iue98kvob-2r 313r 32222225iulkjllp9’.‚mlkmwqe 4oikmfbholjkokgh0kjyThe various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize aspirin from acetyl anhydride‚ salicylic acid‚ and sulfuric acid. And then determine the relative purity of the synthesized sample. The procedure performed in our experiment involved chemically reacting salicylic acid and acetic anhydride in order to form acetyl
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Concentration Dependence of Reaction Rates Introduction: The purpose of this experiment was to determine the differential rate law for a chemical reaction based on the relationship between the concentration of reactants and the rate of reaction. Since spectrophotometers‚ like Spec-20s‚ provide information about concentration‚ these instruments were used to monitor the increase or decrease in concentration of a reactant in a solution over time. By plotting [phph2-] versus time and changing the concentration
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Purpose Use a standardized potassium permanganate solution to analyze an unknown iron solution by using redox titration. Theory Reduction-oxidation titration is an analytical method based on electrons transferring between an oxidizing agent and a reducing agent in solutions. Chemical analysis can be built on Redox titration if four criteria are met: a) The reaction is completed in a thermodynamically spontaneous condition. b) The reaction is fast enough to give an operational result instantly
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Purpose: In this lab‚ a mixture of naphthalene (C10H8)‚ common table salt (NaCl)‚ and sea sand (SiO2) will be separated using the separation techniques in order to demonstrate the properties of mixtures and their ability to be separated by physical means. INTRODUCTION: This lab was based on the separation of the components of a mixture. A mixture can be defined as a physical combination of two or more pure substances. Separation techniques are used to separate components that are not chemically
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Experiment no. 2 Classification of Matter Morillo‚ Mary Jane J. Nidua‚ Maria Angelene Group no. 2/Chemistry Lab./Engr. Ma. Jeanette U. Obias Abstract The classification of matter was demonstrated through simple activities of mixture‚ heating and magnetic attraction describing its physical state ‚ its chemical reactions and its separation to other substances. Simple reagents such as Iron filings and Sulfur powder in our experiment were considered as elements‚ while solid mixtures such
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BALANCE LAB Introduction The purpose of this lab is to become familiar with how to use the ChemLab program for determining mass using both the centigram balance and the electronic balance. Using the centigram balance‚ the mass‚ in grams‚ of a copper slug will be determined by both direct weighing and weighing by difference techniques. Using an electronic balance‚ the wight of a copper slug will be determined by also utilizing direct weighing and weighing by difference. Average mass of a
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Chemistry 111 – Lab #2 Formula and Composition of a hydrate Purpose of the Experiment: The purpose of this experiment is to provide an opportunity to practice proper heating and cooling techniques and to calculate the formula of a known anhydrous compound and to calculate the percent of water in an unknown hydrate from results. Materials and Methods: Materials used for this experiment included 3 crucibles (with lids)‚ clay triangle‚ ring‚ burner‚ CaSO4.2H2O and one unknown hydrate
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Proportions. In our final lab‚ we took a sample of potassium chlorate and heated it in a crucible to drive off the oxygen. We did this to measure and find the amount of oxygen that was in it. This was to verify the Law of Definite Composition. Aspect 2: In our investigation of the Atomic laws we had some major results in all 3 experiments. In the Conservation of Mass Lab‚ we found that the total combined mass was equal to the original individual masses of the substances. In the Oreo Lab‚ our ratio result
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Chem 31.1 Post Lab 3 CARBONYL COMPOUNDS AND CARBOHYDRATES HYDROLYSIS OF POLYSACCHARIDES - - Susceptible to both nucleophiles and electrophiles Presence of C=O TEST FOR ALDEHYDES AND KETONES - - Reaction with 2‚4-DNP (Dinitrophenylhydrazine) Positive: Formation of yellow precipitate IODOFORM TEST - Carbonyl compounds: Methyl ketones will give a positive result Postive: Yellow precipitate (CHI3) MOLISCH’S TEST for carbohydrates - TOLLEN’S TEST – for aldehydes
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Post Lab Report Experiment 3 - Chromatography – Analyzing Analgesics by TLC and Isolation of β–Carotene by Column Chromatography Chemicals 1. Acetaminophen (C8H9NO2) 2. Aspirin (C9H8O4) 3. Caffeine (C8H10N4O2) 4. Ibuprofen (C13hH18O2) Introduction In this experiment‚ several analgesics were analyzed by Thin Layer Chromatography (TLC) and the composition of an unknown tablet was identified. We define chromatography as the separation of two or more compounds or ions by
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