚ the attractions to the water are broken by the heat energy and the water escape from the crystal. After heating the salt crystal is called as anhydrous‚ which
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