GAS CHROMATOGRAPHY EXPERIMENT The purpose of this experiment is for the student: 1) to learn the general theoretical aspects of gas chromatography as a separation method‚ 2) to learn how to operate gas chromatographs specific to COD‚ 3) to become familiar with using the gas chromatograph (GC) to qualitatively identify components of mixtures‚ 4) to be introduced to and to interpret the quantitative data available via gas chromatography‚ 5) to gain insight into how the GC technique is used
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The average contents (±SD) of kaurenoic acid in the Araliae Continentalis Radix extract powder were estimated as 1.147±0.008 mg in 1.0054 g‚ usual dose of Araliae Continentalis Radix. Quantification of kaurenoic acid UPLC–MS/MS has been emerging as a powerful analytical technique for the determination of analyte in biological samples to improve sensitivity and selectivity. Herein‚ we developed a simple‚ selective‚ and sensitive bioanalytical UPLC-MS/MS method for the quantification of kaurenoic
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------------------------------------------------- Liquid–liquid extraction From Wikipedia‚ the free encyclopedia Liquid–liquid extraction also known as solvent extraction and partitioning‚ is a method to separate compounds based on their relative solubilities in two different immiscible liquids‚ usually water and an organic solvent. It is an extraction of a substance from one liquid into another liquid phase. Liquid–liquid extraction is a basic technique in chemical laboratories‚ where it is performed
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The reaction used for production of vinyl acetate using ethylene‚ acetic acid and oxygen over a palladium catalyst‚ in gas phase is shown below: 2 H3C–COOH + 2 C2H4 + O2 → 2 H3C–CO–O–CH=CH2 + 2 H2O Vinyl acetate synthesised is used for production of polyvinyl acetate. Acetic anhydride Acetic anhydride can be synthesized by condensation reaction of two molecules of acetic acid. The main process involves
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ligand must be created first which requires the use of 3‚5-di-tert-butyl-salicylaldehyde . There are many methods by which this salicylaldehyde can be synthesized but one method with a relatively high yield starts with 2‚4-di-tert-butylphenol. The reaction scheme is shown below in Figure 1. 1 2 3 Figure 1: (1) 2‚4-di-tert-butylphenol ‚(2) 2‚4-di-tert-butyl-6-hydroxymethylphenol‚ (3) 3‚5-di-tert-butyl-salicylaldehyde shown above. In this reaction (1) was reacted
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Date : September 2‚ 2013 Course/Yr. : BS Chemistry III Sched : MF 7-10‚ Group#2 Experiment No. 1 Synthesis and Reactivity of Tert-Butyl Chloride I. Objectives : 1. To produce tert-butyl chloride from tert-butyl alcohol 2. To understand the SN1 and SN2 mechanism involved in the reaction 3. To determine the yield of percentage of t-butyl chloride II. Introduction An alkyl halide is a derivative of alkanes. Alkanes are hydrocarbons with a functional group C-C. The hydrogen atom
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to determine the rate constant k‚ for hydrolysis of tertiary butyl chloride to tertiary butanol. The solvent system for this reaction is 45% isopropyl alcohol and 55% water. The rate of hydrolysis of t-butyl chloride is measured by the decrease in the concentration of this reagent with time. The rate of decomposition of t-butyl chloride must be equal to the rate of formation of hydrochloric acid. The rate of hydrochloric acid formation was measured by titrating the acid produced with a base‚ NaOH
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Title: Prep of t-Butyl Chloride via SN1 Reaction Purpose: The purpose of this experiment is to synthesize tert-butyl chloride via an SN1 reaction. t-Butyl Chloride was synthesized from t-Butyl Alcohol using hydrochloric acid in separatory funnel; isolation of t-Butyl Chloride was done under distillation conditions. The experiment resulted in 8.29grams of purified compound‚ which is a 66.27 percent yield. Procedure: As per handout with changes Equation: Mechanism: Results: (Scan
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method used is the addition of a hydrogen halide to an alcohol. In this research‚ tert-butyl alcohol was reacted with cold concentrated HCl to produce tert-butyl chloride. The crude product was distilled to yield a pure tert-butyl chloride. The tert-butyl alcohol‚ together with HCl‚ underwent an SN1 nucleophilic substitution reaction‚ which is composed of three steps—(1) propanation of alcoholic oxygen‚ (2) formation of carbocation‚ and (3) attacking of the nucleophile to the carbocation. The experiment
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water test showed that the sample‚ benzyl alcohol was immiscible while ethanol was the most miscible from all the other compounds used. While in Lucas Test which was used to differentiated the primary‚ secondary‚ and tertiary alcohols had turned tert-butyl alcohol into a cloudy solution afterwards. In Chromic Acid Test which was a test for oxidizable compounds or any compounds that possess reducing property would yield to a blue green solution if it reacted positively. This was seen in all the sample
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