Quiz #1 Attempt 1 Written: Jul 7‚ 2012 9:48 AM - Jul 7‚ 2012 9:50 AM Submission View Your quiz has been submitted successfully. Question 1 1 / 1 point At what time do you have to complete your online prelab assignment to be allowed to participate in the lab? Question options: A week before the lab Day before the lab at 10 pm The morning of lab day at 8 am One hour before the lab Question 2 1 / 1 point Which materials/chemicals belong in the desiccator? Question options: Drying
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Spectroscopic Analyses Data tables IR Spectroscopy Hydrobenzoin Peaks (cm-1) | Stretches | Intensity | 3332 (cm-1) | O—H stretch | Strong and broad | 3027 | C—H stretch | Medium and Weak | 14450-1620 (cm-1) | Benzene ring stretch | Medium | Benzil Peaks (cm-1) | Stretches | Intensity | 3062 (cm-1) | Csp2—H stretches | Strong | 1677 (cm-1) | C==O stretch | Strong | 1445 | Benzene ring stretch | Strong | 936
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of dibenzyl ketone (1‚3-diphenyl-2-propanone) with benzil in the presence of base. The reaction then proceeded with an aldol condensation reaction.5 This product was obtained using extraction (reflux)‚ recrystallization and vacuum filtration to separate the product from the waste. Experiment Scheme: Figure 1: Experiment Reaction5 Figure 2: Step wise reaction mechanism including aldol condensation reaction5 Procedure: About 1.55-g of benzil‚ 1.51-g of dibenzylketone and 12-mL of ethanol were
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forming hydronium. A carbonyl is formed as well as nitrogen dioxide gas. Simultaneously the oxygen separates itself from nitrogen dioxide by pushing its electrons onto the positively charged nitrogen. This forms benzil and nitrogen dioxide gas. The next series of reactions will occur using the benzil product formed and potassium hydroxide. Next‚ there is a nucleophilic
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chromatography 3. Separation of a three – component mixture by extraction 4. Completion of experiments from day 1 to 4 5. NMR workshop 6. Sandmeyer Reaction: Preparation of p-chloronitrobenzene 7. Synthesis of benzilic acid from benzil 8. Aldol Condensation: Preparation of ethyl cinnamate 9. Isolation of caffeine from tea 10. Completion of isolation of caffeine from tea 11. Catchup day and completion of experiments School of Chemistry University
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point 99 Grainy yellow Becoming all liquid 101 Clear 2nd trial Temperature (¡ÆC) Observation Unmelted Shiny light yellow crystal First liquid appear point 95 Grainy yellow Becoming all liquid 97 Clear C. Melting point of mixture (Unknown + Benzil) Temperature (¡ÆC) Observation Unmelted Shiny light yellow crystal First liquid appear point 95 Grainy yellow Becoming all liquid 97 Clear ¥±. Discussion of results Assessment of sample purity for a known substance. By comparing observed range
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solvents‚ melting point (for solids)‚ and boiling point (for liquids). In this experiment‚ we will use melting point‚ boiling point‚ and solubility to identify certain solids and liquids. First‚ we will melt benzoic acid‚ benzoin‚ and an unknown substance. I believe the benzoin will have a small range melting point because it is a pure substance.
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Mapua Institute of Technology School of Chemical Engineering and Chemistry Muralla St.‚ Intramuros‚ Manila Melting Point and Boiling Point of Organic Compounds Group No. 5 Manacup‚ Cris Vincent L. Oblena‚ Adrian D. Ong‚ Joshua Jyro B.* *Leader ABSTRACT In compounds‚ two of the physical properties affected by the varying structures are melting point and boiling point. Through the use of the Thomas-Hoover Melting Point Apparatus or the micro method‚ the melting and boiling point of
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the resin exuded from the bark of several species of Styrax trees. The fragrant resin smells like vanilla and is sometimes known as “gum benzoin”. It’s used to make incense and to slow fragrance release in perfumes. Benzoates are derived from benzoic acid. Today benzoic acid is made in the laboratory from other chemicals instead of being extracted from gum benzoin. Cinnamon contains benzoic acid. Source: AliciaC Benzoic Acid and Sodium Benzoate Pure benzoic acid is a white to colorless solid
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Objective: The purpose of this experiment was to prepare the Grignard reagent methylmagnesium iodide and react it with benzoin to form the 3o alcohol 1‚2-diphenyl-1‚2-propanediol‚ through an addition reaction pathway. Introduction: Grignard reagents are alkyl or aryl-magnesium halides that act as the nucleophile in Grignard reactions‚ where ketones are reacted with the reagent‚ then treated with acid to produce an alcohol. In the case of this experiment‚ methylmagnesium iodide was created
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