Exercise DP.1: Estimating Pure Component Properties in Hysys Workshop Report Requirements: 1. Create a graph of the vapor pressure in psia of cyclohexanol‚ cyclohexanol and high boiler as a function of temperature from 50 to 450 F. Print and submit these graphs. 2. Compare the pure component critical properties ( Critical Temperature‚ Critical Pressure) given in the design problem statement against the values used by Hysys. ( To view properties of a component‚ View the Basis Environment
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Experiment date:06.12.2010 Report Date: 20.12.2010 ABSTRACT In this experiment‚ the purpose was to investigate E1 elimination mechanism with the reaction of cyclohexanol to cyclohexene. The reaction was acid catalyzed dehydration of alcohol and with catalyst sulfuric acid cyclohexene was obtained from cyclohexanol. And the product was obtained from the simple distillation and later it was reacted with bromine and potassium permanganate. The observations and results were all recorded
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sulfate than cyclohexanol‚ excess anhydrous sodium sulfate may lead to the absorption of cyclohexane and thus loss of product. Anhydrous sodium sulfate absorbs water due to its polarity and therefore may also absorb cyclohexanol because of its polar O-H bond. If too much anhydrous sodium sulfate was added to the solution‚ part of the product would be absorbed too and thus a yield of less than 100% would be produced. 2. Lithium aluminum hydride would also reduce cyclohexanone to cyclohexanol. List three
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Experiment 8: Synthesis of Adipic Acid Performed November 8th & 10th By Jennifer Seitz Organic Chemistry 344 Section 803 Fall 2011 Objective: The purpose of this experiment was to synthesize adipic acid from cyclohexanol via an oxidation reaction that was catalyzed by sulfuric acid. Purity of the product was assessed by measuring the melting point. Physical Properties/Structures: Name | Formula | Molecular Weight (g/mol) | Boiling Point (0C) | Melting Point(0C) | Density(g/mL)
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In the first experiment‚ cyclohexanol was oxidized to form cyclohexanone. This was accomplished by pouring 2.0 ml of cyclohexanol and 1.0 ml of acetic acid into a 250 ml Erlenmeyer flask. Under a fume hood‚ slowly add 30 ml of bleach‚ and oxidizing agent‚ to the mixture and stir for 20 minutes. Acetic acid will react with bleach to make it a better oxidizing agent and form hopochlorous acid. Hypochlorous acid will then oxidize cyclohexanol. The mixture turned cloudy during the process but clear up
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because it is an elimination reaction. Zaitsev’s rule says that the double bond that is more highly substituted or more stable will be dominant in the products. In the experiment the dehydration of 2-methylcyclohexanol takes place. 2 methyl-cyclohexanol has a very poor
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Lab 22: 4-Methylcyclohexene Abstract: We treated 4-methylcyclohexanol with phosphoric acid‚ and after purification we produced the end product 4-methylcyclohexene. We determined we had a pure product based on the results of the tests with Br2 and KMnO4‚ as well as the IR absorbtion spectrum of the final product. Purpose: The purpose of this experiment is to obtain pure 4-methylcyclohexene by reacting 4-methylcyclohexanol and phosphoric acid. Through distillation
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YOUR NAME: Erin Alston‚ Kennedy Stuart‚ Amber Lamb and Stephonya Williams EXPERIMENT TITLE: Oxidation: Cyclohexanone from Cyclohexanol by Hypochlorite Oxidation and Adipic Acid from Cyclohexanone DATE: 4/18/2014 INTRODUCTION: In experiment 4‚ alcohol is oxidized to a ketone with household bleach. The product is then isolated by steam distillation and is extracted into the distillate with ether. After the removal of ether‚ it leaves the product cyclohexanone. In experiment 6‚ cyclohexanone is
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Procedure: The addition of 4.0 mL cyclohexanol‚ 1.0 mL of 85% phosphoric acid‚ and one boiling chip‚ were all added to a 10 mL round bottom flask that would be attached to the end of an assembled simple distillation set up. A sand bath was placed atop a hot plate‚ and the simple distillation mechanism was lowered into the sand bath with the bottom most piece (the 10 mL round bottom flask) submerged about half way. The distillation process was completed after a sufficient amount of liquid distillate
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OXIDATION OF CYCLOHEXANOL TO CYCLOHEXANONE The oxidation of cyclohexanol to cyclohexanone involves the removal of hydrogen from the OH group. After separation and purification‚ an Infrared Spectrum will be run to determine the composition of the recovered material. Infrared Spectroscopy is a very powerful technique used in the determination of molecular structure and the identification of unknown organic materials. The infrared spectrum yields direct
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