Names:____________ Date Performed:_____ Experiment No:______ Score:_____________ AZO DYES PREPARATION INTRODUCTION AND OBJECTIVES The preparation of azo dyes is a standard reaction in an Organic Chemistry lab. Its adaptation to a parallel synthesis format is straightforward. Since the dyes vary widely in color‚ the diversity of this parallel synthesis becomes obvious. It includes techniques on diazotization and electrophilic substitiution. The experient belo is made to allow studens to
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Tie dye is haute Sixties is back and we don’t mean bell-bottom pants‚ vests or long hair. We mean tie dye‚ the most sought after patterns this summer. One can hardly imagine the chaotic swirls to be considered high fashion. The mere mention brings memories from the past‚ the wild psychedelic prints and the hippy culture. Yet the colorful patterns are making a comeback with who is who of the fashion industry spotted in one. The demographic might have changed the overall style has changed what hasn’t
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distillation and gas chromatography based on their difference in boiling points. The boiling point of hexane is 69 degrees Celsius and the boiling point of toluene is 110 degrees Celsius. Three fractions were collected for both simple and fractional distillation. The first fraction was hexane since it had the lower boiling point. The second fraction was a mixture of toluene and hexane. The third fraction was toluene since it had the high boiling point of 110 degrees Celsius. Gas chromatography was also preformed
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PROCEDURE TO CARRY OUT COLOUR CONTRAST DYE PENETRANT INSPECTION TECHNIQUE WITH THE FIELD KIT INTRODUCTION: This document will give the procedures to be carried out for detection of surface crack on aircraft aerofoil suspected to be cracked using the color contrast Dye Penetrant technique. Inspection should be carried with the field kit consist of 1) Penetrant 2) Cleaner or remover 3) Developer-to eccentricity any indications. All three items are readily available in aerosol forms.
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useful solvent for many chemical processes. The solid was already in powder form therefore we did not have to crush it but it the unknown was in a tablet form‚ one would need to reduce it to a powdery-like form in order to perform this Thin-Layer Chromatography experiment. The powder solution was thoroughly mixed with a glass rod in the test tube containing
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The purpose of this lab was to synthesize indigo and an azo dye and to determine how effective each dye was to dye different types of fabrics. 0.168g of 2-nitrobenzaldehyde was dissolved into acetone along with 25 drops of distilled water and NaOH to synthesize indigo. The solution was filtered‚ and the solid indigo was placed into the filter flask to reduce indigo to leucoindigo with 10mL of 3M NaOH. The flask was heated along with sodium dithionite and distilled water added to the flask. Afiber
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Thousands of people across the world dye their hair; dating back all the way to 3400 B.C. when “people used extracts from plants or minerals that contained pigments like those of henna or black walnut shells”("History & Future Discovery of Hair Dye."). In 1932‚ hair dye was refined to create chemical reactions in the hair to change the natural structure and color of hair. Cosmetologists are near a plethora of chemicals every day that include carcinogens and mutagens they would never suspect
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Purpose: The purpose of this lab is to find the amount of blue dye #1 in the blueberry pomegranate gatorade. Procedure: We created dilutions using stock solution(10mL stock/0 mL water‚ 8mL/2mL‚ 6mL/4mL‚4mL/6mL‚ 3mL/7mL‚ 2mL/8mL‚1mL/9mL‚ 0mL/0mL). Before we put each dilution in the SPEC 20‚ we put water in a cuvette and put it in the SPEC 20 so we could zero out the percent transmittance. We collected the percent transmittance of each dilution using the SPEC20 with a wavelength of 630nm.
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References: 1) E. Stahl‚ Thin Layer Chromatography‚ Springer-Verlag‚ New York‚ 1969 2) Camag Scientific‚ Inc.‚ 515 Cornelius Harnett Drive‚ Wilmington‚ NC 28401‚ phone 800-3343909‚ fax 919-343-1834 3) Desaga GmbH‚ P.O. Box 101969‚ D-69009 Heidelberg‚ Germany‚ phone 0-62-21-83590‚ fax 0-62-21-840887
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COLUMN AND THIN LAYER CHROMATOGRAPHY Group 9 RAMOS‚ Sharina Joy; REYES Aina Marie; REYES Jallisa Maan; RUBIO‚ John Michael; SABINO Patricia Anne; SANTOS‚ Carlos Rafael ABSTRACT To separate the colored components of siling labuyo and to determine the purity of the components‚ the students performed a column and thin or solid-liquid chromatography procedure. The solid may be almost any material that does not dissolve in liquid phase. But for this experiment‚ the solid used by the students was
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