Results My unknown sample was number 18. I did three melting point trials‚ which resulted in a melting point range of approximately 120°C to 122°C‚ as shown in Table 1. I also did two mixed melting point trials using Benzoic Acid and Succinimide‚ as shown in Table 2. Percent recovery is 28.26 grams. Table 1: Unknown Melting Point Trials Trial Melting Point 1 120°C – 122°C 2 120°C – 122°C 3 119°C - 122°C Table 2: Mixed Melting Point Trials Trial Benzoic Acid MP Unknown #18 MP Succinimide
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Electrophilic Aromatic Iodination of Vanillin Purpose: The purpose of this laboratory experiment is for an aromatic compound to undergo an electrophilic substitution reaction. To carry this out‚ our method combines sodium iodide and common bleach as the oxidizing agent in aqueous alcohol as the solvent. Balanced Chemical Equations: Physical Properties: Name of Chemical Chemical Structure Molar Mass (g/mol) BP/MP (ºC) Density (g/mL) Mass/Vol. Used Purpose 3-methoxy-4-hydroxybenzaldehye
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2.4.4. Toxicokinetics of MT: Both carbendazim and Methyl Thiophanate are classified as benzimidazole fungicides. Carbendazim is a major metabolite of benomyl with closely similar structural and toxicological characteristics. Methyl Thiophanate is also structurally related to both carbendazim and benomyl. Both benomyl and carbendazim are well absorbed after oral exposure (80–85%) but poorly absorbed after dermal exposure (1 or 2%) in rats‚ mice‚ dogs and hamsters. The major
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Isolation‚ purification and characterization of alkaloid caffeine from tea leaves Date Submitted: September 3‚ 2014 Abstract Caffeine is one of the main constituents of tea leaves. In this experiment‚ 0.0039 g of pure caffeine was isolated from tea leaves. This was done through solid-liquid extraction followed by multiple liquid-liquid extraction. Then crude material obtained was then purified by sublimation. The isolated caffeine was subjected to thin layer chromatography (TLC) together
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RESULTS AND CALCULATIONS Ligroin Toluene Ethanol H2O Anthracene Did not dissolve Slightly dissolved Did not dissolve Did not dissolve Benzoic acid Did not dissolve Dissolved Slightly dissolved Did not dissolve Phthalic acid Almost dissolved Almost dissolved Did not dissolve Dissolved Resorcinol Dissolved Dissolved Dissolved Dissolved Sodium naphthionate Did not dissolve Did not dissolve dissolved Dissolved Table 1. Results for the five compounds tested in four different solvents. Functional Group
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Nitration of Methyl Benzoate Date of Completion: February 29‚ 2012 Date Report Submitted: March 14‚ 2012 Objective of Experiment: The purpose of this experiment is was to synthesize methyl 3-nitro benzoate from methyl benzoate through an electrophilic aromatic substitution reaction. Chemical Equation: Materials: Name of Compound Molecular weight MP/BP Grams Used Moles Used Methyl benzoate 136.16 g/mol -12.5 OC /199.6 OC 0.28g 2.056*10-3 Sulfuric acid 63.01 g/mol 10 OC /337OC 0
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Esterification and Hydrolysis: Methyl Benzoate by Fisher Esterification Nitration of Methyl Benzoate Jingling Li 2/16/2014 Purpose of the experiment: To understand the mechanisms for Fisher esterification reactions as an equilibrium process and hydrolysis is the reversal reaction of esterification. Nitrate methyl benzoate by an electrophilic aromatic substitution reaction. Summary of procedures: Add sulfuric acid to the mixture of benzoic and methanol‚ heat up the mixture to 65 oC
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Special Report Methyl ethyl ketone – A techno-commercial profile M ethyl ethyl ketone (MEK or 2-butanone) is an organic compound with the formula CH3C(O)CH2CH3. Its CAS number is 78-93-3. The colorless liquid ketone has a sharp‚ sweet odour of butterscotch and acetone. It is produced industrially on a large scale‚ and also occurs in trace amounts in nature. It is soluble in water and is commonly used as an industrial solvent. With natural and synthetic resins‚ MEK produces solutions with low viscosity
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Lab 8- nitration of Methyl I Benzonate Date of experiment: INTRODUCTION: The nitration of methyl benzoate is an example of an electrophilic aromatic substation reaction. In the experiment the electrophile was the nitronium ion and the aromatic compound was methyl benzoate and with addition of nitrating solution Methyl 3-nitrobenzoate was the product. Methyl benzoate Methyl 3-nitrobenzoate MATERIALS AND METHODOLOGY: The procedures for this experiment
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Analysis of Hydrocarbons Jessa Grace B. Castillo* and Stephanie Chua Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines ______________________________________________ Hydrocarbons are organic compounds containing only hydrogen and carbons and further divided in major types. Hydrocarbons react differently in reagents. The basis of determining an unknown hydrocarbon is due to the differences in reactions of hydrocarbons. An unknown compound is determined using tests.
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