Experiment #10 Volumetric Analysis The Titration of Acids and Bases Purpose This experiment will allow you to gain practical experience in the preparing standard solutions‚ using a pipette and a buret‚ and performing standard titrations. You will use this experience to experimentally determine the concentration of acetic acid in an unknown solution. There are three parts to this experiment‚ they are 1. Preparation a standard solution of oxalic acid (~0.07 M) 2. Preparation a sodium
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IUPUI October 12‚ 2012 Titration of Acids and Bases Introduction According to Arrhenius definition‚ acid is substance that produces H3O+ ion while base is substance that produces OH- ions. The reaction between acid and base often yields the products of salt and water. The formation of water in this neutralization reaction is caused by the combination of H3O+ and OH- ions. In order to determine the concentration of an unknown acid and base‚ a method called acid-base titration is used. The end of
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hydroxide solution to 50ml. 2. Pipette the KH(C8H4O4) solution into a conical flask. Use three drops of phenolphthalein as the indicator. 3. Titrate carefully until a colour change from colourless to pink is observed. 4. Perform a rough titration first‚ then repeat until 3 concordant
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Experiment 4 SOLUTION STOICHIOMETRY ACID-BASE TITRATIONS Determination of the Percent Acetic Acid in Vinegar Objectives: (1) To introduce and use the concept of solution stoichiometry (2) To specifically use solution stoichiometry to determine the percent of acetic acid in vinegar. (3) To prepare a standard solution by the method of titration. Consider the following balanced chemical equations: (1) HCl + NaOH ------> NaCl + HOH (2) H2SO4
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Titration KMnO4+ FeSO4 12/2/2013 At Alsadek Scientific Association Prepared by: Zainab Alfakih & Jinan Krayem Teacher: Dr. Hiba Nassar Contents Introduction 2 Objectives 3 Theoretical Study 3 Definitions 3 Derivations 3 Equipment 4 Setup 5 Procedures 5 Results 6 Discussion 7 Conclusion 8 References 9 I. Introduction: Oxidation Reduction reactions are chemical reactions in which substances undergo changes in oxidation state. Oxidation is defined as the
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Cisplatin Resources 1. M. H. Hanigan and P. Devarajan‚ “Cisplatin nephrotoxicity: molecular mechanisms‚” Cancer Therapy‚ vol. 1‚ pp. 47–61‚ 2003. 2. Santiago Gómez-Ruiz‚ Danijela Maksimović-Ivanić‚ Sanja Mijatović‚ and Goran N. Kaluđerović‚ “On the Discovery‚ Biological Effects‚ and Use of Cisplatin and Metallocenes in Anticancer Chemotherapy‚”Bioinorganic Chemistry and Applications‚ vol. 2012‚ Article ID 140284‚ 14 pages‚ 2012. 3. N/A 4. Santiago Gómez-Ruiz‚ Danijela Maksimović-Ivanić‚ Sanja
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1. Aim To determine the percentage of aspirin in different commercial preparations and to find which is the best value for money 2. Hypothesis The greater the percentage of acetylsalicylic acid (ASA) in the tablet‚ more powerful and efficient the aspirin would be due to the way aspirin works in human’s body. Aspirin is often used to alleviate the pain‚ and the sensation of pain is mainly attributed to a chemical substance called prostaglandins‚ which is responsible to send a strong signal
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Introduction: The purpose of this lab was to learn how to use salicylic acid to make aspirin. Aspirin is the most widely used over-the-counter drug in the world. The average tablet contains about 325 milligrams of acetylsalicylic acid with an inert binding material such as starch. Aspirin is used to relieve pain‚ reduce inflammation‚ and lower fever. Aspirin originally was derived by boiling the bark of the white willow tree. Although the salicin in willow bark has analgesic properties‚ purified
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Table of Contents Introduction Materials Chemicals Equipment Safety Containers Measuring Devices Other Equipment Procedure Synthesis of Aspirin Crystalizing the Aspirin Recrystallizing the Crude Aspirin Finding the Melting Point Range Safety Precautions Acetic Anhydride Sulphuric and Salicylic Acid Heating Observations Mass of Aspirin Synthesized Melting Point Calculations Percentage Yield Maximum Yield Crude Product Final Product Melting Range Percentage Error Crude
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b. Characterization of Aspirin B. Set – up Fig. 11.1. Suction Filtration Set – up C. Table 11.1 List of Necessary Chemicals Sample Structure Purpose Physical Properties Hazards Salicylic Acid Starting Material Appearance: white powder Molar Mass: 138.12 g/mol Melting Point: 1590C Boiling Point: 2110C Density: 1.44 g/cm3 Mildly irritating (pulmonary irritants). Harmful by inhalation‚ ingestion and through skin absorption. Acetic Anhydride
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