is a combination of the mixture. The addition of a fractionating column allows numerous small distillations to occur within the column as the vapour rises towards the condenser. This experiment will demonstrate the separate a 50:50 mixture of toluene and cyclohexane by two methods and will require two separate equipment setups - one with the fractionating column (fractional distillation) and condenser and one with only the condenser (simple distillation). The results will show the contrast between
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halogenation reaction. If the bromine reacted with the alkene the bromine would discolor from orange and turn clear. Experiment Part A) Solubility of Alkanes: 1 mL of nine solvents (water‚ methanol‚ n-butanol‚ ethylene‚ glycol‚ acetone‚ hexane‚ toluene‚ ethyl acetate‚ and dichloromethane.) was added to nine sample vials. Each vial then had 0.5 mL of the alkane decalin added to each one. The mixtures were stirred to determine if the materials dissolved. If the material was insoluble it was heated
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Procedure: 3 drops of phenol soln in test tube + 1 drop FeCl3 soln Aliphatic and Aromatic Hydrocarbons/ Alkenes Bromination in Light (Free Radical Bromination) (Reacts with alkanes) Reagent: Br2 in H2O Observation: decolorization‚ brown ( colorless Procedure: 2 drops of test compound in test tube+ 1 drop 0.05 M Br2 in H2O‚ shake well‚ record observations Bromination in Dark (Electrophilic Addition Halogenation) (Reacts with alkenes) Reagent: Br2 in H2O Observation: decolorization
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other to react twice with a Grignard followed by removal of the protecting group by acid hydrolysis to give final product (C2). Method: Ethyl acetoacetate (30.03g)‚ ethylene glycol (15.01g) and toluene-p-sulphonic acid (0.13g) were added to a 250 cm3 round bottomed flask‚ containing a stirrer bar and toluene (100 cm3)‚ fitted with a condenser and dean-stark head. Solution was heated strongly under reflux using a heater stirrer block for approximately one hour. During heating 4.5 cm3 of water was collected
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Department of Occupational Therapy‚ College of Rehabilitation Sciences University of Santo Tomas‚ Espaňa Street‚ Manila 1008 Date Submitted: February 2‚ 2011 Abstract: Organic compounds hexane‚ heptane‚ cyclohexane‚ cyclohexene‚ benzene‚ and toluene were subjected to different physical and chemical tests todifferentiate their intrinsic physical properties and chemical properties in terms ofstructure and behaviour. Nitration test (test for the presence of aromatic ring)‚ Bromine test (test for
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: Jun. 12‚ 2009) Abstract : 2-Acetylcyclohexanone was synthesized by acylation reaction of acidic anhydride using enamine as organiocatalyst instead of a strong base‚ NaOH‚ resulting in milder reaction conditions. The reaction was conducted in toluene and direct distillation of the reaction mixture before hydrolysis was leaded to a high yield of the pyrrolidine enamine. This condition was leaded good yields (73.6%) without side reactions. Acylation gave an enol form (71.7%) and a keto form (28
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Introduction 3 Results 4 Discussion 6 Conclusion 7 Experimental 7 References 8 Preparation of 2-Acetylcyclohexanone Introduction When hydrogens are present on the α-carbon of ketones (like the reaction used in this experiment)‚ carbonyl compounds and aldehydes‚ they turn the compound slightly acidic1. These functional groups are removed by using a basic solution as shown in (i) below1. The product formed with water is stable only due to resonance‚ but does
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alkene. Apparatus: dropper‚ test tube‚ hot plate Chemical reagents: bromine‚ toluene‚ cyclohexane‚ cyclohexene‚ acidified KMnO4‚ dichloromethane Method A. Bromine test 1.6 clean and dry test tube were taken and were labelled them A until F 2.1ml of dichloromethane were placed into each test tube 3.1 ml of cyclohexane were placed into tubes A and B‚1 ml cyclohexene were placed into test tube C and D‚1ml toluene to test tube E and F 4. 5 drops of bromine water were placed into each test tube
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Analysis of Hydrocarbons Leoncito‚ Alyssa Lynn‚ Libatique‚ Keith Martin P.‚ Ligot‚ Nestlhyn B.*‚ Lim‚ Jamie Therese T. Department of Psychology‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Four organic samples: hexane‚ cyclohexene‚ napthalene and toulene were given to serve as reference standards to characterize and distinguish four unknown given samples. Nitration‚ bromine and basic oxidation testswere conducted to classify the different samples from being an aliphatic‚ or aromatic
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soots and smoke were produced. C6H14 + 19/2 O2 6CO2 + 7H2O Cyclohexene Orange flame burned vigorously. A small amount of black soot and smoke were produced during the burning process. C6H10 + 17/2 O2 6CO2 + 5H2O Toluene Orange flame burned very vigorously. A large amount of black soot and smoke were produced during the burning process. C7H8 + 9O2 7CO2 + 4H2O Unknown A There was orange flame and burned mildly during the burning process. No soots
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