process by which one liquid can be separated from another liquid‚ or a liquid from a nonvolatile solid. In this experiment‚ the distillations of cyclohexane and toluene mixture were carried out. The purpose of this experiment is to compare the efficiency of simple distillation versus fractional distillation for separation of a mixture of toluene and cyclohexane. The mixture was first separated using simple distillation. A simple distillation apparatus was set up and a Thermowell heater containing
Premium Distillation
ORGANIC CHEMISTRY LAB 2: Separation of Organic Liquid Mixtures Introduction: In this experiment‚ a mixture of two compounds‚ cyclohexane and toluene‚ was separated into fractions by the techniques of simple and fractional distillation. The individual fractions that were gathered from the distillation were analyzed using gas chromatography (GC) and used to compare the efficiencies of the two different distillation techniques. The ultimate goal of this experiment was to determine whether simple
Premium Distillation
Lab 1: Alkene Addition: Bromination of (E)-stilbene I. Introduction: 1. The purpose of the experiment was to perform an electrophilic addition reaction by using pyridinium tribromide to brominate (E)-stilbene and to identify whether it formed the meso- or racemic product through melting point analysis. 2. This is the mechanism for the bromination of (E)-stilbene. However‚ this is the mechanism for Br2 and in class we us Pyridinium Tribromide instead due to the difficulties associated
Premium Acetic acid Reagent Stoichiometry
1 Turpentine oil 2 Phenol 3 Toluene 4 BF-3 Acetate 5 Soda Ash Recipe Sr no Raw material In kg 1 Turpentine oil (pinene ) 1455 2 Phenol (100%) 430 3 toluene 900 4 BF-3 acetate 50 5 Soda ash 2 Water for washing 2000 kg TOTAL 2837 YIELD 1925 KG Terpene Phenolic Resin (Polymerization Reaction). Turpentine Oil/ + Phenol + BF3 Catalyst +Toluene Pinene (on 100% basis)
Premium
is to convert toluene to nitrotoluene through the process of aromatic nitration. This is done by electrophilic aromatic substitution. The aromatic organic compound‚ toluene‚ is reacted under mild conditions with an electrophile‚ the nitronium ion‚ resulting in a product of nitrotoluene. Failure to use mild conditions may result in polynitration. Different reaction conditions were studied to understand the effect of nitrating agent concentrations on the results. Initially‚ toluene is combined
Premium Nitration Sulfuric acid Electrophilic aromatic substitution
more completely. The boiling point (bp) of our unknown compounds was taken from the flat regions of the fractional distillation curve. Our unknown mixture contained hexane (bp 69 ºC) and toluene (bp 110.6 ºC). Analysis via gas chromatography allowed us to determine the relative percentage of hexane and toluene at fractions near the beginning and end of our distillations. Relative percentages have been recorded in the table below‚ and our calculations are shown on page 5. Conclusion This week
Premium Distillation Chemical compound
Required: -4 Test tubes -Dropper - Cyclohexane (C6H12) (3ml) - Cyclohexene (C6H10) (3ml) - Toluene (CH3C6H5) (3ml) - Potassium Permanganate solution (KMnO4) .01 mol L-1 (4ml) - Sulfuric Acid (H2SO4) 2mol L-1 (2ml) - Bromine Water (Br2) (5ml) Procedure: Reaction of hydrocarbons with acidified permanganate: 1) Into three separate‚ labeled test tubes place 1 ml of cyclohexane‚ cyclohexene and toluene respectively. 2) In a separate test tube add 4 ml of 0.01mol L-1 KMnO4 to 2 ml of 2mol L-1
Premium Potassium permanganate Acid Bromine
Solvents used were water‚ methanol‚ n-butanol‚ ethylene glycol‚ acetone‚ hexane‚ toluene‚ ethyl acetate‚ and dichloromethane. Then added to the vials was 0.5 mL of isooctane in each one. The vials were then swirled and observed to determine solubility. In part two of the experiment‚ 0.5 mL of concentrated sulfuric acid was added into
Premium Chemistry Ethanol Oxygen
Chemistry : Important Questions For CBSE Class XII ( Haloalkanes and Haloarenes) (Q.1) Choose the incorrect statement about the benzyl chloride: ( 1 mark ) (a) It is less reactive than alkyl halides. (b) It can be oxidized to benzaldehyde by boiling with copper nitrate solution. (c) It is a lachrymatory liquid and answers beilstein’s test. (d) It gives a white precipitate with alcoholic silver nitrate (Q.2) Dry ether The reaction RX + 2Na + RX _______________? R-R + 2NaXis called. ( 1 mark
Premium Chlorine Carboxylic acid Alcohol
less volatile liquid. Thus the temperature has to increase or spike to boil the remaining substance. In the case of toluene and cyclohexane‚ cyclohexane is more volatile and has a lower boiling point. Simple distillation only evaporates and condenses a liquid once where in fractional
Premium Distillation