gasses react under certain conditions. These conditions‚ such as introducing a flame to the gas as well as oxygen and CO2‚ caused other reactions to occur. Experiment Before I began the experiment I gathered all my supplies from the given list in the lab manual. From there I began the actual experiment and diluted the HCL placed in a test tube and then placed the ZN in the tube as well. I placed the stopper and gas delivery plastic system on the test tube and arranged the tube in the well plate
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Melting Point Determination Lab Materials: Graduated pipette Capillary tube Tin wipe Sample Melting temperature apparatus Thermometer Procedure: Take open end of capillary tube and tap it gently into sample. Take tin wipe and place over the opening. Gently tab it so the sample will funnel to the bottom of the tube. You may also use a graduated pipette to accomplish this. Now‚ place the capillary tube in the designated spot in the melting apparatus‚ and once placed‚ turn the apparatus
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| | | |Chem201L | | Determination of an Unknown Compound using Mixed Melting Point Method Winnie Adrian Ibanez‚ Jerome Allan Japitana‚ and Dante Jimenez III Group no. 7‚ 2Chem a Department of Chemistry‚ College of Science‚ University of Santo Tomas‚ España‚ Manila‚ 1015‚ Philippines |ARTICLE INFO
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and Purification of Solids- Part 2- Recrystallization Courtney Percival CH 337 Laboratory‚ Section 037 Department of Chemistry Portland State University‚ Portland OR ABSTRACT INTRODUCTION Recrystallization is a commonly used tool in laboratories when dealing with impure solids. "An effective recrystallization is one in which 1) a high degree of purity is achieved as well as 2) a maximum recovery of sample".1 Solubility‚ the tendency of a substance to dissolve in a liquid‚ is an important physical
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Hsieh Experiment 2: Boiling Points o Date experiment was performed: September 16‚ 2011 o Objective: To determine the boiling point of organic compounds such as tert-butyl alcohol‚ sec-butyl alcohol‚ n-butyl alcohol‚ and an unknown. o Principle: Boiling point is the temperature at which gas and liquid phases coexist in equilibrium. At this temperature‚ the vaporization rate and the condensation rate are equal. The liquid and vapor reach a state of dynamic equilibrium: liquid molecules evaporate
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Organic Chemistry Lab/ Chem 234 02/17/13 Lab 2: Melting Points Purpose: To determine the purity of a substance using melting point as physical property. We must also learn how to identify an unknown compound using its melting point. We got to identify an unknown compound using mixture melting point and finally we must learn to obtain an accurate melting point using Mel-Temp apparatus. Procedure: Set voltage to obtain the desired heating rate at the anticipated melting point range. The voltage
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average set of results by about 2‚ but‚ when graphing the alkalise by the boiling and melting point they both follow the same slope‚ it continues to rise just like the results gathered in the example do. 2. Which of the 2 unknown substances was which? How did you figure this out? The two unknown substances were the methanol and propenol because each of them were being tested in this experiment to discover the boiling point of each of these alcohols by analysing each of their temperatures to eventually
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PRE-LAB REPORT Lab: Density of Liquids and Solids Purpose of the experiment: The purpose of this lab is to help understand how to resolve the density of liquids and solids. Also‚ the lab is supposed to teach us how to record lab data and how to measure volume and mass the correct way. Lastly‚ it’s designed to help us understand significant values and its relationship to measurements and data recording. Lab Techniques: One technique that will be used during this lab is comparing the
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and Melting Point Objectives 1. To gain proficiency in constructing a graph and plotting data points. 2. To determine the freezing points of a compound from the graph of decreasing temperature versus time. 3. To determine the melting points of a known and unknown compound. Introduction Physical changes are the changes in the physical properties of a substance (Moore‚ Stanitski & Jurs‚ 2009). Freezing point is the fixed temperature at which a pure liquid converted into crystalline solid. Melting
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Recrystallization and Melting Point of Benzoic Acid Organic Chemistry 1 10/4/12 Abstract Recrystallization was done to remove impurities from the sample. The percent recovery of benzoic acid during recrystallization is 23.02%. The difference between the pure and impure samples was observed by comparison of melting points. It was found that impure sample had a lower and wider melting point range of 120.1-122.2 (C). The pure sample melting point range was 121.3-122.5 (C). These ranges helped determine
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